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2005 Fiscal Year Final Research Report Summary

Property Evaluation and Application of Ultrafine Grained Steel

Research Project

Project/Area Number 15206077
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionKYUSHU UNIVERSITY

Principal Investigator

TAKAKI Setsuo  KYUSHU UNIVERSITY, Faculty of Engineering, Professor, 大学院・工学研究院, 教授 (90150490)

Co-Investigator(Kenkyū-buntansha) HIGASHIDA Kenji  KYUSHU UNIVERSITY, Faculty of Engineering, Associate Professor, 大学院・工学研究院, 助教授 (70156561)
TSUCHIYAMA Toshihiro  KYUSHU UNIVERSITY, Faculty of Engineering, Associate Professor, 大学院・工学研究院, 助教授 (40315106)
MORIKAWA Tatsuya  KYUSHU UNIVERSITY, Faculty of Engineering, Research Associate, 大学院・工学研究院, 助手 (00274506)
NAKASHIMA Koichi  KYUSHU UNIVERSITY, Faculty of Engineering, Research Associate, 大学院・工学研究院, 助手 (30363378)
NAKADA Nobuo  KYUSHU UNIVERSITY, Faculty of Engineering, Research Associate, 大学院・工学研究院, 助手 (50380580)
Project Period (FY) 2003 – 2005
Keywordsultrafine Brained steel / mechanical milling / dislocation density / mechanical property / Hall-Petch
Research Abstract

For the purpose of evaluating the properties of submicron fine grained steels and exploring their possibilities of application, this study had been carried out for three years. We had 8 themes for investigating the submicron fine grained steels, but they are classified into three categories : (1)Fabrication and processing technique of submicron fine grained steels, (2)Microstructure analysis, (3)Evaluation of mechanical properties, and (4)Analysis of strengthening mechanism.
We succeeded to fabricate submicron fine grained steels by adopting powder metallurgy technique (mechanical milling process). In addition, hot excursion method to form rod steel of several cm in diameter was also developed for applying to automobile parts. As for the analysis of the microstructure obtained, the local structure analysis and measurement of the dislocation density were performed by X ray diffractometry for fine selected areas ; the submicron grained structure and the dislocation substructure were caref … More ully observed with TEM ; the orientation distribution and the texture were examined with FE-SEM-EBSP method. The mechanical properties were investigated by means of tensile testing at various temperatures ranging from low temperature of liquid nitrogen to elevated temperature. As a result, it was clarified that the submicron fine grained steels do not cause brittle fracture but ductile fracture even at low temperature, and that they exhibit superplasticity at elevated temperature, leading to the excellent deformability. Besides, we insisted that the combination of the grain refinement strengthening and other strengthening mechanism should be important to realize further strengthening. On the basis of this idea, the effect of combination of grain refinement and nano-Cu precipitation was investigated, and then we found that the yield strength of the steel is sometimes explained by the addition of both strengthening mechanism. However, it was also found the new facts that the ultrafine grained steel never exhibits age hardening and dislocation strengthening; thus we feel that the submicron fine grained steels should be moved to nano-grained material in the next stage. Less

  • Research Products

    (17 results)

All 2005 2004 2003

All Journal Article (17 results)

  • [Journal Article] Deformation Behavior of Ultrafine Grained Iron2005

    • Author(s)
      S.TAKAKI, K.KAWASAKI, Y.FUTAMURA, T.TSUCHIYAMA
    • Journal Title

      Materials Science Forum 503-504

      Pages: 317-322

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Characterization of nanocrystalline ferrite produced by mechanical milling of pearlitic steel2005

    • Author(s)
      S.Ohsaki, K.Hono, H.Hidaka, S.Takaki
    • Journal Title

      Scripta Materialia 52

      Pages: 271-276

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] 「研究成果報告書概要(欧文)」より2005

    • Author(s)
      S.TAKAKI, K.KAWASAKI, Y.FUTAMURA, T.TSUCHIYAMA
    • Journal Title

