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1996 Fiscal Year Final Research Report Summary

結晶の照射効果に及ぼす電子励起および格子励起の相乗効果

Research Project

Project/Area Number 07455260
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Physical properties of metals
Research InstitutionKYUSHU UNIVERSITY

Principal Investigator

KINOSHITA Chiken  Kyushu University, Faculty of Engineering, Professor, 工学部, 教授 (50037917)

Co-Investigator(Kenkyū-buntansha) YASUDA Kazuhiro  Kyushu University, Faculty of Engineering, Research Associate, 工学部, 助手 (80253491)
SHIIYAMA Kenichi  Kyushu University, Faculty of Engineering, Research Associate, 工学部, 助手 (30243900)
MATSUMURA Syo  Kyushu University, Faculty of Engineering, Associate Professor, 工学部, 助教授 (60150520)
Project Period (FY) 1995 – 1996
KeywordsCeramics / MgAl_2O_4 / Al_2O_3 / irradiation / TEM / radiation damage / ionization / displacement
Research Abstract

We have investigated the role of ionization and PKA (primary knock on atom) energy spectrum on the physical properties in ceramic insulators. The ceramics studied in this study are stoichiometric- and nonstoichiometric- magnesium aluminate spinel, alumina and magnesia.
In situ observations of microstructural evolution were carried out under concurrent irradiation with ions and electrons in TEM-accelerator facilities. We have found that the intense ionization and/or subthreshold nuclear energy, that is the nuclear energy which does ont produce displacements of atoms, suppress the formation of interstitial dislocation loops or promote the formation of bubbles in ceramics. Results were discussed in terms of ratio of ionizing to nuclear stopping power, energy density in displacement of cascades and the flux distribution of focused electron beam. An importance of cation diffusion driven by low energy electron irradiation has been found for the concurrent irradiation effects.
A special TEM holders has been developed in this study for in situ measurements of electrical conductivity under electron irradiation in a high voltage electron microscope. The ionizing radiation increases electrical conductivity (RIC : radiation induced conductivity) in ceramic insulators at the early stage of irradiation. Displecement damage can be important at high dose irradiation. We have also discussed the mechanism of thermally stimulated conductivity which can be a critical problem for fusion insulators.

  • Research Products

    (24 results)

All Other

All Publications (24 results)

  • [Publications] T.Sonoda,H.Abe,C.Kinoshita and H.Naramoto: ""Formation and growth process of defect clusters in magnesia under ion irradiation"" Nuclear Instrument and Method,Physical Research. B(印刷中). (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] T.Sonoda,C.Kinoshita and A.Manabe: ""Effects of OH^- ions on the formation process of defect clusters in MgO crystals"" J.Nuclear Materials. (印刷中). (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] K.Yasuda,C.Kinoshita et al.: ""Concurrent irracliation effects with ionization and displacement on the formation precess of defect clusters in magnesium" Proc.of the 7th inf.symp.on advanced nuclear energy research. (印刷中)aluminate spinal. (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] N.Yu,K.E.Sickafus,M.Nastasi,K.Yasuda et al.: ""A study of ion-beam induced lattice damage in flouride structure materials : zirconia and calucium flouride"" Nuclear Instrument and Method,Physical Research. B(印刷中). (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] M.M.R.How lader,T.Izu,C.Kinoshita et al.: ""In situ measurements of electrical conductivity of alumina under electron irradiation in a high voltage electron microscop" J.Nuclear Materials. 239. 245-252 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] C.Kinoshita and S.J.Zinkle: ""Potential and limitations of ceramics in terms of structural and electrical integrity in fusion environments"" J.Nuclear Materials. 233-237. 100-110 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] K.Shiiyama,T.Izu,C.Kinoshita et al.: ""Measurements of electrical conductivity of ceramics under electron irradiation in a high voltage electron microscope"" J.Nuclear Materials. 233-237. 1332-1335 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] K.Yasuda,C.Kinoshita M.Kutsuwada et al.: ""Nucleation and growth process of defect clusters in copper during helium ion irradiation"" J.Nuclear Materials. 233-237. 1332-1337 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] C.Kinoshita,H.Abe S.Maeda et al.: ""Effects of concurrent irradiation with ions and electrons on the formation process of defect clusters in covalent and ionic crystals"" J.Nuclear Materials. 219. 152-160 (1995)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] C.Kinoshita,K.Fukumoto K.Fukuda et al.: ""Why is magnesium aluminate spinal radiation resistant material?" J.Nuclear Materials. 219. 143-151 (1995)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Abe,C.Kinoshita and Y.Denda: ""Stability of cascades under ion and electron irradiation in germanium"" Proc.of Materials Research Society Symposium. 373. 487-492 (1995)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Abe,H.Naramoto and C.Kinoshita: ""Amorphization of graphite under ion or electron irradiation"" Proc.of Materials Research Society Symposium. 373. 383-388 (1995)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] S.J.Zinkle, C.Kinoshita: "Defect production in Ceramics" J.Nucl. Mater.(in press). (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] T.Sonoda, H.Abe, C.Kinoshita and H.Naramoto: "Formation and growth process of defect clusters in magnesia under ion irradiation" Nucl. Inst. Meth. Phys. Res. B.(in press). (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] T.Sonoda, C.Kinoshita and A.Manabe: "Effects of Oh ions of the formation process of defect clusters in MgO crystals" J.Nucl. Mater.(in press). (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] K.Yasuda, C.Kinoshita, R.Morisaki and H.Abe: "Concurrent irradiation effects with ionization and displacement on the formation process of defect clusters in magunesium aliminate spinel" Proc. of the 7th international ymposium on advanced nuclear energy research, Takasaki, Japan (JAERI). (in press). (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] N.Yu, K.E.Sickafus, M.Nastasi, K.Yasuda et al.: "A study of ion-beam induced lattice damage in flouride-structure materials : zirconia and calucium flouride" Nucl. Inst. Meth. Phys. Res.B (in press). (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] C.Kinoshita and S.J.Zinkle: "Potential and limitations of ceramics in terms of structural and electricak integrity in fusion environments" J.Nucl. Mater.233-237. 100-110 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] K.Shiiyama, T.Izu, C.Kinoshita, M.Kutsuwada: "Measurements of electrical conductivity of ceramics under electron irradiation in a high voltage electron microscope" J.Nucl. Mater.233-237. 1332-1335 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] K.Yasuda, C.Kinoshita M.Kutsuwada and H.Hirai: "Nucleation and growth process of defect clusters in copper during helium ion irradiation" J.Nucl. Mater.233-237. 1051-1056 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] C.Kinoshita, H.Abe, S.Maeda and K.Fukumoto: "Effect of Concurrent Irradiation with Ions and Electrons on the Formation Process of Defect Clusters in Covalent and Ionic Crystals" J.Nucl. Mater.219. 152-160 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] C.Kinoshita, K.Fukumoto, K.Fukuda, F.A.Garner and G.W.Hollenberg: "Why is Magnesia Spinel Radiation-Resistant Material?" J.Nucl. Mater.219. 143-151 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H.Abe, C.Kinoshita and Y.Denda: "Stability of Cascades under Ion and Electron Irradiation in Germanium" Mat. Res. Soc. Symp. Proc.Vol.373. 487-492 (1995)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H.Abe, H.Naramoto and C.Kinoshita: "Amorphization of Graphite under Ion or Electron Irradiation" Mat. Res. Soc. Symp. Proc.Vol.373. 383-388 (1995)

    • Description
      「研究成果報告書概要(欧文)」より

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Published: 1999-03-09  

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