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2005 Fiscal Year Final Research Report Summary

Quantitative evaluation of microstructure in concretes by SEM-BSE image analysis

Research Project

Project/Area Number 16560398
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Civil engineering materials/Construction/Construction management
Research InstitutionKanazawa University

Principal Investigator

IGARASHI Shin-ichi  Kanazawa University, Graduate School of Natural Science and Technology, Associate Professor, 自然科学研究科, 助教授 (50168100)

Co-Investigator(Kenkyū-buntansha) KUBO Yoshimori  Kanazawa University, Graduate School of Natural Science and Technology, Research Associate, 自然科学研究科, 助手 (50324108)
Project Period (FY) 2004 – 2005
KeywordsBack-scattered Electron Image / Image Analysis / Powers-Brownyard Model / W / C Estimation / Internal Curing / Stereology / 3D Particle Size Distribution / Diffusion Coefficient
Research Abstract

Major results obtained in this research are as follows ;
1. The degrees of hydration of determined by the BSE image analysis were consistent with the Powers model. The volume fractions of each constituent phase can be calculated by the combination of BSE image analysis and the Powers model.
2. Lower W/C ratios and the addition of mineral admixtures resulted in less fine capillary pores.
3. The gap-graded pore structure in which the volume of fine capillary pores is quite smaller than that of large pores, affects the development of compressive strength.
4. There exists a good correlation between compressive strength and the coarse capillary porosity measured by the image analysis.
5. Coarse capillary pore structure revealed by the image analysis reflected differences in mix proportions, ages and curing conditions.
6. The presence of larger amounts of fine capillary pores in cement pastes with silica fume may be responsible for greater autogenous shrinkage in silica fume-containing concrete at … More early ages.
7. The gel-space ratio theory by Powers and Brownyard can be applied to cement pastes containing mineral admixtures such as silica fume and fly ash. However, the ultimate strength extrapolated from the theory is smaller in the admixture-containing cement pastes than in the ordinary cement pastes with the same water/binder ratio. This results from the greater volume ratio of coarse pores to the total porosity in the cement pastes with the extenders.
8. Water cement ratios of hardened concretes can be estimated by the proper combination of the image analysis and the degree of hydration determined by the non-evaporable water content.
9. The 3D particle size distribution of unhydrated cement was obtained from the 2D distribution by the Saltykov method.
10. The mean diameter in the 3D distribution can be used as a parameter of degree of hydration of cement.
11. Water cement ratios of hardened concretes can be properly determined by a combination of the mean diameter and the degree of hydration.
12. Diffusion coefficients of cement pastes with and without admixtures were obtained by the solvent exchange method. There was a good correlation between the coefficients and characteristic diameters in coarse capillary pore structure.
13. Effects of the internal water supply on microstructure around the water reservoirs were examined by the image analysis. The image analysis showed that the distance to supply water from the reservoir is at most few hundred micrometers. Less

  • Research Products

    (26 results)

All 2006 2005 2004

All Journal Article (26 results)

  • [Journal Article] 超吸水性ポリマーの使用による自己収縮の抑制効果2006

    • Author(s)
      五十嵐心一, 渡辺暁央
    • Journal Title

      セメントコンクリート論文集 59

      Pages: 109-116

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Effects of Pozzolanic reaction on the evolution of coarse capillary pore structure and phase constitution in cement pastes with mineral admixtures2006

    • Author(s)
      Igarashi, S., Watanabe, A.
    • Journal Title

      Proc.of International RILEM-JCI seminar, Concrete Life '06 (in press)

      Pages: 83-93

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Prevention of Autogenous Deformation by Internal Curing Using Super Absorbent Polymer Particles2006

    • Author(s)
      Igarashi, S., Watanabe, A.
    • Journal Title

      Cement Science and Concrete Technology No.59, Vol.59

      Pages: 109-116

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Effects of Pozzolanic reaction on the evolution of coarse capillary pore structure and phase constitution in cement pastes with mineral admixtures2006

    • Author(s)
      Igarashi, S., Watanabe, A.
    • Journal Title

      Proc.of International RILEM-JCI Seminar, Concrete Life '06 (ed. K.Kovler)

      Pages: 83-93

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] 残存未水和セメント粒子の粒度分布の評価に基づくと水セメント比の推定2005

    • Author(s)
      五十嵐心一, 池崎由典, 渡辺暁央
    • Journal Title

      コンクリート工学論文集 16・1

      Pages: 87-95

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] 反射電子像の画像解析による鉱物質混和材混入セメントペーストの細孔構造の解明2005

    • Author(s)
      渡辺暁央, 五十嵐心一, 川村満紀
    • Journal Title

      土木学会論文集 No.781/V-66

      Pages: 145-155

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Evaluation of Capillary Pore Size Characteristics in High Strength Concrete at Early Ages2005

    • Author(s)
      Igarashi, S., Watanabe, A., Kawamura, M
    • Journal Title

      Cement and Concrete Research 35・3

      Pages: 513-519

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] 2,3の手法により求めたセメントの水和度の比較2005

    • Author(s)
      井上豪, 五十嵐心一
    • Journal Title

      コンクリート工学年次論文集 27・1

      Pages: 541-546

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] セメント硬化体の物質透過性に及ぼす粗大毛細管空隙構造の影響2005

