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2019 Fiscal Year Research-status Report

Characteristic evaluation and development of composite material by hybrid infiltration reaction method

Research Project

Project/Area Number 18K03839
Research InstitutionHiroshima University

Principal Investigator

崔 龍範  広島大学, 工学研究科, 助教 (00457269)

Co-Investigator(Kenkyū-buntansha) 佐々木 元  広島大学, 工学研究科, 教授 (30192595)
松木 一弘  広島大学, 工学研究科, 教授 (30253115)
Project Period (FY) 2018-04-01 – 2021-03-31
Keywords構造材料 / 高強度 / 金属間化合物 / 複合材料 / 複雑形状 / 大型製造 / 機械的特性
Outline of Annual Research Achievements

電気自動車やハイブリッドカーに使用される構造材料には軽量化、高強度及び耐摩耗性等が求められている。現在使用されている鉄系材料には限界がある。上の特性を満たすためには、高強度や耐摩耗性を有する複合材料の開発が必要となり、本研究ではニッケル多孔体とアルミとの反応により生成される粒子状金属間化合物複合材料の複雑形状及び大型製造を目指し、社会的なニーズに合わせた「ものつくり」を実現させることを目的としている。
ニッケル多孔体とアルミとの反応性により生成される粒子状金属間化合物複合材料の複雑形状及び大型化の製造プロセスを構築するために、ハイブリット含浸反応法用いて大型サイズ及び一部分適用の作製を試みた。
圧力及び温度などのプロセスの改善による作製された複合材料の組織観察及び機械的特性、熱的特性を評価した。また、ハイブリット含浸反応法により、大型サイズ及び金属の表面のみ(厚さ、10mm未満)複合材料が含まれる材料の開発に成功した。また、機械的特性評価として、硬度試験を、熱的特性としては、熱伝導率と線熱膨張係数の測定を行った。

Current Status of Research Progress
Current Status of Research Progress

2: Research has progressed on the whole more than it was originally planned.

Reason

金属間化合物粒子分散複合材料を新たな製造する申請者の特許(特許第5988667号, 金属間化合物強化複合材料及びその製造方法)を用い、データベースを構築済みである。
更に、大型サイズ及び複雑形状の新たな金属多孔体(w:150mm×t: 150mm×h:10mm、outer dia.:150mm & inter dia. 100mm×t: 150mm×h:10mm)を用い、ハイブリット含浸反応法による複合材料の大型化及び複雑形状を有する複合材料の作製も進んでいる。

Strategy for Future Research Activity

作製された大型及び複雑形状の複合材料を、SEMとFE-SEMを用い微細組織を観察を行い、
材料内部の欠陥、分散率、面積率などの測定を行う。
機械的特性評価としては、摩耗特性評価及び線熱膨張係数などをデータを取得していく。

  • Research Products

    (28 results)

All 2020 2019

All Journal Article (5 results) (of which Int'l Joint Research: 5 results,  Peer Reviewed: 5 results,  Open Access: 3 results) Presentation (21 results) (of which Int'l Joint Research: 21 results,  Invited: 1 results) Patent(Industrial Property Rights) (2 results)

  • [Journal Article] Spark Sintering of TiB2 Reinforced Fe Matrix Composites with Both High Thermal Conductivity and Hardness, and Their Microstructural Characterizations2020

    • Author(s)
      Ke Yujiao, Matsugi Kazuhiro, Xu Zhefeng, Choi Yongbum, Wang Mingzhi, Yu Jinku
    • Journal Title

      Materials Transactions

      Volume: 61 Pages: 548-556

    • DOI

      10.2320/matertrans.MT-M2019286

    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Synthesis of 30 vol%TiB2 Containing Fe5Ti Matrix Composites with High Thermal Conductivity and Hardness2019

    • Author(s)
      Yujiao Ke, Kazuhiro Matsugi, Zhefeng Xu, Yu He, Yongbum Choi, Mingzhi Wang and Jinku Yu
    • Journal Title

      Materials Transactions

      Volume: 60 Pages: 2516-2524

    • DOI

      doi:10.2320/matertrans.MT-M2019168

    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Development Of Short Carbon Fiber Reinforced Aluminium Matrix Composites By Low Pressure Infiltration Process2019

    • Author(s)
      Xuan Meng, Yongbum Choi, Kazuhiro Matsugi, Wentao Hu and Wenchang Liu
    • Journal Title

      Materials Science and Engineering

      Volume: 547 Pages: 1-6

    • DOI

      https://iopscience.iop.org/article/10.1088/1757-899X/547/1/012024

    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Fabrication of Cr based electrodeposited composite film using nano ZrO2 particles on aluminum substrate2019

