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1996 Fiscal Year Final Research Report Summary

Developement of in situ structural analyzes of bonding between different materials

Research Project

Project/Area Number 06555209
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section試験
Research Field Material processing/treatments
Research InstitutionNagoya University

Principal Investigator

KIZUKA Tokushi  Nagoya University School of Engineering, Research Associate, 工学部, 助手 (10234303)

Co-Investigator(Kenkyū-buntansha) ISHIDA Yoichi  Tokyo University Faculty of Engineering, Professor, 工学部, 教授 (60013108)
TANAKA Nobuo  Nagoya University School of Engineering, Associate Professor, 工学部, 助教授 (40126876)
Project Period (FY) 1994 – 1996
Keywordsbonding / Transmission electron microscopy / hetero bonding / in situ analysis / atomic resolution
Research Abstract

Atomic scale solid state direct bonding in time-resolved high-resolution transmission electron microscopy was realized by using the piezodriven specimen holder. The structural variations of atomic arrangements in approach, contact, bonding and separation processes between two gold tips were observed at atomic scale. It was found that the nanometer-sized gold tips contact spontaneously when the tips approach at the critical distance corresponding to a few atomic distance underi intense electron irradiation. The crystallographic boundary forms after the contact. A few layrs near the surfaces and bonding-boundaries are responsible for the bonding and separation processes. New kinds of atomic scale mechanical tests such as the friction test, the compressing, tensile and shear deformation tests were proposed.

  • Research Products

    (13 results)

All Other

All Publications (13 results)

  • [Publications] T. Kizuka et al.: "Cross-sectional high-resolution transmission electron microscopy of atomic scale contact and noncontact-type scannings on Sold surfaces" Phys. Rev.B55 (in print). (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] T. Kizuka et al.: "Time-resolved HREM of solid state direct bonding of gold and zinc oxide nanocrystallites" Appl. Phys. Lett.(in print). (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] T. Kizuka et al.: "Time-resolved HREM of atomic scale solid state direct bonding of Sold tips" J. Electron Microscopy. 46 (in print). (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] T. Kizuka et al.: "Time-resolved atomic observation of fragmentation of gold clusters by HREM" Surf. Rev. Lett.,. 3. 1187-1190 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] T. Kizuka et al.: "Critical grainsize for structural transformation in vacuum-deposited molybdenum films" Surf. Rev. Lett.,. 3. 1181-1185 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] T. Kizuka et al.: "Structure and hardness of narocry stalline silver" J. Mat. Sci.(in print). (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] T.Kizuka: "Nanometer scale electron beam processing and in-situ atomic observation of vacuum-deposited MgO films in high-resolution electron microscopy" Phil.Mag.A. 71. 631-639 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] T.Kizuka: "Time-resolved atomic observation of fragmentation of gold clusters by high-resolution electron microscopy" Surf.Rev.Lett.3. 1187-1190 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] T.Kizuka: "Critical grain size for structural transformation in vacuum-deposited molybdenum films" Surf.Rev.Lett.3. 1181-1185 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] T.Kizuka: "Dynamic high-resolution electron microscopy of grain boundary migration and structural transformation in nanocrystalline ZnO" Trans.JIM. (in print). (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] T.Kizuka: "Structure and hardness of nanocrystalline silver" J.Mat.Sci.(in print). (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] T.Kizuka: "Cross sectional high-resolution transmission electron microscopy of atomic scale contact and non-contact type scanning on gold surfaces" Phys.Rev.B. (in print). (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] T.Kizuka: "Time-resolved high-resolution electron microscopy of solid state direct bonding of gold and zinc oxide nanocrystallites" Appl.Phys.Lett.(in print). (1997)

    • Description
      「研究成果報告書概要(欧文)」より

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Published: 1999-03-09  

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