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1999 Fiscal Year Final Research Report Summary

Microscopic analysis of deformation and fracture of metal matrix composites

Research Project

Project/Area Number 09650749
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Composite materials/Physical properties
Research InstitutionHiroshima University

Principal Investigator

SASAKI Gen  Hiroshima Univ., Dept. of mech. eng., Assoc. prof., 工学部, 助教授 (30192595)

Co-Investigator(Kenkyū-buntansha) YOSHIDA Makoto  Hiroshima Univ., Dept. of mech. eng., Research assoc., 工学部, 助手 (80277847)
FUKUNAGA Hideharu  Hiroshima Univ., Dept. of mech. eng., Prof., 工学部, 教授 (90034347)
Project Period (FY) 1997 – 1999
KeywordsMetal matrix composite / TEM / SEM / Fracture / Deformation / Interface / Mechanical property / Structural material
Research Abstract

The metal matrix composites were fabricated by the squeeze casting, semi-solid casting, stirring casting and the hot pressing. Reinforcements used in this study are mainly SiC, AlィイD218ィエD2BィイD24ィエD2OィイD233ィエD2, TiOィイD22ィエD2 particles/whisker/fiber and matrices are aluminum, magnesium and titanium alloys. Furthermore, Niobium/MoSiィイD22ィエD2 lamellar composites were fabricated by hot pressing. At first, the relationship between the fabrication condition and the mechanical properties were investigated. Then, in order to investigate the control factor of the mechanical properties, the microstructure, the deformation and the fracture structure were observed in atomic scale by the scanning and transmission electron microscopy. The main control factors are the deterioration of the reinforcement, the structure changes of the ceramics/matrix interface and the change of the matrix microstructure (or character). We focused the investigation of the effect of interface structure and reaction on the deformation and fracture. By considering the control method of the interface structure, we presented the design principle of the composite fabrication.
Following is the topics in this study. Interface reaction temperature of TiOィイD22ィエD2/Al composite decreased by the doping the third element for the surface of the TiOィイD22ィエD2 particles. Heat stability of the AlィイD218ィエD2BィイD24ィエD2OィイD233ィエD2 whisker / Al, Mg alloy matrix composites increased by the formation of the thin and homogeneous MgAlィイD22ィエD2OィイD24ィエD2 layer on the whisker. Nb/MoSiィイD22ィエD2 lamellar composites having high fracture toughness was fabricated by the addition of the third elements to MoSiィイD22ィエD2 sheet. In fiber-reinforced composites, it is found that the creep rupture lifetime was predicted by the probability model considering the time dependence of the load resistance of the fiber.

  • Research Products

    (62 results)

All Other

All Publications (62 results)

