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1999 Fiscal Year Final Research Report Summary

Crystallographic study on phase transformation and artificial interface in ceramics

Research Project

Project/Area Number 09650763
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionEhime University

Principal Investigator

NAKAI Kiyomichi  Ehime university, Faculty of engineering, Associate professor, 工学部, 助教授 (60038114)

Co-Investigator(Kenkyū-buntansha) KOBAYASHI Sengo  Ehime university, Faculty of engineering, Research associate, 工学部, 助手 (10304651)
OHOMORI Yasuya  Ehime university, Faculty of engineering, Professor, 工学部, 教授 (10233280)
Project Period (FY) 1997 – 1999
Keywordsphase decomposition / phase equilibrium / mechanical property / microstructure evolution / cyystallography / interphase interface / composite material / intermetallics
Research Abstract

The phase-decomposition processes and -equilibria in ceramics and intermetallics have been investigated, because their properties depend largely on the microstructures. In the present investigations, the morphology and crystallography of the microstructures have been extensively examined, and the mechanisms for the microstructure evolutions have been clarified.
Details in the present investigations are as follows ; the mechanisms of carbide and/or oxide precipitation in mechanically alloyed Mo-HfC or Mo-TiC composite materials in high-temperature regions, the effects of impurities on oxide formation in oxygen-doped silicon, the mechanism of purification of silicon by the oxide-precipitation, the mechanisms of phase-decomposition and -equilibria in TiAl-based intermetallics, the effects of addition of Cr, Zr or Mo to Ti-Al binary alloys on the stability of β phase, the mechanism of the β phase decomposition in the ternary Ti-AI-X alloys, the effects of nitrides and/or carbide nucleation on formation of primary ferrite in low C steels, the effects of addition of various elements on phase-decomposition and -equilibria in high Cr steels, the mechanism of phase-decomposition and -equilibria in Ti-based materials for human being, the aging processes in Al alloys, and the formation processes of various intermetallic compounds.
The structures of interphase interfaces have been examined, and clarified to be dominant factor controling size distribution of precipitates and precipitation anisotropy by the crystallographic analyses for phase-equilibria and -decomposition in ceramics and alloys. It is concluded that crystallographic analyses for phase-transformation and -equilibrium are indispensable to control the material properties.

  • Research Products

    (48 results)

All Other

All Publications (48 results)

