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1998 Fiscal Year Final Research Report Summary

Microstructural Stability and Hall-Petch Relationship for Fine-Grained Alloys Fabricated by ECAP

Research Project

Project/Area Number 09650764
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionFukuoka University of Education

Principal Investigator

FURUKAWA Minoru  Fukuoka Univ.of Education, Facul.of Edu., Assoc.Prof., 教育学部, 助教授 (90112276)

Project Period (FY) 1997 – 1998
KeywordsECAP method / Severe plastic strain / Ultra fine grain / Microstructural stability / Hall-Petch relationship / Transmission electron microscope / Superplasticity
Research Abstract

1. Fine grain sizes of 1.2, 0.3, 0.7, 0.7, 0.2 and 1.2 mum were obtained by ECA pressing for pure Al, Al-3% Mg, AI-0.2% Zr, A1-0.2% Sc, A1-3% Mg-0.2% Sc and A1-5.5% Mg-2.2% Li-0.12% Zralloys, respectively. Fine grain was stable up to 473 K both for pure Al and AI-3% Mg alloys. On the other hand, the thermal stability of fine grain was kept up to 573 K for AI-0.2% Zr alloy. Furthermore, the stability both for AI-.0.2% Sc and AI-3% Mg-0.2% Sc alloys was preserved up to a temperature as high as 673 K.The reason why fine grain in the Al alloys containing Zr or Sc is stable up to higher temperature than that in the pure Al and Al-3% Mg alloy is attributed to the existence of fine-dispersed AI_3Zr and Al_3Sc particles. And the Al_3Sc is more effective than AI_3Zr to inhibit recrystallization in Al alloys. For the AI-5.5% Mg-2.2% Li-0.12% Zr alloy, fine grain was kept up to 673 K.
2. For the AI-3% Mg alloy, the Hall-Petch relationship of Hv=46+35d^<-1/2> (where Hv is Vickers microhardness and d is average grain size) was valid in the range of grain size of 0.2 to 100 mum. On the other hand, for the AI-5.5% Mg-2.2% Li-0.12% Zr alloy, the Hall-Petch relationship of Hv=75+27d^<-1/2> was valid in the range of grain sizes of 2 to 60 mum.
3. Elongations to failure was 1030 in the testing condition of 673 K and 3.3x10^<-2> s^<-1> for A1-3% Mg-0.2% Sc alloy On the other hand, the elongation was 1200% in the testing condition of 623 K and 10^<-2> S^<-1> for Al-5.5% Mg-2.2% Li-0.12% Zr alloy. Grain size in the fracture region was larger than that in the gripped region. This indicates that grain growth induced by stress takes place during tensile testing at elevated temperatures.

  • Research Products

    (48 results)

All Other

All Publications (48 results)