    • Author(s)
      Kota SATO, Kenjiro SUGIO, Yongbum CHOI, Gen SASAKI, Asep Ridwan SETIAWAN and Aditianto RAMELAN
    • Journal Title

      Materials Science and Engineering

      Volume: 547 Pages: 1-8

    • DOI

      https://iopscience.iop.org/article/10.1088/1757-899X/547/1/0120271

    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Applicability of As-Cast on beta-type Titanium Alloys Proposed in the Compositional Region with Different Tensile Deformation Types2019

    • Author(s)
      Xi-Long Ma, Kazuhiro Matsugi, Zhe-Feng Xu, Yong-Bum Choi, Ryohei Matsuzaki, Jie Hu, Xin-Gang Liu and Hao Huang
    • Journal Title

      Materials Transactions

      Volume: 60 Pages: 2426-2434

    • DOI

      https://doi.org/10.2320/matertrans.F-M2019848

    • Peer Reviewed / Int'l Joint Research
  • [Presentation] Development Of High Strength And High Thermal Conductivity Mold Material With Hetero Structure2019

    • Author(s)
      Hitoshi SAWADA, Kenjiro SUGIO, Yongbum CHOI, Gen SASAKI
    • Organizer
      The 12th Korea-Japan Joint Symposium on Composite Materials
    • Int'l Joint Research
  • [Presentation] Both Effects Of Powder Mixing And Spark Sintering For 30vol%TiB2 Strengthened Steels With Ti Macro-Alloying MMCs2019

    • Author(s)
      Yujiao KE, Kazuhiro MATSUGI, Yongbum CHOI
    • Organizer
      The 12th Korea-Japan Joint Symposium on Composite Materials
    • Int'l Joint Research
  • [Presentation] Effect Of Surface Structure Of Carbon Materials On Reactivity For Iron2019

    • Author(s)
      Shunsuke FUJII, Kenjiro SUGIO, Yongbum CHOI, Gen SASAKI
    • Organizer
      The 12th Korea-Japan Joint Symposium on Composite Materials
    • Int'l Joint Research
  • [Presentation] Relationship Between Effective Thermal Conductivity And Interfacial Thermal Resistance Of Al-AlN And Al-Si Composites2019

    • Author(s)
      Takuya KAWATA, Kenjiro SUGIO, Yongbum CHOI, Gen SASAKI
    • Organizer
      The 12th Korea-Japan Joint Symposium on Composite Materials
    • Int'l Joint Research
  • [Presentation] Effect Of Matrix On Characteristics For Multipurpose Of Carbon Short Fiber Reinforced Composite2019

    • Author(s)
      Xuan MENG, Yongbum CHOI, Kazuhiro MATSUGI
    • Organizer
      The 12th Korea-Japan Joint Symposium on Composite Materials
    • Int'l Joint Research
  • [Presentation] Preparation Of Almina Short Fiber Dispersed Aluminum Alloy Composites With Functional Gradient Structure2019

    • Author(s)
      Shinji WATANABE, Kenjiro SUGIO, Yongbum CHOI, Gen SASAKI
    • Organizer
      The 12th Korea-Japan Joint Symposium on Composite Materials
    • Int'l Joint Research
  • [Presentation] Characteristics Of The Carbon Nanofibre Dispersed Copper Composites Prepared By Spark Plasma Sintering2019

    • Author(s)
      Koyo FUJIMURA, Kenjiro SUGIO, Gen SASAKI, Yongbum CHOI
    • Organizer
      The 12th Korea-Japan Joint Symposium on Composite Materials
    • Int'l Joint Research
  • [Presentation] Development Of Manufacturing Process Of Porous AlN Reinforced Fe Matrix Composite2019

    • Author(s)
      Yusuke SETO, Yongbum CHOI, Kazuhiro MATSUGI, Kenjiro SUGIO
    • Organizer
      The 12th Korea-Japan Joint Symposium on Composite Materials
    • Int'l Joint Research
  • [Presentation] Manufacturing Process Of Graphene Reinforced Metal Matrix Composite With High Volume Rate Of Graphene2019

    • Author(s)
      Yosuke DOBASHI, YongBum CHOI, Kazuhiro MATSUGI, Gen SASAKI
    • Organizer
      The 12th Korea-Japan Joint Symposium on Composite Materials
    • Int'l Joint Research
  • [Presentation] New Manufacturing Process of Al3Ni Ceramic Particles Reinforced Composite2019

    • Author(s)
      Yongbum CHOI , Kazuhiro MATSUGI
    • Organizer
      The 36th International Japan-Korea Seminar on Ceramics
    • Int'l Joint Research / Invited
  • [Presentation] Fabrication and Characterization of Porous Material Using CNTs Block for Fabrication of Matrix Composites Materials2019

