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2000 Fiscal Year Final Research Report Summary

Transmission electron microscope observation of cracks introduced in bulk crystals

Research Project

Project/Area Number 10305045
Research Category

Grant-in-Aid for Scientific Research (A).

Allocation TypeSingle-year Grants
Section一般
Research Field Physical properties of metals
Research InstitutionNagoya University

Principal Investigator

SAKA Hiroyasu  Nagoya University, Graduate School of Engineering, Professor, 工学研究科, 教授 (90023267)

Co-Investigator(Kenkyū-buntansha) SASAKI Katsuhiro  Nagoya University, Graduate School of Engineering, Assistant Professor, 工学研究科, 講師 (00211938)
KURODA Kotaro  Nagoya University, Graduate School of Engineering, Professor., 工学研究科, 教授 (30161798)
Project Period (FY) 1998 – 2000
KeywordsCrack / Transmission electron microscopy / dislocations / bulk crystals / focused ion beam technique
Research Abstract

Fracture of materials is one of the most important subjects in materials science. There are two approaches to the study of fracture of materials. One is macroscopic one and the other is atomistic simulation using a computer. However, there is a big gap between these extremes and it is information on mesoscopic scale that bridges this gap. In order to get such information on mesoscopic scale transmission electron microscopy should be the most appropriate technique. However, it is extremely difficult to prepare a foil specimen which contain S the very tip of a crack.
The purpose of the present study is to examine by transmission electron microscopy those cracks which were introduced in bulk crystals applying a focused ion beam technique to preparation of a thin foil specimen from pre-selected area such as a crack tip. This contributes much to bridge the gap between macroscopic approach and atomistic simulation. In this study, Si, GaAs, alumina and quasicrystals were used as specimens and the defect structures at and near the tips of the cracks were observed comprehensively.

  • Research Products

    (12 results)

All Other

All Publications (12 results)

  • [Publications] Suprijadi and H.Saka: "On the nature of a dislocation wake along a crack introduced in Si at the DBTT"Phil.Mag.Lett.. 78. 435-443 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Saka,J.Shimatani,Suprijadi and T.Nango: "FIB/TEM observation of defect structure underneath an indentation in silicon"Mat.Res.Soc.Symp.Proc.. 522. 71-76 (1998)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] H.Saka,G.Nagaya: "Plan-view observation of crack tips in bulk materials by FIB/HVEM"Radiation Effects & Defects in Solids. 148. 319-332 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] M.Wollgarten,H.Saka: "Microstructural investigation of the brittle-ductile transition in Al-Pd-Mn quasicrsytals"Phil.Mag.A. 79. 2195-2208 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Suprijadi and H.Saka: "Cross-sectional and plan-view observation of cracks introduced in Si at the DBTT"Mat.Res.Soc.Symp.Proc.. 538. 169-174 (1999)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Suprijadi and H.Saka: "TEM observation of dislocation emission from a crack at DBTT in Si"Materi.Trans. 42. 28-32 (2001)

    • Description
      「研究成果報告書概要(和文)」より
  • [Publications] Suprijadi and H.Saka: "On the nature of a dislocation wake along a crack introduced in Si at the ductile-brittle transition temperature"Phil.Mag.Lett.. 78. 435-443 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H.Saka, J.Shimatani, Suprijadi and T.Nango: "FIB/TEM observation of defect structure underneath an indentation in silicon"Mat.Res.Soc.Symp.Proc.. 522. 71-76 (1998)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] H.Saka, G.Nagaya, T.Sakuishi and S.Abe: "Plan-view observation of crack tips in bulk materials by FIB/HVEM"Radiation Effects & Defects in Solids. 148. 319-332 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] M.Wollgarten, H.Saka and A.Inoue: "Microstructural investigation of the brittle-ductile transition in Al-Pd-Mn quasicrsytals"Phil.Mag., A. 79. 2195-2208 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Suprijadi and H.Saka: "Cross-sectional and plan-view observation of cracks introduced in Si at the ductile-brittle transition temperature"Mat.Res.Soc.Symp.Proc.. 538. 169-174 (1999)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Publications] Suprijadi, and H.Saka: "TEM observation of dislocation emission from a crack at DBTT in Si"Materi.Trans.. 42. 28-32 (2001)

    • Description
      「研究成果報告書概要(欧文)」より

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Published: 2002-03-26  

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