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2007 Fiscal Year Final Research Report Summary

The quantitative evaluation of effect of strain gradient on the strengthening and structure refinement of metals during ultra large straining

Research Project

Project/Area Number 18360329
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionToyohashi University of Technology

Principal Investigator

UMEMOTO Minoru  Toyohashi University of Technology, Dept.of Production Systems Engineering, Prof (90111921)

Co-Investigator(Kenkyū-buntansha) TSUCHIYA Koichi  National Institute for Materials Science, Structural Functions Research Group, Researcher (50236907)
TODAKA Yoshikazu  Toyohashi University of Technology, Dept.of Production Systems Engineering, Asst. Prof (50345956)
Project Period (FY) 2006 – 2007
Keywordsultra large strain / strain gradient / strengthening / grain refinement / high pressure torsion / crystallization / pressure induced transformation / GN dislocation
Research Abstract

In the present investigation, using specimens with different strain and strain gradient prepared by high pressure torsion machine, the effect of strain gradient on the strengthening and refinement of microstructure were studied. The measurement of hardness for HPTed pure metals such as Al, Ti, Ni, Cu, Fe revealed that recrystallization takes place in the pure metals with low melting point such as Al and Cu. Pressure induced transformation was observed in pure Ti. Thus using pure Fe in which only the effect of strain and strain gradient appears, the effect of strain and strain gradient on the hardness was studied. The clear strain gradient hardening was observed in the HPTed pure Fe. The HPTed Fe showed the ultimate tensile strength of 2GPa, and the total elongation increased with applied strain. The effect of high pressure during HPT was examined using pure Ti which transformed from phase to w phase when HPTed at high pressure. The volume fraction of CO phase increases with strain and with decreasing oxygen content. The co phase is metastable at ambient conditions and it transforms back to a phase during heating.

  • Research Products

    (49 results)

All 2008 2007 Other

All Journal Article (26 results) (of which Peer Reviewed: 13 results) Presentation (22 results) Remarks (1 results)

  • [Journal Article] Effect of strain path in high-pressure torsion process on hardening in commercial purity titanium,2008

    • Author(s)
      Y. Todaka, M. Umemoto, A. Yamazaki, J. Sasaki and K. Tsuchiya
    • Journal Title

      Materials Transactions 49,1

      Pages: 47-53

    • Description
      「研究成果報告書概要(和文)」より
    • Peer Reviewed
  • [Journal Article] Formation of surface nanocrystalline structure in steels by shot peening and role of strain gradient on grain refinement by deformation.2008

    • Author(s)
      Y. Todaka, M. Umemoto, Y. Watanabe, A. Yamazaki, W. Chaohui and K. Tsuchiya
    • Journal Title

      Materials Transactions 49,1

      Pages: 7-14

    • Description
      「研究成果報告書概要(和文)」より
    • Peer Reviewed
  • [Journal Article] Effect of strain path in high-pressure torsion process on hardening in commercial purity titanium2008

    • Author(s)
      Y. Todaka, M. Umemoto, A. Yamazaki, J. Sasaki, K. Tsuchiya
    • Journal Title

      Materials Transactions 49,1

      Pages: 47-53

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Formation of surface nanocrystalline structure in steels by shot peening and role of strain gradient on grain refinement by deformation2008

    • Author(s)
      Y. Todaka, M. Umemoto, Y. Watanabe, A. Yamazaki, W. Chaohui, K. Tsuchiya
    • Journal Title

      Materials Transactions 49, 1

      Pages: 7-14

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Formation of surface nanocrystalline structure in steels by shot peening and role of strain gradient on grain refinement by deformation.2007

    • Author(s)
      Y. Todaka, M. Umemoto, Y. Watanabe, A. Yamazaki, W. Chaohui and K. Tsuchiya
    • Journal Title

      ISIJ International 47,1

      Pages: 157-162

    • Description
      「研究成果報告書概要(和文)」より
    • Peer Reviewed
  • [Journal Article] Nanostructured Shape Memory Alloys for Biomedical Applications.2007