  • [Publications] M.Furukawa: "Microstructural Characteristics of an Ultrafine Grain Metal Processed with Equal-Channel Angular Pressing" Materials Characterization. Vol.37. 277-283 (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Z.Horita: "Evolution of Grain Boundary Structure in Submicrometer-Grained Al-Mg Alloy" Materials Characterization. Vol.37. 285-294 (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] M.Furukawa: "Recry stallization in Ultrafine-Grained Materials with Non-Equilibrium Grain Boundaries" Proceedings of the Third International Comference on Recrystallization and Related Phenamena (Rex'96). 147-160 (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] M.Furukawa: "Structural Evolution and the Hall-Petch Relationship in an Al-Mg-Li-Zr Alloy with Ultra-Fine Grain Size." Acta Metallurgica et Materialia. Vol.45 No.11. 4751-4757 (1997)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] M.Furukawa: "Microstructural Characteristics and Superplastic Ductility in a Zn-22% Al Alloy with Submicrometer Grain Size." Materials Science and Engineering A. Vol.A241,No.1〜2. 122-128 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] M.Furukawa: "Age Hardening and the Potential for Superplasticity in a Fine Grained Al-Mg-Li-Zr Alloy." Matallurgical and Materials Transactions A. Vol.29A,January. 169-177 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] M.Furukawa: "Fabrication and Properties of a Submicrometer-Grained Zn-22% Al Alloy" Proceedings of International Conference on Thermomechanical Processing of Steels and Other Materials, Thermec'97. 1875-1881 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Z.Horita: "Characterization of Ultra-Fine Grained Materials Produced by Torsion Straining" Proceedings of International Conference on Thermomechanical Processing of Steels and Other Muterials,Thermec'97. 1937-1943 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] P.B.Berbon: "Superplasticity in Alloys Processed by Equal-Channel Angular Pressing" Superplastieity and Superplastic Forming'1998. 127-134 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] M.Furukawa: "Microstructural Evolution in Pure Aluminum During Equal-Channel Angular Pressing" Modeling the Mechanical Response of Structural Materials. 165-172 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] P.B.Berbon: "Application of Equal-Channel Angular Pressing for Producing Superplastre Alloys" Modeling the Mechanieal Response of Structural Materials. 173-180 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 小村省吾: "拘束強ひずみ加工で作製した超微細粒組織" 日本金属学会会報(まてりあ). 第37巻第5号. 376-376 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] T.G.Langdon: "Using Intense Plastic Straining for High-Strain Rate Superplasticity" Journal of Materials (JOM). Vol.78,No.1. 41-45 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] M.Furukawa: "Factors Influencing the Flow and Hardness of Materials with Ultrafine Grain Sizes" Philosophical Magazine A. Vol.50,No.6. 203-215 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] S.Komura: "High Strain Rate Superplasticity in an Al-Mg Alloy Containing Scandium" Scripta Metallurgica et Materialia. Vol.38,No.12. 1851-1856 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Hasegawa: "Grain Refinement and Potential for Superplasticity in AL Alloys Containing Small Particles" Proceedings of the Third Pacific Rim International Conference on Advanced Materials and Processing (PRICM-3). 1873-1878 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] K.Oh-ishi: "Optimizing the Rotation Conditions for the Grain Refinement in Equal-Channel Angular Pressing" Metallurgical and Materials Transactions A. Vol.29A July. 2011-2013 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] P.B.Berbon: "Optimizing the Processing of a Commercial AL-Based Alloy for High Strain Rate Superplasticity" Proceedings of the Third International Symposium on Microstructures and Mechanical Properties of New Engineering Materials (IMSP'97). 81-88 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] P.B.Berbon: "Fabrication of Bulk Ultrafine-Grained Materials Through Intense Plastic Straining" Metallurgical and Materials Transactions A. Vol.29A,September. 2237-2243 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Y.Iwahashi: "Microstructural Characteristic of Ultrafine-Grained Aluminum Produced Using Equal-Channel Angular Pressing" Metallurgical and Materials Transactions A. Vol.29A,September. 2245-2252 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] 堀田善治: "新しい組織制御法としてのEqual-Channel Angular Pressing (ECAP)" 日本金属学会会報(まてりあ). 第37巻第9号. 767-774 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] P.B.Berbon: "Requirements for Achieving High Strain Rate Superplasticity in Cast Aluminum Alloys" Philosophical Magazine Letters. Vol.78,No.4. 313-318 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] P.B.Berbon: "Processing of Aluminum Alloys for High Strain Rate Superplasticity" Hot Deformation of Aluminum Alloys II. 111-124 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] S.Komura: "Superplasticity in an Ultrafine-Grained Al-Mg-Sc Alloy Produced by Equal-Channel Angular Pressing" Hot Deformation of Aluminum Alloys II. 125-138 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] M.Furukawa, Z.Horita, M.Nemoto, R.Z.Valiev and T.G.Langdon: "Microstructural Characteriatics of an Ultrafine Grain Metal Processed with Equal-Channel Angular Pressing." Materials Characterization. Vol.37. 277-283 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Z.Horita, D.J.Smith, M.Furukawa, M.Nemoto, R.Z.Valiev and T.G.Langdon: "Evolution of Grain Boundary Structure in Submicrometer-Grained Al-Mg Alloy." Materials Characterization. Vol.37. 285-294 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] M.Furukawa, Z.Horita, M.Nemoto, R.Z.Valiev and T.G.Langdon: "Recrystallization in Ultrafine-Grained Materials with Non-Equilibrium Grain Boudaries." Proceedings of the Third International Conference on Recrystallization and Related Phenomena. 