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2006 Fiscal Year Final Research Report Summary

Elucidation of effect of hydrogen on giga-cycle fatigue mechanism and establishment of improvement method of fatigue strength reliability

Research Project

Project/Area Number 14001002
Research Category

Grant-in-Aid for Specially Promoted Research

Allocation TypeSingle-year Grants
Review Section Physics
Research InstitutionKyushu University

Principal Investigator

YUKITAKA Murakami  Kyushu University, Faculty of Engineering, Professor, 大学院・工学研究院, 教授 (10038010)

Co-Investigator(Kenkyū-buntansha) KONDO Yoshiyuki  Kyushu University, Faculty of Engineering, Professor, 大学院・工学研究院, 教授 (90325499)
NOGUCHI Hiroshi  Kyushu University, Faculty of Engineering, Professor, 大学院・工学研究院, 教授 (80164680)
MATSUOKA Saburo  Kyushu University, Faculty of Engineering, Associate Professor, 大学院・工学研究院, 助教授 (10354250)
TAKAI Kenichi  Sophia University, Faculty of Science and Engineering, Associate Professor, 理工学部, 助教授 (50317509)
MATSUNAGA Hisao  Fukuoka University, Faculty of Engineering, Associate Professor, 工学部, 助教授 (80346816)
Project Period (FY) 2002 – 2006
KeywordsGiga-cycle fatigue / Hydrogen / Optically Dark Area / The area parameter model / Nonmetallic inclusion / Slip / Tritium autoradiography / Fuel cell system
Research Abstract

In recent years, a special concern has been raised about the development and commercialization of fuel cell (FC) systems to solve both the global warming and energy problems. Under such circumstance, the role of this research project has been significantly increasing to ensure the safety use of FC systems in the near future. In this project, the effect of hydrogen on giga-cycle fatigue mechanism in high strength steels has been studied as well as the effect of hydrogen on fatigue properties of candidate materials for FC systems. The obtained results are as follows:
(1) The evidences of interaction of hydrogen on giga-cycle fatigue failure have been shown by the fatigue tests of hydrogen-content-controlled specimens, the secondary ion mass spectrometry and the tritium autoradiography.
(2) The giga-cycle fatigue mechanism taking the hydrogen interaction into consideration has been proposed. It has been shown that the giga-cycle fatigue strength can be improved by controlling hydrogen content in materials, inclusion size and inclusion type.
(3) A fatigue design method in giga-cycle regime has been proposed based on the area parameter model, the statistics of extremes and the growth curve of the optically dark area (ODA).
(4) A number of reliable fatigue data on the effect of hydrogen has been obtained about the candidate materials for FC systems. In addition, some important findings about the degradation mechanism due to hydrogen have been given, e.g. the slip localization due to hydrogen and the effect of phase transformations on the crack-growth acceleration, etc.
Considering all the results in this project, the following two significant conclusions have been obtained:
(I) Hydrogen does not cause so-called "embrittlement" of materials, but facilitates the dislocation mobility resulting in the slip concentration.
(II) The role of hydrogen trapped by inclusions in giga-cycle fatigue mechanism is to cause the microscopic slip concentration even at the lower stress.

  • Research Products

    (55 results)

All 2006 2005 2004 2003 2002

All Journal Article (53 results) Patent(Industrial Property Rights) (2 results)

  • [Journal Article] 材料組織の異なるステンレス鋼の疲労強度に及ぼす水素チャージの影響2006

    • Author(s)
      金崎俊彦, 永田晃市, 松永久生, 村上敬宜
    • Journal Title

      日本機械学会論文集(A編) 72-713

      Pages: 106-113

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Factors Affecting Ultralong Life Fatigue and Design Method for Components2006

    • Author(s)
      Y.Murakami, J.Nagata, H.Matsunaga
    • Journal Title

      Plenary lecture, Fatigue 2006

      Pages: 12-17

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] オーステナイト系ステンレス鋼の疲労き裂進展挙動および絞り低下に及ぼす水素の影響2006

