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2018 Fiscal Year Annual Research Report

Fatigue crack propagation in steels

Research Project

Project/Area Number 16H06365
Research InstitutionKyushu University

Principal Investigator

津崎 兼彰  九州大学, 工学研究院, 教授 (40179990)

Co-Investigator(Kenkyū-buntansha) 小山 元道  九州大学, 工学研究院, 助教 (20722705)
福島 良博  九州大学, 工学研究院, 助教 (40156774)
野口 博司  九州大学, 工学研究院, 教授 (80164680)
濱田 繁  九州大学, 工学研究院, 准教授 (90432856)
Project Period (FY) 2016-05-31 – 2021-03-31
Keywords疲労変形 / 疲労き裂停留 / 微小疲労き裂 / ひずみ時効 / マルテンサイト変態 / 鉄鋼材料
Outline of Annual Research Achievements

本研究では、出口を見据えた夢のある基礎研究領域として、部材の設計強度を決定する金属疲労に注目して、「疲労き裂研究の新領域」を拓くことを目的としています。そのために、研究代表者達が独自に見出した常識を破る現象である(1)アルミ合金での疲労限の出現と(2)鉄鋼での低サイクル疲労の長寿命化の二つを研究シーズとして、そのメカニズムを徹底解明します。その知見をもとに、(a)高い疲労限を持つオーステナイト系ステンレス鋼や(b)水素環境下でも疲労特性が劣化しない鉄鋼など、従来常識を打ち破る新規の鉄鋼材料の創製を行います。その上で、原子拡散、マルテンサイト変態などによって起こる疲労き裂先端近傍での材質変化を積極的に取り込んだ新しい疲労き裂研究の学問体系の土台を築きます。 第二ステージの初年度となるH30年度は当初計画に従い、応用と基礎の二本立ての取り組みを行いました。主な成果は以下の通りです。
■応用研究:疲労特性に優れた新たな鉄鋼材料を創出する
「耐疲労鋼」については,応力助長型とひずみ誘起型でマルテンサイト変態が起こるFe18Cr8Ni-C合金を用いて、引張強さが同じでも疲労限が大きく上昇することを示しました。「耐水素鋼」については前年度につけた道筋に沿って、水素拡散速度が低いFCC/HCP相に着目して、(FCC+HCP)二相の準安定高エントロピー合金(Fe30Mn10Cr10Co:at%)の疲労き裂進展挙動を調査し、優れた耐水素脆化特性を示すことを見出しました。。
■基礎研究:材質変化を積極的に取り込んだ疲労き裂研究の新機軸を拓く
動的ひずみ時効、マルテンサイト変態、転位プラナリティ、結晶粒径などに着目して、材質変化と疲労き裂進展挙動の関係を調査しました。これらの研究成果は、7報の論文として公表しました。

Current Status of Research Progress
Current Status of Research Progress

1: Research has progressed more than it was originally planned.

Reason

■ 耐疲労鋼での研究進展:プロジェクト1年目に見出した金属疲労に強い組織を持つTRIPマルエージング鋼のメカニズム解明を進めるとともに、応力助長型とひずみ誘起型でマルテンサイト変態が起こるFe18Cr8Ni-C合金を用いて引張強さが同じでも疲労限が大きく上昇することを示しました。これにより第二ステージ応用研究における「耐疲労鋼」の当初目標を達成しました。
■ 研究論文発表:オリジナル論文16報、国際会議プロシーディング論文9報、解説論文1報、合計で論文26報と活発な成果公表を2018年度に行いました。
■ 国際会議での集中的な研究発表:2018年8月のEuropean Conference on Fracture(ECF22@Selbia)にて9件の口頭発表およびProceeding論文投稿を集中的に行い、研究成果を世界に直接発信しました。
■ 2回目のプレス発表:「耐水素鋼」研究の一環として、水素によって熱誘起FCC→HCP変態が抑制されるという従来常識とは異なる新事実を発見し、Scientific Reports誌に論文掲載しました(2018年10月)。この内容についてプレス発表(2017年3月に続いて二度目)を行い、NHKのTVニュースなどで取り上げられました。