    • Author(s)
      Fei Gao, Yongbum Choi, Kazuhiro Matsugi, Kenjiro Sugio, Hiroyuki Suzuki
    • Organizer
      The 10th International Conference on Adanvanced Materials and Processing
    • Int'l Joint Research
  • [Presentation] The Fabrication of (Fe-10Ti)-TiB2 Composites with Both High Thermal Conductivity and Hardness by SPS2019

    • Author(s)
      Yujiao Ke, Kazuhiro Matsugi, Zhefeng Xu, Yu He, Yongbum Choi,Mingzhi Wang, Jinku Yu
    • Organizer
      The 10th International Conference on Adanvanced Materials and Processing
    • Int'l Joint Research
  • [Presentation] Characterizations of the Microstructural and Tensile Properties of Al-9Si-0.3Fe-0.15Mn Alloys with Ti and V Additions2019

    • Author(s)
      Zeze Xiao, Kazuhiro Matsugi, Zhefeng Xu, Taishi Matsuoka, Tomoshi Uomi,Nobuyuki Oda, Hironobu Kominato, and Yasuo Uosaki
    • Organizer
      The 10th International Conference on Adanvanced Materials and Processing
    • Int'l Joint Research
  • [Presentation] Optimization of Both Composition and Manufacturing Process for α-Type Titanium Alloys and Their Characterizations2019

    • Author(s)
      Xilong Ma, Kazuhiro Matsugi, Zhefeng Xu, Yongbum Choi, Ye Liu, Jie Hu, Xingang Liu, Hao Huang
    • Organizer
      The 10th International Conference on Adanvanced Materials and Processing
    • Int'l Joint Research
  • [Presentation] The Relationship Between the Effective Thermal Conductivity and the Orientation of Graphite Flakes in Al Matrix Composites2019

    • Author(s)
      Yan Zhao, Kenjiro Sugio, Yongbum Choi, Sasaki Gen, Zhefeng Xu, Jinku Yu
    • Organizer
      The 10th International Conference on Adanvanced Materials and Processing
    • Int'l Joint Research
  • [Presentation] Manufacturing process of graphene reinforced Al composite and their properties2019

    • Author(s)
      Y.B. Choi, Y. Dobashi K. Matsugi, G. Sasaki, K. Sugio
    • Organizer
      22nd International Conference on Composite Materials
    • Int'l Joint Research
  • [Presentation] Simulation of thermal conductivity for titanium boride particle dispersed aluminum composites2019

    • Author(s)
      Gen Sasaki, K. Kodama, Y. B. Choi, K. Sugio
    • Organizer
      22nd International Conference on Composite Materials
    • Int'l Joint Research
  • [Presentation] Evaluation of interfacial thermal resistance of Al-AlN particle dispersed composites by using image based calculation2019

    • Author(s)
      Kenjiro Sugio, T. Kawata, Y. B. Choi, G. Sasaki
    • Organizer
      22nd International Conference on Composite Materials
    • Int'l Joint Research
  • [Presentation] In-site synthesis of Al Matrix Composite Reinforce with Dispersed Al3Ni Using Porous Nickel2019

    • Author(s)
      Yongbum Choi, Kazuhiro Matsugi, Gen Sasaki, Kenjiro Sugio
    • Organizer
      International Sympoisum on PRecision Engineering and Sustainable Manufacturing
    • Int'l Joint Research
  • [Presentation] Characterization of Short Carbon Fiber Dispersed Flame-Resistant Magnesium Alloy Composites for Practical Use2019

    • Author(s)
      Gen Sasaki, Kentaro Tashiro, Yongbum Choi, Kazuhiro Matsugi, Kenjiro Sugio
    • Organizer
      International Sympoisum on PRecision Engineering and Sustainable Manufacturing
    • Int'l Joint Research
  • [Presentation] Development of a Software to Quantify the Microstructures of Metals and Metal Matrix Composites2019

    • Author(s)
      Kenjiro Sugio, Yongbum Cho, Gen Sasaki
    • Organizer
      International Sympoisum on PRecision Engineering and Sustainable Manufacturing
    • Int'l Joint Research
  • [Patent(Industrial Property Rights)] 予備成形体を要しない炭素繊維強化金属基複合材料の製造プロセスの開発2019

    • Inventor(s)
      崔龍範
    • Industrial Property Rights Holder
      崔龍範
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2019-115782
  • [Patent(Industrial Property Rights)] チタン基複合材料の製造方法2019

    • Inventor(s)
      崔龍範
    • Industrial Property Rights Holder
      崔龍範
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2019-130578

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Published: 2021-01-27  

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