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2004 Fiscal Year Final Research Report Summary

Development of Microactuators Possessing High Power and Large Actuation Utilizing Ti-Ni Sputter-deposited Shape Memory Alloy Films

Research Project

Project/Area Number 14205099
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionUniversity of Tsukuba

Principal Investigator

MIYAZAKI Shuichi  University of Tsukuba, Graduate School of Pure and Applied Sciences, Professor, 大学院・数理物質科学研究科, 教授 (50133038)

Co-Investigator(Kenkyū-buntansha) KIM Hee Young  University of Tsukuba, Graduate School of Pure and Applied Sciences, Assistant Professor, 大学院・数理物質科学研究科, 講師 (20333841)
Project Period (FY) 2002 – 2004
Keywordsshape memory effect / shape memory alloy / Ti-Ni / Ti-Ni-Pd / Ti-Ni-Cu / sputtering / microactuator / martensitic transformation
Research Abstract

Ti-Ni shape memory alloy thin films are expected to be applied for microactuators due to the great advantages such as large shape recovery force and strain. In this research, Ti-Ni thin films were deposited on Si substrates with SiO2 surface by using the radio frequency magnetron sputtering method. Diaphragm microactuators were fabricated by applying the Si photoetching method, and heat-treatment was carried out in order to acquire shape memory effects. The shape of the diaphragm was square with the width of 560 micron meters. The Ti-Ni diaphragm was convex in the martensite phase and flat in the parent phase : the shape change occurred repeatedly by cooling and heating. In order to evaluate the dynamic motion of the diaphragm microactuator, a three-dimensional shape analysis was performed with varying experimental parameters such as frequency and current. It was found that the displacement of the Ti-Ni binary alloy microactuator was changed by changing the current and/or the frequency … More .
A Ti-Ni microactuator revealed an effective cyclic response below a cyclic frequency of several tens Hz. In order to improve the cyclic response, Pd was added to make Ti-Ni-Pd thin films for microactuators, because Pd addition increases the Ms temperature so that a higher cooling rate can be expected at a higher temperature. The maximum Ms temperature of the Ti-Ni was 340K, while that of the Ti-Ni-Pd was 420K which is 80K higher than that of the binary alloy. A Ti-Ni-Pd microactuator revealed effective actuation at 80 Hz. Cu was also added to make Ti-Ni-Cu thin films, which posses a narrower transformation temperature hysteresis and a smaller transformation strain when compared with those of the Ti-Ni films : the hysteresis of the former is only one third of that of the latter. An effective actuation was observed in the Ti-Ni-Cu microactuator even at 100 Hz. A narrow transformation temperature hysteresis can be also expected by using the R-phase transformation. A Ti-Ni microactuator showed an effective motion even at 125 Hz. With the results mentioned above, high speed and powerful microactuators can be fabricated for variety of purposes in the near future. Less

  • Research Products

    (10 results)

All 2005 2004 2003 2002

All Journal Article (9 results) Patent(Industrial Property Rights) (1 results)

  • [Journal Article] Effect of Nano-scaled Precipitates on Shape Memory Behavior of Ti-50.9at%Ni Alloy2005

    • Author(s)
      J.I.Kim, S.Miyazaki
    • Journal Title

      Acta Materialia 53

      Pages: 4545-4554

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Aging-induced Two-stage R-phase Transformation in Ti-50.9at%Ni2005

    • Author(s)
      J.I.Kim, Y.Liu, S.Miyazaki
    • Journal Title

      Acta Materialia 52

      Pages: 487-499

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Fabrication and Characterization of Ti-Ni Shape Memory Thin Film Using Ti/Ni Multilayer Technique2005

    • Author(s)
      H.Cho, H.Y.Kim, S.Miyazaki
    • Journal Title

      Science and Technology of Advanced Materials 6

      Pages: 678-683

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Characterization of High-Speed Microactuator Utilizing Shape Memory Alloy Thin Films2005

    • Author(s)
      M.Tomozawa, K.Okutsu, H.Y.Kim, S.Miyazaki
    • Journal Title

      Materials Science Forum 475-479

      Pages: 2037-2042

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] A TiNiPd Thibn Film Microvalve for High Temperature Applications2004

    • Author(s)
      Y.Liu, M.Kohl, K.Okutsu, S.Miyazaki
    • Journal Title

      Materials Science and Engineering, A 378

      Pages: 205-209

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Thermodynamic Analysis of Aging-induced Multiple-stage Transformation Behavior of NiTi2004

    • Author(s)
      Y.Liu, J.I.Kim, S.Miyazaki
    • Journal Title

      Philosophical Magazine A 84

      Pages: 2083-2102

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Thermodynamic Analysis of Ageing-induced Multiple-stage Transformation Behavior of NiTi2004

    • Author(s)
      Y.Liu, J.I.Kim, S.Miyazaki
    • Journal Title

      Phil.Mag.A 84

      Pages: 2083-2102

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Ageing-inducede Two-stage R-phase Transformation in Ti-50.9at%Ni2004

    • Author(s)
      J.I.Kim, Y.Liu, S.Miyazaki
    • Journal Title

      Acta Materialia 52

      Pages: 487-499

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] 形状記憶合金薄膜マイクロアクチュエータ2003

    • Author(s)
      宮崎修一
    • Journal Title

      未来材料 3

      Pages: 2-5

    • Description
      「研究成果報告書概要(和文)」より
  • [Patent(Industrial Property Rights)] Ti-Ni-Cu系形状記憶合金2002

    • Inventor(s)
      宮崎修一, 他4
    • Industrial Property Rights Holder
      科学技術振興事業団
    • Patent Publication Number
      特開2002-294371
    • Filing Date
      20021009 公開
    • Description
      「研究成果報告書概要(和文)」より

URL: 

Published: 2007-12-13  

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