Strategy for Future Research Activity

当初の目標を超える研究の進展があり、予定以上の成果が見込まれます。これは当初の研究計画と方法が綿密に練られていて正当であったためと自己評価しています。プロジェクト初年度に前倒し導入した高分解能SEMによる疲労き裂周囲の転位像観察は大いに力を発揮して、導入後の二年間で多くの新知見獲得と論文公表を達成することが出来ました。今後も当初計画に従って着実に研究を遂行する予定でおります。
2018年12月に福井大学で開催された日本機械学会材料力学カンファレンスで「構造材料に生ずる疲労・破壊の力学と材料学」と題するオーガナイズドセッションを企画しました。関連の研究者と良い討論が出来ました。このオーガナイズドセッションはは2019年も継続開催を申請し、開催が認められています。このように関連研究者との討論の場を適宜設けることも進めて参ります。

  • Research Products

    (45 results)

All 2019 2018 Other

All Int'l Joint Research (2 results) Journal Article (26 results) (of which Int'l Joint Research: 7 results,  Peer Reviewed: 26 results,  Open Access: 10 results) Presentation (16 results) (of which Int'l Joint Research: 11 results,  Invited: 4 results) Remarks (1 results)

  • [Int'l Joint Research] マサチューセッツ工科大学(米国)

    • Country Name
      U.S.A.
    • Counterpart Institution
      マサチューセッツ工科大学
  • [Int'l Joint Research] コチ大学/アブドラガル大学(トルコ)

    • Country Name
      TURKEY
    • Counterpart Institution
      コチ大学/アブドラガル大学
  • [Journal Article] Lowering Strain Rate Simultaneously Enhances Carbon- and Hydrogen-Induced Mechanical Degradation in an Fe-33Mn-1.1C Steel2019

    • Author(s)
      Tugluca Ibrahim Burkay、Koyama Motomichi、Shimomura Yusaku、Bal Burak、Canadinc Demircan、Akiyama Eiji、Tsuzaki Kaneaki
    • Journal Title

      Metallurgical and Materials Transactions A

      Volume: 50 Pages: 1137~1141

    • DOI

      https://doi.org/10.1007/s11661-018-5080-7

    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Fatigue Resistance of Laminated and Non-laminated TRIP-maraging Steels: Crack Roughness vs Tensile Strength2019

    • Author(s)
      Zhang Zhao、Koyama Motomichi、Wang Meimei、Tasan Cemal Cem、Noguchi Hiroshi
    • Journal Title

      Metallurgical and Materials Transactions A

      Volume: 50 Pages: 1142~1145

    • DOI

      https://doi.org/10.1007/s11661-018-5081-6

    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Fatigue Behavior in an Fe?N Binary Ferritic Steel: Similarity and Difference between Carbon and Nitrogen2019

    • Author(s)
      Habib Kishan、Koyama Motomichi、Sakurada Eisaku、Yoshimura Nobuyuki、Yokoi Tatsuo、Ushioda Kohsaku、Tsuzaki Kaneaki、Noguchi Hiroshi
    • Journal Title

      ISIJ International

      Volume: 59 Pages: 186~191

    • DOI

      https://doi.org/10.2355/isijinternational.ISIJINT-2018-535

    • Peer Reviewed
  • [Journal Article] Resistance to mechanically small fatigue crack growth in ultrafine grained interstitial-free steel fabricated by accumulative roll-bonding2019

    • Author(s)
      Lin X.、Koyama M.、Gao S.、Tsuji N.、Tsuzaki K.、Noguchi H.
    • Journal Title

      International Journal of Fatigue

      Volume: 118 Pages: 117~125

    • DOI

      https://doi.org/10.1016/j.ijfatigue.2018.09.002

    • Peer Reviewed
  • [Journal Article] EBSD and ECCI Based Assessments of Inhomogeneous Plastic Strain Evolution Coupled with Digital Image Correlation2019

    • Author(s)
      Kakimoto Ryohei、Koyama Motomichi、Tsuzaki Kaneaki
    • Journal Title

