• Search Research Projects
  • Search Researchers
  • How to Use
  1. Back to project page

1993 Fiscal Year Final Research Report Summary

Reliable High Pressure Technique for Material Synthesis.

Research Project

Project/Area Number 04044033
Research Category

Grant-in-Aid for international Scientific Research

Allocation TypeSingle-year Grants
SectionJoint Research
Research InstitutionInstitute of Materials Science, University of Tsukuba

Principal Investigator

WAKATSUKI Masao  Instutute of Materials Science, University of Tsukuba, Professor, 物質工学系, 教授 (50114153)

Co-Investigator(Kenkyū-buntansha) 洪 時明  成都科技大, 高温高圧物理研究所, 助教授
羅 湘捷  成都科技大, 高温高圧物理研究所, 助教授
丁 立業  成都科技大, 高温高圧物理研究所, 教授
〓 清泉  成都科技大, 高温高圧物理研究所, 教授
TOKUSHIGE Keinosuke  Technology Administration Division, Ishikawajima-Harima Heavy Industries, Ltd.,, 技術本部, 課長
KAGI Hiroyuki  Instutute of Materials Science, University of Tsukuba, Research Associate, 物質工学系, 助手 (70233666)
TAKANO Kaoru  Instutute of Materials Science, University of Tsukuba, Associate Professor, 物質工学系, 助教授 (60133005)
OHSUKA Kazuhiro  Instutute of Materials Science, University of Tsukuba, Professor, 物質工学系, 教授 (50029881)
SUENO Shigeho  Instutute of Earth Science, University of Tsukuba, Professor, 地球科学系, 教授 (30110513)
HONG Shiming  Instutute of High Temperature-High Pressure Physics, Chengdu University of Scien
LUO Xiaoxiao  Instutute of High Temperature-High Pressure Physics, Chengdu University of Scien
DING Liye  Instutute of High Temperature-High Pressure Physics, Chengdu University of Scien
GOU Qingquan  Instutute of High Temperature-High Pressure Physics, Chengdu University of Scien
Project Period (FY) 1992 – 1993
KeywordsHigh pressure apparatus / Anvils / Pressure medium / Hydraulic pressure control / Heating power control / Pressure evaluation / Temperature evaluation / Diamond synthesis
Research Abstract

Researches in this subject were performed for two years, 1992 and 1993. Cubic anvils designed in Chengdu University of Science and Technology (CUST) were applied successfully to the cubic anvil-type high pressure-high temperature apparatus designed and installed in University of Tsukuba (TU). The CUST-type anvils are effective in the mechanical stability of confining pressure (avoiding the "blowout" accident), though with a need for improvement of the design to raise the pressure efficiency a little. The pressure medium designed and produced in CUST was better than that used in TU conventionally, in showing improved stability of pressure and temperature because of having less thermal transformation undesirable.
The apparatus of CUST, applied with pressure and heating power controlling units designed and supplied by TU, showed a very improved stability and reproducibility in pressures and temperatures. The CUST apparatus was manifested to be used successfully in experiments of growing seed crystals of diamond from a carbon source of graphite at a small excess pressure. This growth process requires a very stable pressure for a long growth term.
Those results show improvement in experimental ability of the both universities and make one expect further development of finer experiments based on the co-operative characters of the both-type apparatuses.

  • Research Products

    (34 results)

All Other

All Publications (34 results)

  • [Publications] M.Wakatsuki,K.J.Takano,H.Kagi and S.Kumagai: "Real-time evaluation of pressure using the pressure effect on emf of thermocouples." Proc.14th AIRAPT International Conf.on High Pressure Science and Technology,Colorado,1993. (in press). (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] W.Li,H.Kagi and M.Wakatsuki: "Growth of single crystals of diamond by a two-stage method." Proc.3rd IUMRS International Conference on Advanced Materials,Tokyo,1993. (in press). (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 若槻雅男: "金属溶媒によるダイヤモンド合成" New Diamond. 9. 4-13 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] K.J.Takano,K.Shino,A.Izawa,M.Miyahara and M.Wakatsuki: "Detection of pressure-induced phase transition in a diamond anvil cell." Japan.J.Appl.Phys.31(3A). 1268-1274 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Kagi,M.Wakatsuki,S.Hayakawa,F.Nakamura,Y.Gohshi,H.Kanda and J.Isoya: "Characterization of trace nickel in Synthetic diamond and its relation ship to the abundance of substitutional nitrogen." Proc 14th AIRAPT International Conference on High Pressure Science and Technology,Colorado,1993. (in press). (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Kagi,M.Wakatsuki,S.Hayakawa,Y.Gohshi,H.Kanda and J.Isoya.: "Trace amount of nickel in synthetic diamond and its implication to substitutional nitrogen." Proc.3rd IUMRS International Conference on Advanced Materials,Tokyo,1993. (in press). (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] K.Matsumoto,H.Yurimoto,K.Kosaka,T.Nakamura and S.Sueno: "A novel ion imager for secondary ion mass spectroscopy." Electron Devices. 40. 82-85 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] O.Koike,H.Yurimoto,H.Nagasawa and S.Sueno: "Ion microprobe measurements of Mg isotopes in type B1 CAI of Allende meteorite." Proc.NIPR Symp.Antarct.Meteorites.6. 357-363 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] K.Otsuka,T.Ohba,M.Tokonami and C.Wayman: "New description of long period stacking order structures of martensites in β-phase alloys." Scripta Met.29. 1359-1364 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Min Piao,K.Otsuka,S.Miyazaki and H.Hirokawa: "Mechanism of the As temperature increase by predeformation in thermo-electric alloys." Matrials Trans.JIM. 34. 919-929 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 〓立,張茹,洪時明,〓清泉: "用SiC和Ni_<70>Mn_<25>Co_5合金合成金剛石的試験" 高圧物理学報. 1993増巻号. 27 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 曹国英,陳叔〓,李会士,〓清泉: "八面体硼皮金剛石的高圧合成研究" 原子与分子物理学報. 10. 2603-2608 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 羅湘捷,丁立業,蔡民東,呉細芽: "人造金剛石鉄磁性雑質的EPR譜特性分析" 成都科技大学学報. 1993(6). 62-68 (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 丁立業,若槻雅男,羅湘捷: "金剛石生長時高圧融剤中石炭的伝輸及其影響" 高圧物理学報. 8(in press). (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] S-M.Hong and M.Wakatsuki: "Diamond formation from the SiC-Co system under high pressure and high temperature." J.Mater.Sci.12. 283-285 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] S-M.Hong,W.Li,X-P.Jia and M.Wakatsuki: "Diamond formation from a system of Sic and a metal." Diamond and Related Materials.2. 508-511 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] M.Wakatsuki,K.J.Takano and H.Kagi: "Formation process of materials at high pressure:in New Functionality Materials,Vol.C,ed.by T.Tsuruta,M.Doyama and M.Seno" Elsevier,Amsterdam, 91-98 (1993)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] M.Wakatsuki, K.J.Takano, H.Kagi and S.Kumagai: "Real-time evaluation of pressure using the pressure effect on EMF of thermocouples" Proc. 14th AIRAPT International Conf. on High Pressure Science and Technology, Colorado, 1993. in press. (1994)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Wei Li, H.Kagi and M.Wakatsuki: "Growth of single crystals of diamond by a two-stage method" Proc. 3rd IUMRS International Conference on Advanced Materials Tokyo, 1993. in press.