      Materials Science Forum 503-504

      Pages: 317-322

  • [Journal Article] 「研究成果報告書概要(欧文)」より2005

    • Author(s)
      S.Ohsaki, K.Hono, H.Hidaka, S.Takaki
    • Journal Title

      Scripta Materialia 52

      Pages: 271-276

  • [Journal Article] Effect of Initial Microstructure on Superplasticity in Ultrafine Grained 18Cr-9Ni Stainless Steel2004

    • Author(s)
      T.Tsuchiyama, Y.Nakamura, H.Hidaka, S.Takaki
    • Journal Title

      Materials Transactions 45

      Pages: 2259-2263

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Effect of Grain Refinement on Thermal Stability of Metastable Austenitic Steel2004

    • Author(s)
      Setsuo Takaki, Kazuhiro Fukunaga, Junaidi Syarif, Toshihiro Tsuchiyama
    • Journal Title

      Materials Transactions 45

      Pages: 2245-2251

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Microstructure Development f Steel during Severe Plastic Deformation2004

    • Author(s)
      S.Takaki, T.Tsuchiyama K.Nakashima, H.Hidaka, K.Kawasaki, Y.Futamura
    • Journal Title

      Metals and Materials International 10

      Pages: 533-539

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] 「研究成果報告書概要(欧文)」より2004

    • Author(s)
      T.Tsuchiyama, Y.Nakamura, H.Hidaka, S.Takaki
    • Journal Title

      Materials Transactions 45

      Pages: 2259-2263

  • [Journal Article] 「研究成果報告書概要(欧文)」より2004

    • Author(s)
      Setsuo Takaki, Kazuhiro Fukunaga, Junaidi Syarif, Toshihiro Tsuchiyama
    • Journal Title

      Materials Transactions 45

      Pages: 2245-2251

  • [Journal Article] 「研究成果報告書概要(欧文)」より2004

    • Author(s)
      S.Takaki, T.Tsuchiyama, K.Nakashima, H.Hidaka, K.Kawasaki, Y.Futamura
    • Journal Title

      Metals and Materials International 10

      Pages: 533-539

  • [Journal Article] High-resolution TEM Analysis of Defect Structures in Mechanically Milled Nanocrystalline Fe2003

    • Author(s)
      M.Murayama, J.M.Howe, H.Hidaka, S.Takaki
    • Journal Title

      ISIJ International 43

      Pages: 755-760

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Effect of Carbon on Nano-Crystallization in Steel during Mechanical Milling Treatment2003

    • Author(s)
      H.Hidaka, T.Tsuchiyama, S.Takaki
    • Journal Title

      Materials transactions 44

      Pages: 1912-1918

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Microstructural Change during Mechanical Millling Treatment in Fe-C Alloy Powders with Different Initial Microstructure2003

    • Author(s)
      H.Hidaka, T.Tsuchiyama, S.Takaki
    • Journal Title

      Materials Science Forum 426-432

      Pages: 2717-2722

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Limit of Dislocation Density and Ultra-Grain-Refining on Severs Deformation in Iron2003

    • Author(s)
      S.Takaki
    • Journal Title

      Materials Science Forum 426-432

      Pages: 215-222

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] 「研究成果報告書概要(欧文)」より2003

    • Author(s)
      H.Hidaka, T.Tsuchiyama, S.Takaki
    • Journal Title

      Materials transactions 44

      Pages: 1912-1918

  • [Journal Article] 「研究成果報告書概要(欧文)」より2003

    • Author(s)
      H.Hidaka, T.Tsuchiyama, S.Takaki
    • Journal Title

      Materials Science Forum 426-432

      Pages: 2717-2722

  • [Journal Article] 「研究成果報告書概要(欧文)」より2003

    • Author(s)
      S.Takaki
    • Journal Title

      Materials Science Forum 426-432

      Pages: 215-222

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Published: 2007-12-13  

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