    • Author(s)
      金崎俊彦, 峯洋二, 福島良博, 村上敬宜
    • Journal Title

      日本機械学会論文集(A編) 72-717

      Pages: 653-660

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] 非金属介在物起点の疲労き裂による疲労限度の消滅と人工微小欠陥から発生した疲労き裂の停留2006

    • Author(s)
      村上敬宜, 長田淳治
    • Journal Title

      日本機械学会論文集(A編) 72-720

      Pages: 1123-1130

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Effects of hydrogen charge on microscopic fatigue behaviour of annealed carbon steels2006

    • Author(s)
      H.Uyama, M.Nakashima, K.Morishige, Y.Mine, Y.Murakami
    • Journal Title

      Fatigue & Fracture of Engineering Materials & Structures 29-12

      Pages: 1066-1074

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] ステンレス鋼の疲労き裂進展特性に及ぼす水素の影響とマルテンサイト変態2006

    • Author(s)
      金崎俊彦, 楢崎千尋, 峯洋二, 松岡三郎, 村上敬宜
    • Journal Title

      日本機械学会論文集(A編) 72-723

      Pages: 1717-1724

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] The effect of hydrogen on fatigue properties of steels used for fuel cell system2006

    • Author(s)
      Yukitaka Murakami, Hisao Matsunaga
    • Journal Title

      International Journal of Fatigue 28

      Pages: 1509-1520

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] The effect of hydrogen on fatigue properties of metals used for fuel cell system2006

    • Author(s)
      Y.MURAKAMI
    • Journal Title

      International Journal of Fracture 28

      Pages: 167-195

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Effect of Hydrogen Charge on Fatigue Strength of Stainless Steel.2006

    • Author(s)
      KANEZAKI Toshihiko, NAGATA Koichi, MATSUNAGA Hisao, MURAKAMI Yukitaka
    • Journal Title

      Transactions of the Japan Society of Mechanical Engineers. A, Vol. 72, No. 713

      Pages: 106-325

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Factors Affecting Ultralong Life Fatigue and Design Method for Components2006

    • Author(s)
      Y.Murakami, J.Nagata, H.Matsunaga
    • Journal Title

      Plenary lecture, Fatigue 2006, Atlanta

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] The Effect of Hydrogen on Fatigue Crack Growth Behavior and Ductility Loss of Austenitic Stainless Steels2006

    • Author(s)
      KANEZAKI Toshihiko, MINE Yoji, FUKUSHIMA Yoshihiro, MURAKAMI Yukitaka
    • Journal Title

      Transactions of the Japan Society of Mechanical Engineers. A, Vol. 72, No. 717

      Pages: 653-660

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Elimination of Conventional Fatigue Limit due to Fatigue Crack Originated at Nonmetallic Inclusion, and Non-propagation of Fatigue Crack Originated at Artificial Small Hole2006

    • Author(s)
      MURAKAMI Yukitaka, NAGATA Junji
    • Journal Title

      Transactions of the Japan Society of Mechanical Engineers. A, Vol. 72, No. 720

      Pages: 1123-1130

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Effects of hydrogen charge on microscopic fatigue behaviour of annealed carbon steels2006

    • Author(s)
      H.Uyama, M.Nakasahima, K.Morishige, Y.Mine, Y.Murakami
    • Journal Title

      Fatigue & Fracture of Engineering Materials & Structures Vol. 29, No. 12

      Pages: 1066-1074

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Effect of Hydrogen on Fatigue Crack Growth and Martensitic Transformation of Stainless Steels2006

    • Author(s)
      KANEZAKI Toshihiko, NARAZAKI Chihiro, MINE Yoji, MATSUOKA Saburo, MURAKAMI Yukitaka
    • Journal Title

      Transactions of the Japan Society of Mechanical Engineers. A, Vol. 72, No. 723

      Pages: 1717-1724

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] The effect of hydrogen on fatigue properties of steels used for fuel cell system2006

    • Author(s)
      Yukitaka Murakami, Hisao Matsunaga
    • Journal Title

      International Journal of Fatigue Vol. 28

      Pages: 1509-1520

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] The effect of hydrogen on fatigue properties of metals used for fuel cell system2006