      Tetsu-to-Hagane

      Volume: 105 Pages: 222~230

    • DOI

      https://doi.org/10.2355/tetsutohagane.TETSU-2018-072

    • Peer Reviewed
  • [Journal Article] Growth Behavior of a Mechanically Long Fatigue Crack in an FeCrNiMnCo High Entropy Alloy: A Comparison with an Austenitic Stainless Steel2019

    • Author(s)
      Mizumachi Shunsuke、Koyama Motomichi、Fukushima Yoshihiro、Tsuzaki Kaneaki
    • Journal Title

      Tetsu-to-Hagane

      Volume: 105 Pages: 215~221

    • DOI

      https://doi.org/10.2355/tetsutohagane.TETSU-2018-073

    • Peer Reviewed
  • [Journal Article] ECCI Characterization of Dislocation Structures at a Non-propagating Fatigue Crack Tip: Toward Understanding the Effects of Mn-C and Cr-N Couples on Crack Growth Resistance2018

    • Author(s)
      Habib Kishan、Koyama Motomichi、Tsuchiyama Toshihiro、Noguchi Hiroshi
    • Journal Title

      Metallurgical and Materials Transactions A

      Volume: 50 Pages: 426~435

    • DOI

      https://doi.org/10.1007/s11661-018-4972-x

    • Peer Reviewed
  • [Journal Article] An unconventional hydrogen effect that suppresses thermal formation of the hcp phase in fcc steels2018

    • Author(s)
      Koyama Motomichi、Hirata Kenji、Abe Yuji、Mitsuda Akihiro、Iikubo Satoshi、Tsuzaki Kaneaki
    • Journal Title

      Scientific Reports

      Volume: 8 Pages: 16136

    • DOI

      https://doi.org/10.1038/s41598-018-34542-0

    • Peer Reviewed / Open Access
  • [Journal Article] First-Principles Study on Hydrogen Diffusivity in BCC, FCC, and HCP Iron2018

    • Author(s)
      Hirata K.、Iikubo S.、Koyama M.、Tsuzaki K.、Ohtani H.
    • Journal Title

      Metallurgical and Materials Transactions A

      Volume: 49 Pages: 5015~5022

    • DOI

      https://doi.org/10.1007/s11661-018-4815-9

    • Peer Reviewed
  • [Journal Article] Surface orientation dependence of hydrogen flux in lenticular martensite of an Fe-Ni-C alloy clarified through in situ silver decoration technique2018

    • Author(s)
      Koyama Motomichi、Yamasaki Daisuke、Tsuzaki Kaneaki
    • Journal Title

      Materials Letters

      Volume: 228 Pages: 273~276

    • DOI

      https://doi.org/10.1016/j.matlet.2018.06.022

    • Peer Reviewed
  • [Journal Article] Split and Shift of <i>ε</i>-martensite Peak in an X-ray Diffraction Profile during Hydrogen Desorption: A Geometric Effect of Atomic Sequence2018

    • Author(s)
      Koyama Motomichi、Abe Yuji、Tsuzaki Kaneaki
    • Journal Title

      ISIJ International

      Volume: 58 Pages: 1745~1747

    • DOI

      https://doi.org/10.2355/isijinternational.ISIJINT-2018-260

    • Peer Reviewed
  • [Journal Article] Non-propagating fatigue cracks in austenitic steels with a micro-notch: Effects of dynamic strain aging, martensitic transformation, and microstructural hardness heterogeneity2018

    • Author(s)
      Nishikura Yuri、Koyama Motomichi、Yamamura Yusuke、Ogawa Takuro、Tsuzaki Kaneaki、Noguchi Hiroshi
    • Journal Title

      International Journal of Fatigue

      Volume: 113 Pages: 359~366

    • DOI

      https://doi.org/10.1016/j.ijfatigue.2018.04.027

    • Peer Reviewed
  • [Journal Article] Microstructural mechanisms of fatigue crack non-propagation in TRIP-maraging steels2018

    • Author(s)
      Zhang Z.、Koyama M.、Wang M.M.、Tsuzaki K.、Tasan C.C.、Noguchi H.
    • Journal Title