  • [Publications] L.J.Yao: "Reactivity of aluminum borate whisker with aluminun alloys"Mat.Sci.Eng.. A225. 59-68 (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] G.Sasaki: "Microstructure of TiO_2 (rutile)/Al composite"Proc.ICCM-11. 7・3. 24-31 (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Fukunaga: "Reaction Squeeze Cast processing and intermetallic dispersed aluminum matrix composites"Proc.ICCM-11. 7・3. 182-190 (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Fukunaga: "Reactioa Squeeze Casting process"Proc.of International conference on thermomechanical processing of steels&other materials(THERMEC'97). 7・1. 1111-1117 (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] G.Sasaki: "TiO_2 composites by squeeze casting and hardness/microstructure change by heat treatment"Proc.of Australasia-Pacific forum on intelligent processing and manufacturing of materials (IPMM '97). 2. 872-882 (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] L.Yao: "Interfacial Reaction and Interface Structure of Al_<18>B_40_<33>w/Al Composites"Proc.5th Japan lnternational SAMPE Symposium a Exhibition (JISSE-5). 10. 423-428 (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 土取功: "TiO2/Al複合材料の固相反応における微量元素添加による反応促進効果"日本金属学会誌. 61・6. 544-552 (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] S.P.Lee: "Processing and Interfacial Reaction of Nb/MoSi_<12> Laminate Composites and Their Effects on Impact Properties"Proc.European conference on composite maierials (E;CCM-8). 6・4. 263-270 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] L.J.Yao: "Effect of lnterfacial Reaction on Bending Strength of Al_<18>B_4O_<33> Whisker Reinforced Aluminum Composites"Meta.Mat.Trans.A. 29A・5. 1517-1525 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] S.P.Lee: "Interfacial Microstructures and Impact Properties for Nb/MoSi_2 Laminate Composites"Composite Interface. 5・5. 405-419 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] J.Pan: "Effect of lnterface Reaction on Strength 0f Al_<18>B_4O_<33>w Reinforced Al-Alloy Composites"Proc.the 6th lnt'l Conf.on Aluminum Alloys (ICAA-6). 7・3. 1885-1890 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] G.Sasaki: "Fracture Mechanism of Al_<18>B_4O_<33> whisker Reinforced Aluminum Alloy Composites"Proc.ACCM-1. 10・2. 541-1-4 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] S.Takeuchi: "Mechanical Properties of Aluminum-Borate Whisler Reinforcec Magnesium Alloy Composites by Semi-Solid Process"Proc.ACCM- 1. 10・2. 533-1-4 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Fukunaga: "Interfacial Reaction and applicability of Al_<18>B_4O_<33>/Al Composites"European conference on composite materials(SCCM-8). 6・4. 75-81 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] G.Sasaki: "Interfaces in Al_<18>B_4O_<33>/Al and Mg Alloy Composites"Electron Microscopy 1998. 9・2. 813-814 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] J.Pan: "Interfacial Reaction and Its Effect on Strength of Al_<18>B_4O_<33>/Al Composites"Mat.Sci.Eng.. A15. 1044-1048 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] G.Sasaki: "Relationship between interfacial reaction and mechanical properties of Al_<18>B_4O_<33> whisker reinforced Mg,Al alloy composites"第2回中日複合材料交流会論文集. 10. 11-14 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Sang-Pill Lee: "Nb/MoSi_2積層複合材料の衝撃特性に及ぼす製造条件の影響"日本金属学会誌. 62・4. 351-357 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] M.Yoshida: "Preparation of alumina borate whisler reinforced semi-solid Mg alloy composites by squeeze casting"Proc.8th Japan-US Conf.on Composite Materials. 9. 579-588 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Sang-Pill Lee: "Al_<18>B_4O_<33>w/Al複合材料とアルミニウムの積層材料の衝撃特性に及ぼす積層構造の影響"軽金属. 48・5. 232-236 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 佐々木元: "マグネシウム基複合材料の微細構造と機械的性質"まてりあ. 37・6. 542 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 佐々木元: "Al_<18>B_4O_<33>w/Al,Mg合金複合材料の界面構造"日本金属学会誌. 63・5. 577-580 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] G.Sasaki: "Tnterfacial microstructure and fhature characterization of Al_<18>B_4O_<33>/Al alloy composites"Mat.Sci.Res.Int'l. 5・4. 276-279 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] G.Sasaki: "Electron microscopy analysis of squeeze casting Al_<18>B_4O_<33>/AZ91D composites"ICCM-12. 432 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] J.Pan,: "Compatibility of Si-C-0 Fiber and Si-C Fiber with Aluminum"ICCM-12. 640 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] M.Yoshida: "Preparation and Characterization of Aluminum Borate Whisker Reinforced Magnesium Alloy Composites by Semi-solid Processs"Adv.Composite Mater.. 8・3. 259-268 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] G.Sasaki: "Michrostructure and its effects on bending strength of Al_<18>B_4O_<33> reinforced Mg,Al matrix composites fabricated by squeeze casting process"Proc.of lnt'l Symp.on Adv.Forming and Die Manufacturing Technology (AFDM'99). 9. 131-136 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] G.Sasaki: "Mechanical Properties and Microstructures of Magnesium Matrix Composites"第2回中日複合材料交流会論文集. 10. 65-70 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] J.Pan: "Preparation and Property Evaluation of SiC/Al Composites Wires"Proc.of 16^<th> Inter.Jpn-Korea Seminar on Ceramics. 252-256 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] S.P.Lee: "Interfacial Control of Nb/MoSi_2 Laminate Composites and Its Effect on Impact Properties"Proc.of 16^<th> Inter.Jpn-Korea Seminar on Ceramics. 257-261 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 佐々木元: "ナノから原子、電子構造へ -複合材料の機能を電子顕微鏡で探ってみたら-"BOUNNDARY. 15・9. 7-11 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] L. J. Yao: "Reactivity of aluminum borate whisker with aluminum alloys"Mat. Sci. Eng.. A225. 59-68 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] G. Sasaki: "Microstructure of TiOィイD22ィエD2 (rutile)/Al composite"Proc. ICCM-11. 7・3. 24-31 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H. Fukunaga: "Reaction Squeeze cast processing and intermetallic dispersed aluminum matrix composites"Proc. ICCM-11. 7・3. 