    • Author(s)
      K. Tsuchiya, Q. Cao, A. Hosokawa, M. Katahira, Y. Todaka and M. Umemoto
    • Journal Title

      Materials Science Forum 539-543

      Pages: 505-510

    • Description
      「研究成果報告書概要(和文)」より
    • Peer Reviewed
  • [Journal Article] Role of strain gradient and dynamic transformation on the formation of nanocrystalline structure produced by severe plastic deformation.2007

    • Author(s)
      M. Umemoto, Y. Todaka, J. Li and K. Tsuchiya
    • Journal Title

      Materials Science Forum 539-543

      Pages: 2787-2792

    • Description
      「研究成果報告書概要(和文)」より
    • Peer Reviewed
  • [Journal Article] Dissolution of cementite in carbon steels by ball drop deformation and laser heating.2007

    • Author(s)
      Yoshikazu Todaka, Minoru Umemoto, Akifumi Ohno, Mayumi Suzuki, Yuji Kawabata, Koichi Tsuchiya.
    • Journal Title

      Journal of Alloys and Compounds 434-435

      Pages: 497-500

    • Description
      「研究成果報告書概要(和文)」より
    • Peer Reviewed
  • [Journal Article] Role of strain gradient on the formation of nanocrystalline structure produced by severe plastic deformation.2007

    • Author(s)
      J. G. Li M. Umemoto, Y. Todaka, K. Tsuchiya.
    • Journal Title

      Journal of Alloys and Compounds 434-435

      Pages: 290-293

    • Description
      「研究成果報告書概要(和文)」より
    • Peer Reviewed
  • [Journal Article] A microstructural investigation of the surface of a drilled hole in carbon steels.2007

    • Author(s)
      J. G. Li M. Umemoto, Y. Todaka, K. Tsuchiya.
    • Journal Title

      Acta Materiaria 55

      Pages: 1397-1406

    • Description
      「研究成果報告書概要(和文)」より
    • Peer Reviewed
  • [Journal Article] Role of strain gradient on grain refinement by severe plastic deformation.2007

    • Author(s)
      Yoshikazu Todaka, Minoru Umemoto, Jun Yin, Zhiguang Liu and Koichi Tsuchiya.
    • Journal Title

      Materials Science and Engineering: A 462, 1-2, 25

      Pages: 264-268

    • Description
      「研究成果報告書概要(和文)」より
    • Peer Reviewed
  • [Journal Article] Properties of amorphous/nanocrystalline TiNi shape memory alloys produced by plastic deformation.2007

    • Author(s)
      K. Tsuchiya, M. Katahira, A. Hosokawa, Y. Todaka and M. Umemoto
    • Journal Title

      Proceedings of the 11th World Conference on Titanium(JIMIC5), The Japan Institute of Metals

      Pages: 483-486

    • Description
      「研究成果報告書概要(和文)」より
    • Peer Reviewed
  • [Journal Article] Influence of heat generation during HPT-straining on strengthening and grain refinement in commercial purity Ti.2007

    • Author(s)
      Y. Todaka, M. Umemoto, A. Yamazaki, J. Sasaki and K. Tsuchiya
    • Journal Title

      Proceedings of the 11th World Conference on Titanium(JIMIC5), The Japan Institute of Metals

      Pages: 207-210

    • Description
      「研究成果報告書概要(和文)」より
    • Peer Reviewed
  • [Journal Article] Formation of ultrafin grained structure in SUS 304 stainless steel produced by high pressure torsion(HPT).2007

    • Author(s)
      J. G. Li, M. Umemoto, Y. Todaka and K. Tsuchiya
    • Journal Title

      Materials Science Forum 561-565

      Pages: 847-852

    • Description
      「研究成果報告書概要(和文)」より
    • Peer Reviewed
  • [Journal Article] Formation of nanocrystalline structure in steels by severe plastic deformation.2007

    • Author(s)
      Y. Todaka, M. Umemoto, C. Wang and K. Tsuchiya
    • Journal Title