      International Journal of Fatigue

      Volume: 113 Pages: 126~136

    • DOI

      https://doi.org/10.1016/j.ijfatigue.2018.04.013

    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Comparative study of hydrogen embrittlement in stable and metastable high-entropy alloys2018

    • Author(s)
      Ichii Kenshiro、Koyama Motomichi、Tasan Cemal Cem、Tsuzaki Kaneaki
    • Journal Title

      Scripta Materialia

      Volume: 150 Pages: 74~77

    • DOI

      https://doi.org/10.1016/j.scriptamat.2018.03.003

    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Temperature dependence of transgranular fatigue crack resistance in interstitial-free steel and Fe-C steels with supersaturated carbon: Effects of dynamic strain aging and dynamic precipitation2018

    • Author(s)
      Li Bochuan、Koyama Motomichi、Sakurada Eisaku、Yoshimura Nobuyuki、Ushioda Kohsaku、Noguchi Hiroshi
    • Journal Title

      International Journal of Fatigue

      Volume: 110 Pages: 1~9

    • DOI

      https://doi.org/10.1016/j.ijfatigue.2018.01.003

    • Peer Reviewed
  • [Journal Article] Fatigue Behavior of Fe-Cr-Ni-based Metastable Austenitic Steels with an Identical Tensile Strength and Different Solute Carbon Contents2018

    • Author(s)
      Ogawa Takuro、Koyama Motomichi、Nishikura Yuri、Tsuzaki Kaneaki、Noguchi Hiroshi
    • Journal Title

      ISIJ International

      Volume: 58 Pages: 1910~1919

    • DOI

      https://doi.org/10.2355/isijinternational.ISIJINT-2018-098

    • Peer Reviewed
  • [Journal Article] Fatigue Crack Growth Behavior and Associated Microstructure in a Metastable High-Entropy Alloy2018

    • Author(s)
      Eguchi Takeshi、Koyama Motomichi、Fukushima Yoshihiro、Tasan Cemal Cem、Tsuzaki Kaneaki
    • Journal Title

      Procedia Structural Integrity

      Volume: 13 Pages: 831~836

    • DOI

      https://doi.org/10.1016/j.prostr.2018.12.159

    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Strain Rate Sensitivity of Microstructural Damage Evolution in a Dual-Phase Steel Pre-Charged with Hydrogen2018

    • Author(s)
      Kumamoto Tsubasa、Koyama Motomichi、Tsuzaki Kaneaki
    • Journal Title

      Procedia Structural Integrity

      Volume: 13 Pages: 710~715

    • DOI

      https://doi.org/10.1016/j.prostr.2018.12.118

    • Peer Reviewed / Open Access
  • [Journal Article] Small fatigue crack growth in a high entropy alloy2018

    • Author(s)
      Suzuki Kai、Koyama Motomichi、Noguchi Hiroshi
    • Journal Title

      Procedia Structural Integrity

      Volume: 13 Pages: 1065~1070

    • DOI

      https://doi.org/10.1016/j.prostr.2018.12.224

    • Peer Reviewed / Open Access
  • [Journal Article] Proposal of fractographic analysis method coupled with EBSD and ECCI2018

    • Author(s)
      Kaida Taketo、Koyama Motomichi、Hamada Shigeru、Noguchi Hiroshi、Sakurada Eisaku、Yokoi Tatsuo、Ushioda Kohsaku
    • Journal Title

      Procedia Structural Integrity

      Volume: 13 Pages: 1076~1081

    • DOI

      https://doi.org/10.1016/j.prostr.2018.12.226

    • Peer Reviewed / Open Access
  • [Journal Article] Effect of Si on temperature dependence of non-propagation limit of small fatigue crack in a Fe-C alloy2018

    • Author(s)
      Kishida Kohei、Koyama Motomichi、Yoshimura Nobuyuki、Sakurada Eisaku、Yokoi Tatsuo、Ushioda Kohsaku、Tsuzaki Kaneaki、Noguchi Hiroshi
    • Journal Title