    • Author(s)
      田野原孝之, 五十嵐心一
    • Journal Title

      コンクリート工学年次論文集 27・1

      Pages: 823-828

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Determination of Degree of Hydration and Water/Cement Ratio by Stereological Analysis of Unhydrated Cement Particles2005

    • Author(s)
      Igarashi, S., Ikezaki, Y., Watanabe, A.
    • Journal Title

      Proc.of CONMAT'05 and Mindess Symposium (CD-ROM)

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Determination of degree of hydration and water/cement ratio by three dimensional particle size distribution of unhydrated cement in concrete2005

    • Author(s)
      Igarashi, S., Ikezaki, Y., Watanabe, A.
    • Journal Title

      Concrete Research and Technology Vol.16, No.1

      Pages: 87-95

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Coarse capillary pore structures and phase constitution in cement paste with mineral admixtures2005

    • Author(s)
      Watanabe, A., Igarashi, S., Kawamura
    • Journal Title

      Journal of Materials, Concrete structures and pavements No.781/V-66

      Pages: 145-155

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Evaluation of Capillary Pore Size Characteristics in High Strength Concrete at Early Ages2005

    • Author(s)
      Igarashi, S., Watanabe, A., Kawamura, M
    • Journal Title

      Cement and Concrete Research Vol.35, No.3

      Pages: 513-519

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Several methods to estimate the degree of hydration in cement pastes2005

    • Author(s)
      Inoue, T., Igarashi, S.
    • Journal Title

      Proc.of the Japan Concrete Institute Vol.27, No.1

      Pages: 541-546

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Effects of Coarse capillary pore structures on diffusion properties in cement pastes2005

    • Author(s)
      Tanohara, T., Igarashi, S.
    • Journal Title

      Proc.of the Japan Concrete Institute Vol.27, No.1

      Pages: 823-828

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Determination of Degree of Hydration and Water/Cement Ratio by Stereological Analysis of Unhydrated Cement Particles2005

    • Author(s)
      Igarashi, S., Ikezaki, Y., Watanabe, A
    • Journal Title

      Proc.of CONMATO5 and Mindess Symposium (CD-ROM)

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] 加圧処理を施した繊維補強RPCの微視的構造と力学的特性2004

    • Author(s)
      渡辺暁央, 五十嵐心一, 川村満紀
    • Journal Title

      コンクリート工学年次論文集 26・1

      Pages: 09-314

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] 軽量骨材による内部養生が高強度コンクリートの内部組織形成に及ぼす影響2004

    • Author(s)
      加藤俊充, 五十嵐心一, 川村満紀
    • Journal Title

      コンクリート工学年次論文集 26・1

      Pages: 675-680

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] 画像解析による硬化コンクリートの配合推定2004

    • Author(s)
      池崎由典, 五十嵐心一, 川村満紀
    • Journal Title

      コンクリート工学年次論文集 26・1

      Pages: 2019-2024

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Analysis of Cement Pastes and Mortars by a Combination of Backscatter-Based SEM Image Analysis and Calculations Based on the Powers Model2004

    • Author(s)
      Igarashi, S., Kawamura, M., Watanabe, A.
    • Journal Title

      Cement and Concrete Composites 26・8

      Pages: 977-985

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Effects of curing conditions on the evolution of coarse capillary pores in cement pastes2004

    • Author(s)
      Igarashi, S., Watanabe, A., Kawamura, M.
    • Journal Title

      Concrete Science and Engineering, A Tribute to Arnon Bentur, Proc.of the Intl.RILEM Symp. PRO36

      Pages: 105-116

    • Description
      「研究成果報告書概要(和文)」より
  • [Journal Article] Microstructure and Strength of RPC Treated by Pre-Setting Pressurization2004

    • Author(s)
      Watanabe, A., Igarashi, S., Kawamura, M.
    • Journal Title

      Proc.of the Japan Concrete Institute Vol.26, No.1

      Pages: 309-314

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Effects of internal curing by lightweight aggregate on microstructure in high strength concrete2004

    • Author(s)
      Kato, T., Igarashi, S., Kawamura, M.
    • Journal Title

      Proc.of the Japan Concrete Institute Vol.26, No.1

      Pages: 675-680

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Estimation of Mix Proportions of Hardened Concretes by Image Analysis2004

    • Author(s)
      Ikezaki, Y., Igarashi, S., Kawamura, M.
    • Journal Title

      Proc.of the Japan Concrete Institute Vol.26, No.1

      Pages: 2019-2024

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Analysis of Cement Pastes and Mortars by a Combination of Backscatter-Based SEM Image Analysis and Calculations Based on the Powers Model2004

    • Author(s)
      Igarashi, S., Kawamura, M., Watanabe, A.
    • Journal Title

      Cement and Concrete Composites Vol.26, No.8

      Pages: 977-985

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Effects of curing conditions on the evolution of coarse capillary pores in cement pastes2004

    • Author(s)
      Igarashi, S., Watanabe, A., Kawamura, M.
    • Journal Title

      Concrete Science and Engineering, A Tribute to Arnon Bentur, Proc.of the Intl.RILEM Symp.PRO36

      Pages: 105-116

    • Description
      「研究成果報告書概要(欧文)」より

URL: 

Published: 2007-12-13  

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