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1994 Fiscal Year Final Research Report Summary

A new fringe method for characterization of ROUGHNESS of inner layrs in semiconductor crystals and dielectric thin layrs

Research Project

Project/Area Number 04555006
Research Category

Grant-in-Aid for Developmental Scientific Research (B)

Allocation TypeSingle-year Grants
Research Field Applied materials
Research InstitutionDepartment of Physics, Gakushuin University

Principal Investigator

OGAWA Tomoya  Gakushuin Univ., Dept.of Phys., Professor, 理学部, 教授 (50080437)

Co-Investigator(Kenkyū-buntansha) MA Minya  Gakushuin Univ., Dept.of Phys., Guest Researcher, 理学部, 客員研究員 (60255263)
NARAOKA Kiyoiki  Gakushuin Univ., Dept.of Phys., Guest Researcher, 理学部, 客員研究員
OYAMA Yasunao  Gakushuin Univ., Dept.of Phys., Assistant, 理学部, 助手 (20265573)
Project Period (FY) 1992 – 1994
KeywordsSi wafer / SIMOX / denuded zone / Cz-Si / intrinsic gettering / GaAs wafer / multi-quantum layr / diffraction of light
Research Abstract

A new fringe method was developed for characterization of "roughness" of inner layrs and interfaces in semiconductor devices because the roughness are very important for semiconductor technologies. Here, brightness and clearness, or visibility, of the fringe pattern are determined by scattering from the objects to be surveyed, because size and density of dots and spots which compose the fringes are proportional to size and density of particles and grains located at the interfaces or roughness on the layrs while their scattered intensities are dependent upon refractive index difference between matrix and the objects.
(1) A SIMOX wafer is prepared by proper heat treatments from a silicon wafer showered by heavy but homogeneous implantation of oxygen ions, and thus a thin and flat oxide layr is generated in the wafer. The layr is made of fine oxide particles which efficiently act as light scatterers. The fringe patterns obtained by SIMOX wafers are usually bright and clear with fine dots w … More hich inform us the layr is a homogeneous assemble of fine oxide particles.
(2) when denuded zone and oxide particles for intrinsic gettering (IG) are generated in a CZ-Si wafer after application of proper heat treatments to the wafer, an interface between the zone and the IG region is clearly observed by this fringe method. Oxide particles located near the interface are quantitatively measured, which is very important for planar circuits on the wafer.
(3) Optical quality of multi-layrs with quantum well structure was comprehensively checked by this fringe method because this fringe pattern will be observed only when any optical inhomogeneity is present in the layrs grown on substrate.
(4) Since etch pits and steps on crystal faces indicate crystallographic anisotropy, the light intensities scattered by the pits and steps are dependent upon the direction of incident light against their crystallographic orientations, which has been clearly observed by some GaAs wafers.
To measure "roughness" of inner layrs or interfaces which are unable to measure before this fringe method, a new method has been developed here, which is, of course, governed by an electronic system. Less

  • Research Products

    (21 results)

All Other

All Publications (21 results)

  • [Publications] 小川智哉: "Piled up dislocations in vapour phase grown ZnSe crystals" Philosophical Magazine. (in press). (1995)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 小川智哉: "Defects in β-BaB203 (BBO) crystals observed by laser scanning tomography" J. Crystal Growth. 141. 393-398 (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 小川智哉: "Effect of human blood addition on dendritic growth of cupric chloride crystals in aqueous solutions" J. Crystal Growth. 142. 147-155 (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 小川智哉: "Characterization of GdBa2Cu307 superconducting thin films by a new optical interference fringe method" J. Materials Science. 29. 3702-3704 (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 小川智哉: "Crystal perfection and detection of defects just under wafer surfaces of semiconducting and insulating materials" Institute of Physics, Conference Series. 135. 127-130 (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 小川智哉: "Characterization of interface and surface structures by ultra-thin film interference fringes" Institute of Physics, Conference Series. 135. 267-270 (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 小川智哉: "Materials and Process Characterization for VLSI '94" Asia-Pacific Microanalysis Association, 583 (1994)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Ma & Ogawa: ""Piled-up dislocation in a vapor phase grown ZnSe crystals observed by light scattering tomography"" Phil.Mag. in press. (1995)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Ogawa: ""Detection of defects near a wafer surface by Brewster angle illumination"" Materials and Process Characterization for VLSI,1994 ed. by X.F.Zong, M.K.Balaz & J.J.Wang, Asia-Pacific Microanalysis Associaton, Shanghai, China. 34-38 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Shibata & Ogawa: "Effect of human blood addition on dendritic growth of cupric chloride crystals in aqueous solutions" J.Crystal Growth. 142. 147-155 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Mai & Ogawa: "Characterization of GdBa2Cu307 superconducting thin films by a new optical interference fringe method" J.Materials Science. 29. 3702-3704 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Tan & Ogawa: "Defects in beta-BBO(beta barium borate) crystals observed by laser scanningtomography" J.Crystal Growth. 141. 393-398 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Nango & Ogawa: "Crystal perfection and detection of defects just under wafer surfaces of semiconducting and insulating materials" Inst.Phys.Conf.Ser. No. 135. 127-130 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Lu & Ogawa: "Characterization of interface and surface structures by ultra-thin film interference fringes" Inst.Phys.Conf.Ser. No.135. 267-270 (1994)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Lu & Ogawa: "Effect of surface structure upon ultra-thin interference fringes" J.Materials Research. 8. 2315-2318 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Ogawa: "Characterization of dielectric crystals by light scattering tomography" Ferroelectronics. 142. 19-29 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Ogawa: "Light scattering tomography to evaluate and characterize crystals" From Galileo's OCCHIALINO to Optoelectronics ed.by P.Mazzoldi, World Science, Singapore. 578-585 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Ataka & Ogawa: "Nucleation and growth of oxide precopitates in CZ-Si wafers" J.Materials Research. 8. 2889-2892 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Ogawa: "Optical characterization of silicon wafers for ULSI" Materials Sci. & Eng. B 20. 172-174 (1993)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Sakai & Ogawa: "A study on IR light intensities scattered from defects in an In-doped LEC CaAs crystalsas functions of wava-length andintensity of bias light superposed on the defects" Jpn.J.Appl.Phys. 31. 2945-2948 (1992)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Sakai, Kondo & Ogawa: "Raman scattering tomography studies on semi-conductors" Semicond.Sci. Technol. 7. A279-A282 (1992)

    • Description
      「研究成果報告書概要(欧文)」より

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Published: 1996-04-15  

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