    • Author(s)
      Y.MURAKAMI
    • Journal Title

      International Journal of Fracture 138

      Pages: 167-195

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] 高強度鋼の長寿命疲労破壊に及ぼす水素の影響2005

    • Author(s)
      村上敬宜, 長田淳治
    • Journal Title

      材料 54-12

      Pages: 1217-1224

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] 炭素鋼の繰返し応カ-ひずみ特性および疲労挙動に及ぼす水素チャージの影響2005

    • Author(s)
      宇山英幸, 峯洋二, 村上敬宜, 中島優, 森重利紀
    • Journal Title

      材料 54-12

      Pages: 1225-1230

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Fretting Fatigue under Varying Loading below Fretting Fatigue Limit2005

    • Author(s)
      Y.KONDO, C.SAKAE, M.KUBOTA, H.KITAHARA
    • Journal Title

      Fatigue and Fracture of Engineering Materials and Structures 28

      Pages: 501-506

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] 高強度鋼の疲労き裂進展下限界条件に及ぼすき裂寸法,応力比および水素の影響2005

    • Author(s)
      柳原一智, 大柳聡, 久保田祐信, 栄中, 近藤良之
    • Journal Title

      材料 54-12

      Pages: 1237-1243

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] SUS304鋼の疲労特性に及ぼす水素雰囲気の影響2005

    • Author(s)
      河本恭平, 青木雄太, 尾田安司, 野口博司, 東田賢二
    • Journal Title

      日本機械学会論文集(A編) 71-703

      Pages: 443-450

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Fatigue characteristics of a type 304 austenitic stainless steel in hydrogen gas environment2005

    • Author(s)
      Y.AOKI, K.KAWAMOTO, Y.ODA, H.NOGUCHI, K.HIGASHIDA
    • Journal Title

      International Journal of Fracture Vol.133

      Pages: 277-288

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Observation of Hydrogen Distribution around Non-metallic Inclusions in Steels with Tritium Microautoradiography2005

    • Author(s)
      Teppei Otsuka, Hithoshi Hanada, Hidehiko Nakashima, Kan Sakamoto, et al.
    • Journal Title

      Fusion Science and Technology 48

      Pages: 708-711

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Profiling of hydrogen accumulation in a tempered martensite microstructure by means of tritium autoradiography2005

    • Author(s)
      Hitoshi Hanada, T.Otsuka, H.Nakashima, et al.
    • Journal Title

      Scr. Mater 53

      Pages: 1279-1284

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Nicolas GUY and Yukitaka MURAKAMI, Effect of Hydrogen Charge on Fatigue Strength of Martensitic Stainless Steel.2005

    • Author(s)
      Junji NAGATA
    • Journal Title

      Journal of the Society of Materials Science, Japan Vol. 54, No. 12

      Pages: 1217-1224

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Effect of Hydrogen Charge on Cyclic Stress-Strain Properties and Fatigue Behaviour of Carbon Steel.2005

    • Author(s)
      Hideyuki UYAMA, Yoji MINE, Yukitaka MURAKAMI, Masaru NAKAJIMA, Toshiki MORISHIGE
    • Journal Title

      Journal of the Society of Materials Science, Japan Vol. 54, No. 12

      Pages: 1225-1230

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Non-propagating Crack Behavior at Giga-cycle Fretting Fatigue Limit2005

    • Author(s)
      Y.KONDO, C.SAKAE, M.KUBOTA, K.YANAGIHARA
    • Journal Title

      Fatigue and Fracture of Engineering Materials and Structures 28

      Pages: 501-506

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Effect of Crack Size Stress Ratio and Hydrogen on the Near Threshold Fatigue Crack Propagation of High Strength Steel.2005

    • Author(s)
      K.YANAGIHARA, S.OHYANAGI, M.KUBOTA, C.SAKAE, Y.KONDO
    • Journal Title

      Journal of the Society of Materials Science, Japan Vol. 54, No. 12

      Pages: 1237-1243

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Effect of Hydrogen Envionment on Fatigue Characteristics in a Type 304 Austenitic Stainless Steel.2005

    • Author(s)
      K.KAWAMOTO, Y.AOKI, Y.ODA, H.NOGUCHI, K.HIGASHIDA
    • Journal Title