      General Abstract: Electronic, and Photonic Materials Division, TMS(The Minerals, Metals & Materials Society)

      Pages: 87-93

    • Description
      「研究成果報告書概要(和文)」より
    • Peer Reviewed
  • [Journal Article] Formation of surface nanocrystalline structure in steels by shot peening and role of strain gradient on grain refinement by deformation2007

    • Author(s)
      Y. Todaka, M. Umemoto, Y. Watanabe, A. Yamazaki, W. Chaohui, K. Tsuchiys
    • Journal Title

      ISIJ International 47, 1

      Pages: 157-162

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Nanostructured Shape Memory Alloys for Biomedical Applications2007

    • Author(s)
      K. Tsuchiya, Q. Cao, A. Hosokawa, M. Katahira, Y. Todaka, M. Umemoto
    • Journal Title

      Materials Science Forum 539-543

      Pages: 505-510

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Role of strain gradient and dynamic transformation on the formation of nanocrystalline structure produced by severe plastic deformation2007

    • Author(s)
      M. Umemoto, Y. Todaka, J. Li, K. Tsuchiya
    • Journal Title

      Materials Science Forum 539-543

      Pages: 2787-2792

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Dissolution of cementite in carbon steels by ball drop deformation and laser heating2007

    • Author(s)
      Yoshikazu, Todaka, Minoru, Umemoto, Akifumi, Ohno, Mayumi, Suzuki, Yuji, Kawabata, Koichi, Tsuchiya
    • Journal Title

      Journal of Alloys and Compounds 434-435

      Pages: 497-500

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Role of strain gradient on the formation of nanocrystalline structure produced by severe plastic deformation2007

    • Author(s)
      J G. Li, M. Umemoto, Y. Todaka, K. Tsuchiya
    • Journal Title

      Journal of Alloys and Compounds 434-435

      Pages: 290-293

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] A microstructural investigation of the surface of a drilled hole in carbon steels2007

    • Author(s)
      J G. Li, M. Umemoto, Y. Todaka, K. Tsuchiya
    • Journal Title

      Acta Materiaria 55

      Pages: 1397-1406

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Role of strain gradient on grain refinement by severe plastic deformation2007

    • Author(s)
      Yoshikazu, Todaka, Minoru, Umemoto, Jun, Yin, Zhiguang, Liu, Koichi, Tsuchiya
    • Journal Title

      Materials Science and Engineering 462,1-2,25

      Pages: 264-268

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Formation of ultrafin grained structure in SUS 304 stainless steel produced by high pressure torsion (HPT)2007

    • Author(s)
      J G.Li, M. Umemoto, Y. Todaka, K. Tsuchiya
    • Journal Title

      Materials Science Forum 561-565

      Pages: 847-852

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Properties of amorphous/nanocrystalline TiNi shape memory alloys produced by plastic deformation2007

    • Author(s)
      K. Tsuchiya, M. Katahira, A. Hosokawa, Y. Todaka, M. Umemoto
    • Journal Title

      Proceedings of the 11th World Conference on Titanium(JIMIC5), The Japan Institute of Metalr

      Pages: 483-486

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Influence of heat generation during HPT-straining on strengthening and grain refinement in commercial purity Ti2007

    • Author(s)
      Y. Todaka, M. Umemoto, A. Yamazaki, J. Sasaki, K. Tsuchiya
    • Journal Title

      Proceedings of the 11th World Conference on Titanium(JIMIC5), The Japan Institute of Metals

      Pages: 207-210

    • Description
      「研究成果報告書概要(欧文)」より
  • [Journal Article] Formation of nanocrystalline structure in steels by severe plastic deformation2007

    • Author(s)
      Y. Todaka, M. Umemoto, C. Wang, K. Tsuchiya
    • Journal Title

      General Abstract : Electronic, and Photonic Materials Division, TMS (The Minerals, Metals & Materials Society)

      Pages: 87-93

    • Description
      「研究成果報告書概要(欧文)」より
  • [Presentation] HPT 加工により作製したサブミクロン結晶粒バルク純Fe の組織と引張特性2008

