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2015 Fiscal Year Research-status Report

ジルコニアインプラントへの新規ハイドロキシアパタイト成膜法

Research Project

Project/Area Number 15K11167
Research InstitutionNagasaki University

Principal Investigator

バラネザハド アリレザ  長崎大学, 医歯薬学総合研究科(歯学系), 助教 (00608870)

Co-Investigator(Kenkyū-buntansha) 渡邊 郁哉  長崎大学, 医歯薬学総合研究科(歯学系), 教授 (00274671)
白石 孝信  長崎大学, 医歯薬学総合研究科(歯学系), 准教授 (10150468)
尾立 哲郎  長崎大学, 医歯薬学総合研究科(歯学系), 助教 (70513167)
Project Period (FY) 2015-04-01 – 2018-03-31
KeywordsZirconia / Bioactive Coating / Zinc Phosphate
Outline of Annual Research Achievements

Recently zirconia ceramic gains attraction as a dental implant material. However zirconia has been known as a bioinert ceramic therefore to make bioactive surface, different treatments have been developed. For example calcium phosphate coating is one of the methods could induce bioactivity to the zirconia surface. On the other hand, zinc phosphate is known as dental cement. Industrial applications for zinc phosphate coating are corrosion and wear resistance. Previously, it was reported that calcium phosphate could be formed on the zinc phosphatized titanium by using calcium solution. The zirconia tablets were made by biaxial pressing zirconia powder. The pressed tablets were sintered at 1400℃ for 3h. The prepared zirconia discs were placed in the zinc phosphate solution which was made by mixing zinc phosphatizing solution in a hydrothermal vessel maintained at 200℃. SEM images show that plate-like crystals were formed on the zirconia discs surface of the hydrothermally-treated with zinc phosphate solution at 200℃ for 12 h. The coating layer was covered zirconia surface completely. The samples coated with less time duration or lower treatment temperature showed less coating crystals with low surface coverage percentage. The coating layer with thickness less than 5μm of covered on the zirconia surface. In addition, for the XRD patterns 2 series of peaks were assigned for zirconia and zinc phosphate crystals. The intensity of zirconia and zinc phosphate coating peaks has been changed by increasing the thickness of coating layer.

Current Status of Research Progress
Current Status of Research Progress

2: Research has progressed on the whole more than it was originally planned.

Reason

We have coated zirconia by zinc phosphate successfully

Strategy for Future Research Activity

This year calcium phosphate coating will be formed and characterize on the zinc phosphate coating and cell study will be done.

Causes of Carryover

We didn't buy goods.

Expenditure Plan for Carryover Budget

We have plan to order cell study materials.

  • Research Products

    (5 results)

All 2016 2015

All Journal Article (1 results) (of which Peer Reviewed: 1 results) Presentation (4 results) (of which Int'l Joint Research: 3 results)

  • [Journal Article] Fabrication of strongly attached hydroxyapatite coating on titanium by hydrothermal treatment of Ti-Zn-PO4 coated titanium in CaCl2 solution2015

    • Author(s)
      Valanezhad A, Tsuru K, Ishikawa K
    • Journal Title

      J Mater Sci - Mater Med

      Volume: 26 Pages: 212(1-10)

    • Peer Reviewed
  • [Presentation] Zinc phosphate coating on the zirconia dental implants2016

    • Author(s)
      Kodama K, Valanezhad A, Murata H, Watanabe I
    • Organizer
      第67回日本歯科理工学会学術講演会
    • Place of Presentation
      九州大学( 福岡県 福岡市)
    • Year and Date
      2016-04-16 – 2016-04-17
  • [Presentation] Mechanical and biological performance of glass ionomer cement modified by bioactive glass nanoparticles2015

    • Author(s)
      Valanezhad A, Shiraishi T, Sawase T, Watanabe I
    • Organizer
      27th Symposium and Annual Meeting of The International Society for Ceramics in Medicine
    • Place of Presentation
      Bali, Indonesia
    • Year and Date
      2015-10-27 – 2015-10-29
    • Int'l Joint Research
  • [Presentation] Evaluation of the bone regeneration potential of bioactive glass enhanced with PRP and BMP2 in an augmentation model. A comparative study2015

    • Author(s)
      Nourani M, Sumita Y, Valanezhad A, Watanabe I, Asahina I
    • Organizer
      The 15th Meeting of Iranian Academy of Periodontology
    • Place of Presentation
      Tehran, Iran
    • Year and Date
      2015-10-06 – 2015-10-09
    • Int'l Joint Research
  • [Presentation] Effects of bioactive glass nanoparticles on glass ionomer cement properties2015

    • Author(s)
      Valanezhad A, Watanabe I
    • Organizer
      International Porous Powder Materials (PPM)
    • Place of Presentation
      Izmir, Turkey
    • Year and Date
      2015-09-15 – 2015-09-18
    • Int'l Joint Research

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Published: 2017-01-06  

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