      Transactions of the Japan Society of Mechanical Engineers. A, Vol. 71, No. 703

      Pages: 443-450

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Fatigue characteristics of a type 304 austenitic stainless steel in hydrogen gas environment2005

    • Author(s)
      Y.AOKI, K.KAWAMOTO, Y.ODA, H.NOGUCHI, K.HIGASHIDA
    • Journal Title

      International Journal of Fracture 133

      Pages: 277-288

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Observation of Hydrogen Distribution around Non-Metallic Inclusion in the Steel with Tritium Microautoradiagraphy2005

    • Author(s)
      Teppei Otsuka, Hitoshi Hanada, Hidehiko Nakashima, Kan Sakamoto, Masayasu Sugisaki, Kenichi Hashizume
    • Journal Title

      Fusion Science and Technology 48

      Pages: 708-711

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Profiling of hydrogen accumulation in a tempered martensite microstructure by means of tritium autoradiography2005

    • Author(s)
      Hitoshi Hanada, T.Otsuka, H.Nakashima, S.Sasaki, M.Hayakawa, M.Sugisaki
    • Journal Title

      Scr. Mater. 53

      Pages: 1279-1284

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Gigacycle fatigue properties of a modified-ausformed Si-Mn steel and effects of microstructure2004

    • Author(s)
      Y.FURUYA, S.MATSUOKA
    • Journal Title

      METALLURGICAL AND MATERIALS TRANSACTIONS A 35A

      Pages: 1715-1723

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Inclusion-Controlled Fatigue Properties of 1800 MPa-Class Spring Steels2004

    • Author(s)
      Y.Furuya, S.Matsuoka, T.Abe
    • Journal Title

      Metallurgical and Materials Transactions A 35A

      Pages: 3737-3744

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Gigacycle fatigue properties of a modified-ausformed Si-Mn steel and effects of microstructure2004

    • Author(s)
      Y.FURUYA, S.MATSUOKA
    • Journal Title

      METALLURGICAL AND MATERIALS TRANSACTIONS A Vol. 35A

      Pages: 1715-1723

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Inclusion-controlled fatigue properties of 1800 MPa-class spring steels2004

    • Author(s)
      Y.FURUYA, S.MATSUOKA, T.ABE
    • Journal Title

      METALLURGICAL AND MATERIALS TRANSACTIONS A 35A

      Pages: 3737-3744

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] 高強度鋼の超長寿命疲労破壊における水素の影響とODAの破面形態2003

    • Author(s)
      植田徹, 村上敬宜
    • Journal Title

      日本機械学会論文集, A 69-681

      Pages: 908

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] 超長寿命疲労破壊におけるODA(Optically Dark Area)の形成に及ぼす諸因子2003

    • Author(s)
      長田淳治, 村上敬宜
    • Journal Title

      材料 52・8

      Pages: 966

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] 改良オースフォームを適用したSCM440鋼の高サイクル疲労特性(第2報,1600MPaおよび2000MPa級改良オースフォーム材の疲労特性)2003

    • Author(s)
      古谷佳之, 松岡三郎
    • Journal Title

      日本機械学会論文集(A編) 68-673

      Pages: 1334

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] 10^<10>-cycle fatigue properties of 1800 MPa-class JIS-SUP7 spring steel2003

    • Author(s)
      Y.FURUYA, T.ABE, S.MATSUOKA
    • Journal Title

      Fatigue Fract. Engng. Mater. Struct 26

      Pages: 641

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] A novel inclusion inspection method employing 20 kHz fatigue testing2003

    • Author(s)
      Y.FURUYA, S.MATSUOKA, T.ABE
    • Journal Title

      MWTALLURGICAL AND MATERIALS TRANSACTIONS A 34A

      Pages: 2517

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Enhanced susceptibility to delayed fracture in pre-fatigued martensitic steel2003

    • Author(s)
      M.Nagumo, S.Sekiguchi, H.Hayashi, K.Takai
    • Journal Title

      Materials Science and Engineering A344

      Pages: 86

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Hydrogen in Trapping States Innocuous to Environmental Degradation of High-Strength Steels2003