      Procedia Structural Integrity

      Volume: 13 Pages: 1032~1036

    • DOI

      https://doi.org/10.1016/j.prostr.2018.12.192

    • Peer Reviewed / Open Access
  • [Journal Article] Quantification method for parameters affecting multi-scale roughness-induced fatigue crack closure2018

    • Author(s)
      Mizoguchi Tomoki、Koyama Motomichi、Noguchi Hiroshi
    • Journal Title

      Procedia Structural Integrity

      Volume: 13 Pages: 1071~1075

    • DOI

      https://doi.org/10.1016/j.prostr.2018.12.225

    • Peer Reviewed / Open Access
  • [Journal Article] Proposal and verification of novel fatigue crack propagation simulation method by finite element method.2018

    • Author(s)
      Sano Temma、Sasaki Daisuke、Koyama Motomichi、Hamada Shigeru、Noguchi Hiroshi
    • Journal Title

      Procedia Structural Integrity

      Volume: 13 Pages: 1154~1158

    • DOI

      https://doi.org/10.1016/j.prostr.2018.12.240

    • Peer Reviewed / Open Access
  • [Journal Article] Localized Plasticity and Associated Cracking in Stable and Metastable High-Entropy Alloys Pre-Charged with Hydrogen2018

    • Author(s)
      Ichii Kenshiro、Koyama Motomichi、Tasan Cemal Cem、Tsuzaki Kaneaki
    • Journal Title

      Procedia Structural Integrity

      Volume: 13 Pages: 716~721

    • DOI

      https://doi.org/10.1016/j.prostr.2018.12.119

    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] A new design concept for prevention of hydrogen-induced mechanical degradation: viewpoints of metastability and high entropy2018

    • Author(s)
      Koyama Motomichi、Eguchi Takeshi、Ichii Kenshiro、Tasan Cemal Cem、Tsuzaki Kaneaki
    • Journal Title

      Procedia Structural Integrity

      Volume: 13 Pages: 292~297

    • DOI

      https://doi.org/10.1016/j.prostr.2018.12.049

    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Overview of Dynamic Strain Aging and Associated Phenomena in Fe?Mn?C Austenitic Steels2018

    • Author(s)
      Koyama Motomichi、Sawaguchi Takahiro、Tsuzaki Kaneaki
    • Journal Title

      ISIJ International

      Volume: 58 Pages: 1383~1395

    • DOI

      https://doi.org/10.2355/isijinternational.ISIJINT-2018-237

    • Peer Reviewed
  • [Presentation] "Microstructure evolution beneath fatigue fracture surface"2018

    • Author(s)
      M. Koyama, T. Eguchi, S. Mizumachi, C.C. Tasan, K. Tsuzaki
    • Organizer
      International Conference High-Entropy Materials (ICHEM)
    • Int'l Joint Research / Invited
  • [Presentation] “A new challenge to hydrogen-induced mechanical degradation in high strength steels”2018

    • Author(s)
      K. Tsuzaki
    • Organizer
      6th International Conference on Advanced Steels (ICAS)
    • Int'l Joint Research / Invited
  • [Presentation] “Metallurgical aspects of fatigue crack growth resistance in steels: How can we improve it through microstructure control?”2018

    • Author(s)
      K.Tsuzaki, M. Koyama, H.Noguchi.
    • Organizer
      18th International Conference on Strength of Materials (ICSMA18)
    • Int'l Joint Research / Invited
  • [Presentation] "A new concept for prevention of hydrogen-induced mechanical degradation: viewpoints of metastability and high entropy"2018

    • Author(s)
      M. Koyama
    • Organizer
      22nd European Conference on Fracture (ECF22)
    • Int'l Joint Research / Invited
  • [Presentation] 疲労変形解析に向けた引張荷重負荷除荷時のその場ECCI観察2018

    • Author(s)
      中藤敬一朗、小山元道、津崎兼彰
    • Organizer
      日本機械学会 M&M2018材料力学カンファレンス
  • [Presentation] FCC系高エントロピー合金における力学的に長い疲労き裂の進展特性2018