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] M.Wakatsuki: "Synthesis of diamond using metallic solvents (in Japanese)" New Diamond. 9(4). 4-13 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] K.J.Takano, K.Shino, A.Izawa, M.Miyahara and M.Wakatsuki: "Detection of a pressure-induced phase transition in a diamond anvil cell" Japan. J. Appl. Phys.31(A). 1268-1274 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H.Kagi, M.Wakatsuki, S.Hayakawa, F.Nakamura, Y.Gohshi, H.Kanda and J.Iasoya: "Characterization of trace nickel in synthetic diamond and its relationship to the abundance of substitutive nitrogen" Proc. 14th AIRAPT International Conf. on High Pressure Science and Technology, Colorado, 1993. in press. (1994)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H.Kagi, M.Wakatsuki, S.Hayakawa, Y.Gohshi, H.Kanda and J.Isoya: "Trace amount of nickel in synthetic diamond and its implication to substitutive nitrogen" Proc. 3rd IUMRS International Conference on Advanced Materials Tokyo, 1993. in press. (1994)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] K.Matumoto, H.Yurimoto, K.Kosaka, T.Nakamura and S.Sueno: "A novel ion imagery for secondary ion mass spectroscopy" Electron Devices. 40. 82-85 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] O.Koike, H.Yurimoto, H.Nagasawa and S.Sueno: "Ion microprobe measurements of Mg isotopes in type B1 CAI meteorites" Proc. NIPR Antarct. Meteorites. 6. 357-363 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] K.Otsuka, T.Ohba, M.Tokonami and C.Wayman: "New description of long period stacking order structures of martensites in beta-phasealloys" Scripta Met.29. 1359-1364 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Min Piao, K.Otsuka, S.Miyazaki and H.Hirokawa: "Mechanism of the As temperature increase by pre-deformation in thermoelectric alloys" Materials Trans. JIM. 34. 919-929 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] L.Gou, J.Chang, S-M.Hong and Q-Q.Gou: "A trial of synthesizing diamond using SiC and a Ni_<70>Mn_<25>Co_5 alloy (in Chinese)" Chinese Journal of High Pressure Physics. special lssue. 27 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] G-Y.Cao, X-Q.Chen, H-S.Li and Q-Q.Gou: "Study for high pressure synthesis of octahedral diamonds surface-doped with boron (in Chinese)" Chinese Journal of Atomic and Molecular Physics. 10. 2603-2608 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] X-J.Luo, L-Y.Ding, M-D.Chai and X-Y.Wu: "The study of EPR properties of ferromagnetic impurities in synthetic diamond (in Chinese)" Journal of Chengdu University of Science and Technology. 1993(6). 62-68 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] L-Y.Ding, M.Wakatsuki and X-J.Luo: "Transport of carbon in the solvent and its effect on the formation of diamond (in Chinese)" Chinese Journal of High Pressure Physics. 8 in press. (1994)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] S-M.Hong and M.Wakatsuki: "Diamond formation from the SiC-Co system under high pressure and high temperature" J.Mater.Sci.12. 283-285 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] S-M.Hong, W.Li, X-P.Jia and M.Wakatsuki: "Diamond formation from a system of SiC and a metal" Diamond and Related Materials. 2. 508-511 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] M.Wakatsuki, K.J.Takano and H.Kagi: Elsevier, Amsterdam. "Formation process of materials at high pressure", in New Functionality Materials, Vol.C, ed. by T.Tsuruta, M.Doyama and M.Seno, 91-98 (1993)

    • Description
      「研究成果報告書概要(欧文)」より

URL: 

Published: 1995-02-07  

Information User Guide FAQ News Terms of Use Attribution of KAKENHI

Powered by NII kakenhi