  • [Publications] 大森靖也: "Effects of ω phase formation on the decomposition of α"/β duplex phase structure in a metastable β Ti alloy"Mater.Trans.,JIM. 39. 40-48 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 大森靖也: "Crystallographic analysis of α phase formation in a metastable β Ti alloy"Mater.Trans.,JIM. 39. 49-56 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 仲井清眞: "Fe-Cr-C合金パーライトの局所オーステナイト化"日本金属学会会報. 37. 381 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 大森靖也: "Ordering processes in an Al-Li-Cu-Mg-Zralloy"Advanced Materials and Processing,Eds.M.A.Imam,R.DeNale,S.Hanada,Z.Zhong and D.N.Lee,Pub.of TMS. 1. 1293-1298 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 仲井清眞: "Austenite formation and alloy carbide dissolution in Fe-Cr-C steels during heating"Advanced Materials and Processing,Eds.M.A.Imam,R.DeNale,S.Hanada,Z.Zhong and D.N.Lee,Pub.of TMS. 1. 1443-1448 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 仲井清眞: "Effects of Zr-addition on phase stability and phase transformations in a Ti-50at.%Al alloy"Advanced Materials and Processing,Eds.M.A.Imam,R.DeNale,S.Hanada,Z.Zhong and D.N.Lee,Pub.of TMS. 1. 1533-1538 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 仲井清眞: "Formation of austenite and dissolution of alloy carbides in Fe-8.2Cr-Calloys"Zeitschrift fur Metallkunde. 90. 25-37 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 仲井清眞: "Crystallography and interface boundary structure of pearlite with M_7C_3carbide lamellae"Acta Materialia. 47. 1105-1115 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 大森靖也: "Aging behavior of an Al-Li-Cu-Mg-Zralloy"Metall.and Mater.Trans.A. 30A. 741-749 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 仲井清眞: "Mechanism and crystallography of ferrite precipitation from cementite in an Fe-Cr-C alloy during austenitisation"Phil.Mag.A. 79. 1655-1669 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 仲井清眞: "Pearlite to austenite transformation in an Fe-2.6Cr-1Calloy"Acta Materialia. 47. 2619-2632 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 仲井清眞: "Ti-48at.%Al合金中の微細組織形成過程"社団法人日本鉄鋼協会材料の組織と特性部会相分解による組織形成過程研究会. 35-40 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 小林千悟: "δ/γ2相ステンレス鋼におけるδ相の相分解挙動"社団法人日本鉄鋼協会材料の組織と特性部会相分解による組織形成過程研究会. 49-54 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 仲井清眞: "Decomposition of α-phase into massive and Widmanstattenstructures in a Ti-48at.%Al alloy"Solid-Solid Phase Transformations I,Edited by M.Koiwa,K.Otsuka and T.Miyazaki,The Japan Institute of Metals. 1. 153-156 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 大森靖也: "Crystallization processes of Nd-Fe-Cr-B amorphous ribbons"Solid-Solide PhaseTransformations I,Edited by M.Koiwa,K.Otsuka and T.Miyazaki,The Japan Institute of Metals. 2. 1251-1254 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 小林千悟: "Microstructure formation in δ/γ duplex phase stainless steel during isothermal ageing and continuous heating"Solid-Solid Phase Transformations I,Edited by M.Koiwa,K.Otsuka and T.Miyazaki,The Japan Institute of Metals. 2. 1625-1628 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 仲井清眞: "計算状態図による合金鋼中の逆変態に伴う組織変化の解析"日本金属学会会報「まてりあ」. 38. 975-981 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 仲井清眞: "Decomposition of martensite by discontinuous-like precipitation reaction in an Fe-17Cr-0.5C alloy"Acta Materialia. (印刷中).

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 仲井清眞: "Crystallography and structural evolution during reverse transformation in an Fe-17Cr-0.5C tempered martensite"Acta Materialia. (印刷中).

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 仲井清眞: "Phase-equilibria and-decomposition in a Ti-Al-Zr alloy"7th Asia-Pacific Electron Microscopy Conference "Perspective Imaging". (印刷中).

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 仲井清眞: "Decomposition of β phase in a Ti-Al-Cr alloy"7th Asia-Pacific Electron Microscopy Conference "Perspective Imaging". (印刷中).

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 小林千悟: "Microstructure evolutions in a 25Cr-7Ni based stainless steel isothemally aged at 550℃"7th Asia-Pacific Electron Microscopy Conference "Perspective Imaging". (印刷中).

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 小林千悟: "Phase transformations in Al-3.3mass%Li alloy"7th Asia-Pacific Electron Microscopy Conference "Perspective Imaging". (印刷中).

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 仲井清眞: "Decomposition processes of α phase in a Ti-48at%Al alloy"Mater.Trans.JIM. (印刷中).