    • Author(s)
      好井美樹
    • Organizer
      日本金属学会2008年春期大会(第142回)
    • Place of Presentation
      武蔵工業大学世田谷キャンパス
    • Year and Date
      2008-03-28
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] 強ひずみ加工により高強度・高延性化されたサブミクロン純Feの疲労特性2008

    • Author(s)
      永井宏典
    • Organizer
      日本鉄鋼協会2008年春季講演大会(第155回)
    • Place of Presentation
      武蔵工業大学世田谷キャンパス
    • Year and Date
      2008-03-27
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] HPT加工した純Tiにおけるω相の形成と力学特性2008

    • Author(s)
      本敬行
    • Organizer
      日本鉄鋼協会2008年春季講演大会(第155回)
    • Place of Presentation
      武蔵工業大学世田谷キャンパス
    • Year and Date
      2008-03-27
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] HPT加工したサブミクロン結晶粒純Feの組織と力学特性2008

    • Author(s)
      熊谷匡明
    • Organizer
      日本鉄鋼協会2008年春季講演大会(第155回)
    • Place of Presentation
      武蔵工業大学世田谷キャンパス
    • Year and Date
      2008-03-27
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] HPT 加工による ω 相から成るバルクサブミクロン結晶粒純 Ti の創製2008

    • Author(s)
      戸高義一
    • Organizer
      日本金属学会2008年春期大会(第142回)
    • Place of Presentation
      武蔵工業大学世田谷キャンパス
    • Year and Date
      2008-03-26
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] 強ひずみ加工により作製したサブミクロン結晶粒純 Cu の特異な再結晶挙動2008

    • Author(s)
      戸高義一
    • Organizer
      日本金属学会2008年春期大会(第142回)
    • Place of Presentation
      武蔵工業大学世田谷キャンパス
    • Year and Date
      2008-03-26
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] Formation of Ultrafine Grained Structure in SUS 304 Stainless Steel Produced by High Pressure Torsion(HPT)2007

    • Author(s)
      J. G. LiP, Minoru Umemoto, Y. Todaka and K. Tsuchiya
    • Organizer
      The Sixth Pacific Rim International Conference on Advanced Materials and Processing(PRICM6)
    • Place of Presentation
      Jeju, Korea
    • Year and Date
      20071105-09
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] Formation of Ultrafine Grained Structure in SUS 304 Stainless Steel Produced by High Pressure Torsion (HPT)2007

    • Author(s)
      J G. LiP, Minoru, Umemoto, Y. Todaka, K. Tsuchiya
    • Organizer
      The Sixth Pacific Rim International Conference on Advanced Materials and Processing(PRICM6)
    • Place of Presentation
      Jeju,Korea
    • Year and Date
      20071105-09
    • Description
      「研究成果報告書概要(欧文)」より
  • [Presentation] Strengthening and Grain Refinement in Steels by Severe Plastic Deformation2007

    • Author(s)
      Minoru Umemoto, Yoshikazu Todaka, Jinguo Li and Koichi Tsuchiya
    • Organizer
      International Symposium on Ultrafine Grained Steels(ISUGS2007)
    • Place of Presentation
      Kitakyushu, Japan
    • Year and Date
      20071024-26
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] Strengthening and Grain Refinement in Steels by Severe Plastic Deformation2007

    • Author(s)
      Minoru, Umemoto, Yoshikazu, Todaka, Jinguo, Li, Koichi, Tsuchiya
    • Organizer
      International Symposium on Ultrafme Grained Steels (ISUGS2007)
    • Place of Presentation
      Kitakyushu Japan
    • Year and Date
      20071024-26
    • Description
      「研究成果報告書概要(欧文)」より
  • [Presentation] Strengthening and Grain Refinement in Metals by Severe Plastic Deformation2007

    • Author(s)
      M. Umemoto, Y. Todaka, J. Sasaki and K. Tsuchiya
    • Organizer
      14th International Symposium on Metastable and Nano Materials(ISMANAM-2007)
    • Place of Presentation
      Corfu, Greece
    • Year and Date
      20070826-31
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] Strengthening and Grain Refinement in Metals by Severe Plastic Deformation2007