149-160 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] M.Furukawa, Y.Iwahashi, Z.Horita, M.Nemoto, N.K.Tsenev, R.Z.Valiev and T.G.Langdon: "Structural Evolution and the Hall-Petchi Relationship in an Al-Mg-Li-Zr Alloy with Ultra-Fine Grain Size." Acta Metallurgica et Materialia. Vol.45, No.11. 4751-4757 (1997)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] M.Furukawa, Y.Ma, Z.Horita, M.Nemoto, R.Z.Valiev and T.G.Langdon: "Microstructural Charcteristics and Superplastic Ductility in a Zn-22% Al Alloy with Submicrometer Grain Size." Materials Science and Engineering A. Vol.A.241, No.1-2. 122-128 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] M.Furukawa, P.B.Berbon, Z.Horita, M.Nemoto, N.K.Tsenev, R.Z.Valiev and T.G.Langdon: "Age Hardening and the Potential for Superplasticity in a Fine-Grained Al-Mg-Li-Zr Alloy." Metallurgical and Materials Transactions A. Vol.29A, January. 169-177 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] M.Furukawa, Y.Ma, Z.Horita, M.Nemoto, R.Z.Valiev and T.G.Langdon: "Fabrication and Properties of a Submicrometer-Grained Zn-22% Al Alloy." Proceedings of International Conference on Thermomechanical Processing of Steels and Other Materials. 1875-1881 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Z.Horita, D.J.Smith, M.Furukawa, M.Nemoto, R.Z.Valiev and T.G.Langdon: "Characterization of Ultra-Fine Grained Materials Produced by Tosion Straining." Proceedings of International Conference on Thermomechanical Processing of Steels and Other Materials. 1937-1943 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] P.B.Berbon, N.K.Tsenev, R.Z.Valiev, M.Furukawa, Z.Horita, M.Nemoto and T.G.Langdon: "Superplasticity in Alloys Processed by Equal-Channel Angular Pressing." Superplasticity and Superplastic Forming 1998. 127-134 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] M.Furukawa, Z.Horita, M.Nemoto and T.G.Langdon: "Microstructural Evolution in Pure Aluminum During Equal-Channel Angular Pressing." Modelling the Mechanical Response of Structural Materials. 165-172 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] P.B.Berbon, M.Furukawa, Z.Horita, M.Nemoto, N.K.Tsenev, R.Z.Valiev and T.G.Langdon: "Application of Equal-Channel Angular Pressing for Producing Superplastic Aluminum Alloys." Modelling the Mechanical Response of Structural Materials. 173-180 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] S.Komura, A.Utsunomiya, Z.Horita, M.Nemoto, M.Furukawa, P.B.Berbon and T.G.Langdon: "Ultrafine-Grained Structure Produced by Equal-Channel Angular Pressing" Materia Japan. Vol.37 No.5. 376 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] T.G.Langdon, M.Furukawa, Z.Horita and M.Nemoto: "Using Intense Plastic Strainng for High-Strain-Rate Superplasticity." Jounal of Materials (JOM), The Minerals. Vol.50, No.6, June. 41-45 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] M.Furukawa, Z.Horita, M.Nemoto, R.Z.Valiev and T.G.Langdon: "Factors Influencing the Flow and Hardness of Materials with Ultrafine Grain Sizes." Philosophical Magazine A. Vol.78, No.1. 203-215 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] S.Komura, P.B.Berbon, M.Furukawa, Z.Horita, M.Nemoto and T.G.Langdon: "High Strain Rate Superplastisity in an Al-Mg Alloy Containing Scandium." Scripta Metallurgica et Materialia. Vol.138, No.12. 1851-1856 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H.Hasegawa, S.Komura, Z.Horita, M.Furukawa, M.Nemoto and T.G.Langdon: "Grain Refinement and Potential for Superplasticity in Al Alloys Containing Small Particles." Proceedings of the Third Pacific Rim International Conference on Advanced Materials and Processing (PRICM-3). 1873-1878 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] K.Oh-ishi, Z.Horita, M.Furukawa, M.Nemoto and T.G.Langdon: "Optimizing the Rotation Conditions for Grain Refinement in Equal-Channel Angular Pressing." Metallurgical and Materials Transactions A. Vol.29A, July. 2011-2013 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] P.B.Berbon, M.Furukawa, Z.Horita, M.Nemoto, N.K.Tsenev, R.Z.Valiev and T.G.Langdon: "Optimizing the Processing of a Commercial Al-Based Alloy for High Strain Rate Superplasticity." Proceedings of the Third International Symposium on Microstructures and Mechanical Properties of New Engineering Materials (IMSP'97). 81-88 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] P.B.Berbon, N.K, Tsenev, R.Z.Valiev, M.Furukawa, Z.Horita, M.Nemoto and T.G.Langdon: "Fabrication of Bulk Ultrafine-Grained Materials Through Intense Plastic Straining" Metallurgical and Materials Transactions A. Vol.29A, September. 2237-2243 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Y.Iwahashi, M.Furukawa, Z.Horita, M.Nemoto and T.G.Langdon: "Microstructural Characteristics of Ultrafine-Grained Aluminum Produced Using Equal-Channel Angular Pressing." Metallurgical and Materials Transactions A. Vol.29A, September. 2245-2252 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Z.Horita, M.Furukawa, M.Nemoto and T.G.Langdon: "Equal-Channel Angular Pressing (ECAP) : A Novel Method for Microstructural Control." Materia Japan. Vol.37, No.9. 767-774 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] P.B.Berbon, M.Furukawa, Z.Horita, M.Nemoto, N.K.Tsenev, R.Z.Valiev and T.G.Langdon: "Requirements for Achieving High Strain Rate Superplasticity in Cast Aluminum Alloys." Philosophical Magazine Letters. Vol.78, No.4. 313-318 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] P.B.Berbon, M.Furukawa, Z.Horita, M.Nemoto, N.K.Tsenev, R.Z.Valiev and T.G.Langdon: "Processing of Aluminum Alloys for High Strain Rate Superplasticity." Hot Deformation of Aluminum Alloys II. 111-124 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] S.Komura, P.B.Berbon, A.Utsunomiya, M.Furukawa, Z.Horita, M.Nemoto and T.G.Langdon: "Superplasticity in an Ultrafine-Grained Al-Mg-Sc Alloy Produced by Equal-Channel Angular Pressing." Hot Deformation of Aluminum Alloys II. 125-138 (1998)

    • Description
      「研究成果報告書概要(欧文)」より

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Published: 1999-12-08  

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