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Yasuya OHMORI: "Effects of ω phase formation on the decomposition of α"/β duplex phase structure in a metastable β Ti alloy"Mater.Trans, JIM. 39. 40-48 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Yasuya OHMORI: "Crystallographic analysis of α phase formation in a metastable β Ti alloy"Mater.Trans, JIM. 39. 49-56 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kiyomichi NAKAI: "Localized austenitization of pearlite in Fe-Cr-C steel"J.Jpn.Inst.Met.. 37. 381 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Yasuya OHMORI: "Ordering processes in an Al-Li-Cu-Mg-Zr alloy"Advenced Materials and Processing, Eds.M.A.Imam et al., ub.Of TMS. 1. 1293-1298 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kiyomichi NAKAI: "Austenite formation and alloy carbide dissolution in Fe-Cr-C steels during heating"Advenced Materials and Processing, Eds.M. A. Imam et al., ub. Of TMS. 1. 1443-1448 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kiyomichi NAKAI: "Effects of Zr-addition on phase stability and phase transformations in a Ti-50at.%Al alloy"Advenced Materials and Processing, Eds. M. A. Imam et al., ub. Of TMS. 1. 1533-1538 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kiyomichi NAKAI: "Formation of austenite and dissolution of alloy carbides in Fe-8.2Cr-C alloys"Zeitschrift fur Metallkunde. 90. 25-37 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kiyomichi NAKAI: "Crystallography and interface boundary structure of pearlite with MィイD27ィエD2CィイD23ィエD2 carbide lamellae"Acta Materialia. 47. 1105-1115 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Yasuya OHMORI: "Aging behavior of an Al-Li-Cu-Mg-Zr alloy"Metall.And Mater.Trans.A. 30A. 741-749 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kiyomichi NAKAI: "Mechanism and crystallography of ferrite precipitation from cementite in an Fe-Cr-C alloy during austenitisation"Phil.Mag.A. 79. 1655-1669 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kiyomichi NAKAI: "Pearlite to austenite transformation in an Fe-2.6Cr-1C alloy"Acta Materialia. 47. 2619-2632 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kiyomichi NAKAI: "Microstructure evolutions in a Ti-48at%Al alloy"ISIJ Symp.On Phase Decomposition. 35-40 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Sengo KOBAYASHI: "Decomposition of δ phase in a δ/γ stainless steel"ISIJ Symp.On Phase Decomposition. 49-54 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kiyomichi NAKAI: "Decomposition of α-phase into massive and Widmanstatten structures in a Ti-48at.%Al alloy"Solid-Solid Phase Transformations I, Edited by M. Koiwa et al., The Japan Institute of Metals. 1. 153-156 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Yasuya OHMORI: "Crystallization processes of Nd-Fe-Cr-B amorphous ribbons"Solid-Solid Phase Transformations II, Edited by M. Koiwa et al., The Japan Institute of Metals. 2. 1251-1254 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Sengo KOBAYASHI: "Microstructure formation in δ/γ duplex phase stainless steel during isothermal ageing and continuous heating"Solid-Solid Phase Transformations II, Edited by M. Koiwa et al., The Japan Institute of Metals. 2. 1625-1628 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kiyomichi NAKAI: "Analyses of microstructure evolutions by reverse phase transformations in alloy steels"J.Jpn.Inst.Met.. 38. 975-981 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kiyomichi NAKAI: "Decomposition processes of α phase in a Ti-48at%Al alloy"Materials Transactions JIM. (in press).

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kiyomichi NAKAI: "Decomposition of martensite by discontinuous-like precipitation reaction in an Fe-17Cr-0.5C alloy"Acta Materialia. (in press).

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kiyomichi NAKAI: "Crystallography and structural evolution during reverse transformation in an Fe-17Cr-0.5C tempered martensite"Acta Materialia. (in press).

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kiyomichi NAKAI: "Phase-equilibria and -decomposition in a Ti-Al-Zr alloy"7th Asia-Pacific Electron Microscopy Conference "Perspective Imaging". (in press).

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Kiyomichi NAKAI: "Decomposition of β phase in a Ti-Al-Cr alloy"7th Asia-Pacific Electron Microscopy Conference "Perspective Imaging". (in press).

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Sengo KOBAYASHI: "Microstructure evolutions in a 25Cr-7Ni based stainless steel isothermally aged at 550℃"7th Asia-Pacific Electron Microscopy Conference "Perspective Imaging". (in press).

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Sengo KOBAYASHI: "Phase transformations in Al-3.3mass%Li alloy"7th Asia-Pacific Electron Microscopy Conference "Perspective Imaging". (in press).

    • Description
      「研究成果報告書概要(欧文)」より

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Published: 2001-10-23  

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