    • Author(s)
      Kenichi TAKAI, Ryu WATANUKI
    • Journal Title

      ISIJ International 43-4

      Pages: 520

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Fatigue Damage and Its Interaction with Hydrogen in Martensitic Steels2003

    • Author(s)
      M.Nagumo, H.Shimura, T.Chaya, H.Hayashi, I.Ochiai
    • Journal Title

      Material Science and Engineering 348

      Pages: 192-200

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Amorphization associated with crack propagation in hydrogen-charged steel2003

    • Author(s)
      M.Nagumo, T.Ishikawa, T.Endoh, Y.Inoue
    • Journal Title

      Scripta Materialia 49

      Pages: 837-842

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Effect of Hydrogen on Ultralong Life Fatigue Failure of a High Strength Steel and Fracture Morphology of ODA.2003

    • Author(s)
      UEDA Tohru, MURAKAMI Yukitaka
    • Journal Title

      Transactions of the Japan Society of Mechanical Engineers. A, Vol. 69, No. 681

      Pages: 908

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Factors Influencing the Formation of ODA in Ultralong Fatigue Regime.2003

    • Author(s)
      Junji NAGATA, Yukitaka MURAKAMI
    • Journal Title

      Journal of the Society of Materials Science, Japan Vol. 52, No. 8

      Pages: 966-973

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] High-Cycle Fatigue Properties of Modified-Ausformed SCM440 Steels(2^<nd> Report, Fatigue Properties of 1600 MP and 2000 MPa-Class Modified-Ausformed and Tempered Steel.)2003

    • Author(s)
      FURUYA Yoshiyuki, MATSUOKA Saburo
    • Journal Title

      Transactions of the Japan Society of Mechanical Engineers. A, Vol. 68, No. 673

      Pages: 1344

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] 1010-cycle fatigue properties of 1800 MPa-class JIS-SUP7 spring steel2003

    • Author(s)
      Y.FURUYA, T.ABE, S.MATSUOKA
    • Journal Title

      Fatigue Fract. Engng. Mater. Struct. 26

      Pages: 641

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] A novel inclusion inspection method employing 20 kHz fatigue testing2003

    • Author(s)
      Y.FURLTYA, S.MATSUOKA, T.ABE
    • Journal Title

      METALLURGICAL AND MATERIALS TRANSACTIONS A 34A

      Pages: 2517

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Mechanism of fatigue failure in ultralong life regime2002

    • Author(s)
      Y.Murakami, N.N.Yokoyama, J.Nagata
    • Journal Title

      Fatigue Fracture Engng Mater. Struct. 25

      Pages: 735

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Improvement of Gigacycle Fatigue Properties by Modified Ausforming in 1600 and 2000 MPA-Crass Low-Alloy Steels2002

    • Author(s)
      Y.FURUYA, S.MATSUOKA
    • Journal Title

      METALLURGICAL AND MATERIALS TRANSACTIONS A 33A

      Pages: 3421

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Visualization of Hydrogen Desorption Process from Ferrite, Pearlite and Graphite by Secondary Ion Mass Spectrometry2002

    • Author(s)
      K.Takai, Y.Chiba, K.Noguchi, A.Nozue
    • Journal Title

      Metallurgical and Materials Transactions A Vol.33A

      Pages: 2659-2665

    • Description
      「研究成果報告書概要(和文)」より
  • [Patent(Industrial Property Rights)] 疲労強度改善鋼とその製造方法2003

    • Inventor(s)
      蛭川寿, 古谷佳之, 松岡三郎, 阿部孝行
    • Industrial Property Number
      特願2003-313149
    • Acquisition Date
      2003-09-04
    • Description
      「研究成果報告書概要(和文)」より
  • [Patent(Industrial Property Rights)] ギガサイクル疲労特性の評価法とギガサイクル疲労特性が改善された高強度鋼とその製造方法2003

    • Inventor(s)
      古谷佳之, 蛭川寿, 松岡三郎, 阿部孝行
    • Industrial Property Number
      特願2003-341234
    • Acquisition Date
      2003-09-30
    • Description
      「研究成果報告書概要(和文)」より

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Published: 2008-05-27  

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