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1996 Fiscal Year Final Research Report Summary

Development of Fatigue Properties Evaluation System for Mesoscopic Component for Composite Materials

Research Project

Project/Area Number 07555622
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section試験
Research Field Materials/Mechanics of materials
Research InstitutionKYOTO UNIVERSITY

Principal Investigator

HOJO Masaki  Kyoto University, Mesoscopic Materials Res.Ctr., Associate Professor, 工学部, 助教授 (70252492)

Co-Investigator(Kenkyū-buntansha) TAKAHASHI Jun  National Instiute of Materials and Chemical Research, AIST,Senior Researcher, 物質工学工業技術研究所, 主任研究官
MATSUBARA Teruji  Shimadzu Cooporation, Testing and Weiching Equipment Div., Group Head, 試験計測事業部, 主任
NOGUCHI Kenich  Toray Industries, Inc., Composite Materials Research Lab., Senior Researcher, 複合材料研究所, 主席研究員
OCHIAI Shojiro  Kyoto University, Mesoscopic Materials Res.Ctr., Professor, 工学研究科, 教授 (30111925)
KOMAI Kenjiro  Kyoto University, Dept.Mechanical Engineering Professor, 工学研究科, 教授 (70025948)
Project Period (FY) 1995 – 1996
KeywordsComposite materials / Interface / Fatigue strength / Fiber / Resin / Mesoscopic component / low-load capacity fatigue testing machine / Fracture
Research Abstract

Micro composite test was proposed in this study in order to investigate the interfacial strength of composites. This test keeps the boundary condition of fibers and matrix in real composites, and makes it possible to measure the yield and fracture on the interface. Special fatigue testing machine with very low-load capacity was developed for this microcomposite tests by using electromagnetic actuator. The results are summarized as follows :
(1) Development of special low-load capacity fatigue testing system with electromagnetic actuator
A new type fatigue testing machine of the capacity of 2.5N was developed by using a special electromagnetic actuator. This testing machine can control a very small load down to 10mN.The key point for developing this actuator is the disc type spring which keeps the accuracy of the direction of the loading shaft. Fatigue tests at very low load (several tens of mN) were carried out successfully, and the development of the low-load fatigue testing system was … More almost finished.
(2) Composite mesoscopic component tests with different interfacial strength under static and fatigue loadings
Different levels of surface treatment were carried out on PAN based carbon fiber by varying the amount of electricity through the anodic oxidation method. Acid function increased linearly with increasing the amount of electricity. Then, a model composite which is called "micro composite" was manufactured. In micro composite, the central fiber is surrounded by six fibers, and resin was impregnated among them. The boundary condition of the central fiber is similar to that of fiber in real composites. Interfacial strength was measured by pulling out the central fiber. The interfacial strength under static loading depends on the surface treatment of fiber. However, the interfacial strength under fatigue loading was not influenced by the surface treatment of fiber. The results of fatigue tests under different stress ratios showed that the effect of stress ratio was negligible when the fatigue strength is expressed by the maximum stress.
(3) Comparison with macroscopic fatigue properties
The stress-ratio dependency of macroscopic mode II fatigue delamination was completely different from that of interfacial fatigue test. Thus, the mechanism of fatigue fracture is completely different, although the loading mode was similar. Less

  • Research Products

    (12 results)

All Other

All Publications (12 results)

  • [Publications] Masaki Hojo: "Effect of matrix resin on mesomechanism of mode II delamination fatigue crack growth for CFRP laminates" Proceedings of the seventh European conference on composite materials. 1. 81-96 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 北條正樹: "一方向強化CF/PEEK積層板のモードII層間はく離疲労き裂伝ばの破壊機構" 材料. 46. (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 松田聡: "層間高靱化CFRPのモードII層間はく離疲労のメゾ破壊機構" 日本機械学会論文集,A編. 63. 39-45 (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 松田聡: "先進CFRPのモードII層間はく離疲労に及ぼす樹脂靱性の効果" 強化プラスチックス. 42. 49-53 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 辻岡則夫: "炭素繊維表面酸化処理およびサイジング材処理の界面接着への影響" 材料. 46. 163-169 (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 志田穣: "ミクロコンポジット試験による界面の疲労強度評価の解析および実験的検討" 日本機械学会材料力学部門講演会講演論文集(Vol. A). A. 23-24 (1996)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Hojo, M., Matsuda, S., and Ochiai, S.: "Effect of Matrix Resin on Mesomechanism of Mode II Delamination Fatigue Crack Growth for CFRP Laminates" Proceedings of Seventh European Conference on Composite Materials Woodhead Publishing.Vol.1. 81-86 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Hojo, M., Matsuda, S., Higuchi, T., and Ochiai, S.: "Fracture Mechanism for Mode II Propagation of Delamination Fatigue Cracks in CF/PEEK Laminates" Journal of the Society of Materials Science, Japan. Vol.46. (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Matsuda, S., Hojo, M., and Ochiai, S.: "Mesoscopic Fracture Mechanism of Mode II Delamination Fatigue Crack Propagation in Interlayr-Toughened CFRP" Transactions of the Japan Society of Mechanical Engineers, Series A. Vol.63. 39-45 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Matsuda, S., Hojo, M., Ochiai, S., and Higuchi, T.: "Effect of Matrix Resin Toughness on Mode II Delamination Fatigue for Advanced CFRP Lamiantes" Reinforced Plastics. Vol.42. 49-53 (1996)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Tsujioka, N., Maekawa, Z., Hamada, H., and Hojo, M.: "Effect of Surface Oxidation and Sizing Treatment of Carbon Fiber on Interfacial Adhesion" Journal of the Society of Materials Science, Japan. Vol.46. 163-169 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Shida, M., Hojo, M., Ochiai, S., and Sawada, Y.: "Analytical and Experimental Evaluation of interfacial Strength using Micro Composite" Proceedings of the 1996 Annual Meeting of JSME/MMD. Vol.A. 23-24

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      「研究成果報告書概要(欧文)」より

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Published: 1999-03-09  

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