    • Author(s)
      M. Umemoto, Y. Todaka, J. Sasaki, K. Tsuchiya
    • Organizer
      14th International Symposium on Metastable and Nano Materials (ISMANAM-2007)
    • Place of Presentation
      Corfu Greece
    • Year and Date
      20070826-31
    • Description
      「研究成果報告書概要(欧文)」より
  • [Presentation] Phase transformation induced by severe plastic deformation in SUS 304 stainless steell2007

    • Author(s)
      Minoru Umemoto, J. G. Li, Y. Todaka, K. Fujisaku and K. Tsuchiya
    • Organizer
      The 1st International Symposium on Steel Science 2007(IS3-2007)
    • Place of Presentation
      Kyoto, Japan
    • Year and Date
      20070516-18
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] Phase transformation induced by severe plastic deformation in SUS 304 stainless steell2007

    • Author(s)
      Minoru, Umemoto, J G. Li, Y. Todaka, K. Fujisaku, K. Tsuchiya
    • Organizer
      The 1st International Symposium on Steel Science 2007 (IS3 -2007)
    • Place of Presentation
      Kyoto Japan
    • Year and Date
      20070516-18
    • Description
      「研究成果報告書概要(欧文)」より
  • [Presentation] Tensile property of ultrafine grained ferritic steel produced by HPT straining.2007

    • Author(s)
      戸高義一
    • Organizer
      日本鉄鋼協会2007年秋期(第154回)大会
    • Place of Presentation
      岐阜大学
    • Year and Date
      2007-09-20
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] 高速ドリル加工により作製した超微細結晶表層を有する鉄鋼材料の力学特性2007

    • Author(s)
      永井宏典
    • Organizer
      日本鉄鋼協会2007年秋期(第154回)大会
    • Place of Presentation
      岐阜大学
    • Year and Date
      2007-09-20
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] HPT加工した種々の炭素量をもつサブミクロン結晶粒炭素鋼の組織と力学特性2007

    • Author(s)
      熊谷匡明
    • Organizer
      日本鉄鋼協会2007年秋期(第154回)大会
    • Place of Presentation
      岐阜大学
    • Year and Date
      2007-09-20
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] HPT加工を施した純Cuの硬さと組織2007

    • Author(s)
      今井康裕
    • Organizer
      日本金属学会2007年秋期(第141回)大会
    • Place of Presentation
      岐阜大学
    • Year and Date
      2007-09-19
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] 純Tiにおける組織と硬さに及ぼすHPT加工条件の影響2007

    • Author(s)
      本 敬行
    • Organizer
      日本金属学会2007年秋期(第141回)大会
    • Place of Presentation
      岐阜大学
    • Year and Date
      2007-09-19
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] 巨大ひずみ形状不変 HPT 加工による各種金属材料の組織変化2007

    • Author(s)
      戸高義一
    • Organizer
      日本金属学会2007年秋期(第141回)大会
    • Place of Presentation
      岐阜大学
    • Year and Date
      2007-09-19
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] HPT 加工とその後の加熱による純 Ti の組織と力学特性の変化2007

    • Author(s)
      佐々木 洵
    • Organizer
      日本金属学会2007年秋期(第141回)大会
    • Place of Presentation
      岐阜大学
    • Year and Date
      2007-09-19
    • Description
      「研究成果報告書概要(和文)」より
  • [Presentation] HPT 加工したサブミクロン結晶粒バルク純 Fe の高強度・高延性2007

    • Author(s)
      好井美樹
    • Organizer
      日本金属学会2007年秋期(第141回)大会
    • Place of Presentation
      岐阜大学
    • Year and Date
      2007-09-19
    • Description
      「研究成果報告書概要(和文)」より
  • [Remarks] 「研究成果報告書概要(和文)」より

    • URL

      http://martens.pse.tut.ac.jp/research/index.html

URL: 

Published: 2010-02-04  

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