182-190 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H. Fukunaga: "Reaction Squeeze casting process"Proc. of International conference on thermomechanical processing of steels & other materials (THERMEC'97). 7・1. 1111-1117 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] G. Sasaki: "TiOィイD22ィエD2 composites by squeeze casting and hardness/microstructure change by heat treatment"Proc. of Australasia-Pacific forum on intelligent processing and manufacturing of materials (IPMM '97). 2. 872-882 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] L. Yao: "Interfacial Reaction and Interface Structure of AlィイD218ィエD2BィイD24ィエD2OィイD233wィエD2/Al Composites"Proc. 5th Japan International SAMPE Symposium & Exhibition (JISSE-5). 10. 423-428 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] I. Tuchitori: "Enhanced Solid State Reaction of TiOィイD22ィエD2/Al Composites by Doping"J. Jpn. Inst. Met.. 61・6. 544-552 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] S.P. Lee: "Processing and Interfacial Reaction of Nb/MoSiィイD22ィエD2 Laminate Composites and Their Effects on Impact Properties"European conference on composite materials (ECCM-8). 6・4. 263-270 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] L. J. Yao: "Effect of Interfacial Reaction on Bending Strength of AlィイD218ィエD2BィイD24ィエD2OィイD233ィエD2 Whisker Reinforced Aluminum Composites"Meta. Mat. Trans. A. 29A・5. 1517-1525 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] S.P. Lee: "Interfacial Microstructures and Impact Properties for Nb/MoSiィイD22ィエD2 Laminate Composites"Composite Interface. 5・5. 405-419 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] J Pan: "Effect of Interface Reaction on Strength of AlィイD218ィエD2BィイD24ィエD2OィイD233wィエD2 Reinforced Al-Alloy Composites"Proc. the 6th Int'l Conf. on Aluminum Alloys (ICAA-6). 7・3. 1885-1890 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] G. Sasaki: "Fracture Mechanism of AlィイD218ィエD2BィイD24ィエD2OィイD233ィエD2 Whisker Reinforced Aluminum Alloy Composites"Proc. ACCM-1. 10・2. 541-1-541-4 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] S. Takeuchi: "Mechanical Properties of Aluminum-Borate Whisker Reinforced Magnesium Alloy Composites by Semi-Solid Process"Proc. ACCM-1. 10・2. 533-1-533-4 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H. Fukunaga: "Interfacial Reaction and applicability of A1ィイD218ィエD2BィイD24ィエD2OィイD233ィエD2/Al Composites"European conference on composite materials (ECCM-8). 6・4. 75-81 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] G. Sasaki: "Interfaces in A1ィイD218ィエD2BィイD24ィエD2OィイD233ィエD2 and Mg Alloy Composites"Elect. Microscopy. 9・2. 813-814 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] J. Pan: "Interfacial Reaction and Its Effect on Strength of A1ィイD218ィエD2BィイD24ィエD2OィイD233ィエD2 Composites"Mat. Sci. Eng.. A・15. 1044-1048 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] G. Sasaki: "Relationship between interfacial reaction and mechanical properties of A1ィイD218ィエD2BィイD24ィエD2OィイD233ィエD2 whisker reinforced Mg, Al alloy composites"Proc. of 2nd Japan-China Joint Conference. 10. 11-14 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] S.P. Lee: "Effect of Fabricating Conditions on Impact Properties of Nb/MoSiィイD22ィエD2 Laminate Composites"J. Jpn. Inst. Met.. 62・4. 351-357 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] M. Yoshida: "Preparation of alumina borate whisker reinforced semi-solid Mg alloy composites by squeeze casting"Proc. 8th Japan-US Conf. on Composite Materials. 9. 579-588 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] S.P. Lee: "Effect of lamination structure on impact properties of A1ィイD218ィエD2BィイD24ィエD2OィイD233wィエD2/Al and aluminum laminate composites"J. Jpn. Inst. of Light Metals. 48・5. 232-236 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] G. Sasaki: "Microstructure and Mechanical Properties of Magnesium Alloy Matrix Composites"Materia Japan. 37・6. 542 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] G. Sasaki: "Interfaces in A1ィイD218ィエD2BィイD24ィエD2OィイD233ィエD2/Al Mg Alloy Composites"J. Jpn. Inst. Met. 63・5. 577-580 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] G. Sasaki: "Interfacial microstructure and fracture characterization of A1ィイD218ィエD2BィイD24ィエD2OィイD233ィエD2/Al alloy composites"Mat. Sci. Res. Int'l. 5・4. 276-279 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] G. Sasaki: "Electron microscopy analysis of squeeze casting A1ィイD218ィエD2BィイD24ィエD2OィイD233ィエD2/AZ91D composites"ICCM-12. 432 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] J. Pan: "Compatibility of Si-C-O Fiber and Si-C Fiber with Aluminum"ICCM-12. 640 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] M. Yoshida: "Preparation and Characterization of Aluminum Borate Whisker Reinforced Magnesium Alloy Composites by Semi-solid Process"Adv. Composite Mater. 8・3. 259-268 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] G. Sasaki: "Microstructure and its effects on bending strength of AlィイD218ィエD2BィイD24ィエD2OィイD233ィエD2 reinforced Mg, Al matrix composites fabricated by squeeze casting process"Proc. of Int'l Symp. on Adv. Forming and Die Manufacturing Technology (AFDM'99). 9. 131-136 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] G. Sasaki: "Mechanical Properties and Microstructures of Magnesium Matrix Composites"Proc. Of 3rd Japan-China Joint Conference. 10. 65-70 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] J. Pan: "Preparation and Property Evaluation of SiC/Al Composites Wires"Proc. of 16th Inter. Jpn-Korea Seminar on Ceramics. 252-256 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] S. P. Lee: "Interfacial Control of Nb/MoSi2 Laminate Composites and Its Effect on Impact Properties"Proc. of 16th Inter. Jpn-Korea Seminar on Ceramics. 257-261 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] G. Sasaki: "From Nano Scale to Atomic and Electronical Structure -Electron Microscopic Study on the Functional Properties of the Composites."BOUNNDARY. 15・9. 7-11 (1999)

    • Description
      「研究成果報告書概要(欧文)」より

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Published: 2001-10-23  

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