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2017 Fiscal Year Annual Research Report

Ultra-grain refinement as prevention against hydrogen-assisted crack propagation

Research Project

Project/Area Number 16K17981
Research InstitutionKyushu University

Principal Investigator

マカドレ アルノー  九州大学, カーボンニュートラル・エネルギー国際研究所, 学術研究員 (20635891)

Project Period (FY) 2016-04-01 – 2018-03-31
Keywordshydrogen embrittlement / austenite / grain refinement / steel
Outline of Annual Research Achievements

The metastable austenitic stainless steel was produced with six different grain sizes, from 1 micron to 21 microns. Hydrogen was introduced in the steel with different hydrogen gas pressures: 10, 40 and 100 MPa.
Tensile tests showed an overall decrease of the tensile strength for all grain sizes, the decrease of tensile strength occurred at the highest hydrogen content (100 MPa hydrogen gas) only for the smaller grains (1 micron). The 1 micron grains still maintained a tensile elongation of 30%.
In this metastable austenite, large hydrogen contents stabilize the austenitic phase. At low strains (true strain < 0.1), with the highest hydrogen content, there is no strain-induced martensite. This was explained with an increase of slip planarity, with less martensite nuclei being formed.

  • Research Products

    (4 results)

All 2017

All Journal Article (1 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 1 results) Presentation (3 results)

  • [Journal Article] Hydrogen-induced increase in phase stability in metastable austenite of various grain sizes under strain2017

    • Author(s)
      Macadre Arnaud、Tsuchiyama Toshihiro、Takaki Setsuo
    • Journal Title

      Journal of Materials Science

      Volume: 52 Pages: 3419~3428

    • Peer Reviewed / Int'l Joint Research
  • [Presentation] In-situ SEM/EBSD observation of hydrogen-assisted cracking of ultra-fine grained austenite2017

    • Author(s)
      A. Macadre, T. Tsuchiyama, S. Takaki
    • Organizer
      5th International Symposium on Steel Science (ISSS2017)
  • [Presentation] SEM/EBSD tensile testing of hydrogen-charged austenitic steel with ultra-fine grains2017

    • Author(s)
      A. Macadre, T. Tsuchiyama, S. Takaki
    • Organizer
      EUROMAT 2017
  • [Presentation] Comparison of fatigue crack tips with ultra-fine grains in metastable austenite and stable austenite2017

    • Author(s)
      A. Macadre, T. Tsuchiyama, S. Takaki
    • Organizer
      International Workshop on Giant Straining Process for Advanced Materials (GSAM2017)

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Published: 2018-12-17  

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