    • Author(s)
      水町俊介、小山元道、福島良博、津崎兼彰
    • Organizer
      日本機械学会 M&M2018材料力学カンファレンス
  • [Presentation] オーステナイト鋼の疲労限改善に高濃度炭素は必要か:ひずみ時効とひずみ集中2018

    • Author(s)
      小山元道
    • Organizer
      日本機械学会 M&M2018材料力学カンファレンス
  • [Presentation] Fe-Mn-Cフェライト鋼の疲労限度およびコーキシング効果:Mn-C対の作用に着目して2018

    • Author(s)
      内田悠翠、小山元道、福島良博、津崎兼彰
    • Organizer
      日本機械学会 M&M2018材料力学カンファレンス
  • [Presentation] EBSD/ECCIとデジタル画像相関法を併用した塑性ひずみ発達測定法の提案:fcc Ni切欠材の例2018

    • Author(s)
      柿本亮平、小山元道、津崎兼彰
    • Organizer
      日本機械学会 M&M2018材料力学カンファレンス
  • [Presentation] Fatigue Crack Growth Behavior and Associated Microstructure in a Metastable High-Entropy Alloy2018

    • Author(s)
      Takeshi Eguchi, Motomichi Koyama, Yoshihiro Fukushima, Cemal Cem Tasan and Kaneaki Tsuzaki
    • Organizer
      22nd European Conference on Fracture (ECF22)
    • Int'l Joint Research
  • [Presentation] Strain Rate Sensitivity of Microstructural Damage Evolution in a Dual-Phase Steel Pre-Charged with Hydrogen2018

    • Author(s)
      Tsubasa Kumamoto, Motomichi Koyama and Kaneaki Tsuzaki
    • Organizer
      22nd European Conference on Fracture (ECF22)
    • Int'l Joint Research
  • [Presentation] Effects of Si on temperature dependence of non-propagation limit of small fatigue crack in a Fe-C alloy2018

    • Author(s)
      Kohei Kishida, Kohei Kishida, Motomichi Koyama, Nobuyuki Yoshimura, Eisaku Sakurada, Tatsuo Yokoi, Kohsaku Ushioda, Kaneaki Tsuzaki, H. Noguchi
    • Organizer
      22nd European Conference on Fracture (ECF22)
    • Int'l Joint Research
  • [Presentation] Localized Plasticity and Associated Cracking in Stable and Metastable High-Entropy Alloys Pre-Charged with Hydrogen 3332018

    • Author(s)
      Kenshiro Ichii, Motomichi Koyama, Cemal Cem Tasan and Kaneaki Tsuzaki
    • Organizer
      22nd European Conference on Fracture (ECF22)
    • Int'l Joint Research
  • [Presentation] Plasticity-Driven Hydrogen Embrittlement in Stable and Metastable High Entropy Alloys2018

    • Author(s)
      Kenshiro Ichii, Motomichi Koyama, Cemal Cem Tasan, Kaneaki Tsuzaki
    • Organizer
      6th International Conference on Advanced Steels (ICAS)
    • Int'l Joint Research
  • [Presentation] ε-Martensite Plasticity Associated with Fatigue Crack Growth in a Metastable High-Entropy Alloy2018

    • Author(s)
      Takeshi Eguchi, Motomichi Koyama, Yoshihiro Fukushima, Cemal Cem Tasan, Kaneaki Tsuzaki
    • Organizer
      6th International Conference on Advanced Steels (ICAS)
    • Int'l Joint Research
  • [Presentation] Strain Rate Effects on Damage Tolerance in a Hydrogen-Charged Dual-Phase Steel :Crack Initiation, Arrest, and Growth to Failure2018

    • Author(s)
      Tsubasa Kumamoto, Motomichi Koyama, Kaneaki Tsuzaki
    • Organizer
      6th International Conference on Advanced Steels (ICAS)
    • Int'l Joint Research
  • [Remarks] 「鉄鋼材料において水素による異常な変態抑制効果を発見 -鉄の構造を水素で制御する」

    • URL

      http://www.kyushu-u.ac.jp/ja/university/publicity/pressrelease/latest/

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Published: 2019-12-27  

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