• Search Research Projects
  • Search Researchers
  • How to Use
  1. Back to project page

2010 Fiscal Year Final Research Report

Simultaneous correction of spherical and chromatic aberrations by dynamic hollow-cone illumination

Research Project

  • PDF
Project/Area Number 20246015
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Thin film/Surface and interfacial physical properties
Research InstitutionOsaka University

Principal Investigator

TAKAI Yoshizo  大阪大学, 工学研究科, 教授 (30236179)

Co-Investigator(Kenkyū-buntansha) KIMURA Yoshihide  大阪大学, 工学研究科, 准教授 (70221215)
NAGATOMI Takaharu  大阪大学, 工学研究科, 助教 (90314369)
Project Period (FY) 2008 – 2010
Keywords高分解能電子顕微鏡 / 動的ホローコーン照明 / 球面収差補正 / 色収差補正 / 色消し結像条件 / 波動場再構成 / 位相・振幅分離再生
Research Abstract

A novel wave field restoration method under dynamic hollow-cone illumination is demonstrated using a series of 64 azimuthally rotated images in transmission electron microscopy(TEM). The restoration of the exit wave field was performed by utilizing spherical and chromatic aberration-free Fourier components. The images obtained by inverse Fourier transform of the integrated Fourier spectrum for the azimuthally rotated images clearly showed successful separation of real and imaginary components of the exit wave and resolution enhancement beyond the information limit under axial illumination. Another way to achieve higher spatial resolution was also proposed using the three-dimensional Fourier filtering method applied to tilted illumination. In the approach, the degradation of image contrast caused by chromatic aberration was reduced and the image distortion caused by spherical aberration, coma aberration and three-fold astigmatism was corrected, resulting in the achievement of 1. 4 times higher resolution beyond the information limit under axial illumination.

  • Research Products

    (37 results)

All 2011 2010 2009 2008 Other

All Journal Article (15 results) (of which Peer Reviewed: 6 results) Presentation (20 results) Remarks (1 results) Patent(Industrial Property Rights) (1 results)

  • [Journal Article] In-situ Crystal Structure Analysis of Cobalt Nanocompounds Synthesizing Graphite at High Temperatures2011

    • Author(s)
      T. Yahiro and Y. Takai
    • Journal Title

      Jpn. J. Appl. Phys

      Volume: 50(1) Pages: 15103-1-5

    • Peer Reviewed
  • [Journal Article] Study on Molybdenum Oxide Encapsulated inside Carbon Nanotubes Using Transmission Electron Microscope2010

    • Author(s)
      R. Sagawa, W. Togashi, T. Akita and, Y. Takai
    • Journal Title

      Proceedings of IMC17(International Microscopy Congress)

      Volume: 1巻 Pages: M7. 21

    • Peer Reviewed
  • [Journal Article] TEM observation of surface atomic structure of cobalt nanocatalysts producing graphite2010

    • Author(s)
      T. Yahiro and Y. Takai
    • Journal Title

      Proceedings of IMC17(InternationalMicroscopy Congress)

      Volume: 1巻 Pages: M2. 29

    • Peer Reviewed
  • [Journal Article] Resolution Improvement Achieved by Three-Dimensional Fourier Filtering Method Applied to Tilted Illumination in TEM2010

    • Author(s)
      F. Nakatani, K. Kitade and Y. Takai
    • Journal Title

      Proceedings of IMC17(International Microscopy Congress)

      Volume: 1巻 Pages: 12. 27

    • Peer Reviewed
  • [Journal Article] In-situ TEM Observation of Graphite Formation using Cobalt Oxide Nanocrystals2009

    • Author(s)
      T. Yahiro and Y. Takai
    • Journal Title

      7th International Symposium on Atomic Level Characterizations for New Materials and Devices' 09(ALC' 09)

      Volume: 1巻 Pages: 331-332

  • [Journal Article] Three-Dimensional Fourier Filtering Method to Tilted Illumination2009

    • Author(s)
      F. Nakatani, K. Kitade and Y. Takai
    • Journal Title

      7th International Symposium on Atomic Level Characterizations for New Materials and Devices' 09(ALC' 09)

      Volume: 1巻 Pages: 241-242

  • [Journal Article] Development of Computer Assisted Imaging System for TEM with Direct Electron Detection Type CCD Camera2009

    • Author(s)
      H. Kizawa, W. Togashi, M. Hayashida, Y. Kimura and Y. Takai
    • Journal Title

      7th International Symposium on Atomic Level Characterizations for New Materials and Devices' 09(ALC' 09)

      Volume: 1巻 Pages: 239-240

  • [Journal Article] In-situ TEM Observation of Graphite Formation Using Cobalt Oxide Nanocrystals2008

    • Author(s)
      T. Yahiro and Y. Takai
    • Journal Title

      The 9th Asia-Pacific Microscopy Conference(APMC9)

      Volume: 1巻 Pages: 206-207

  • [Journal Article] Aberration-Free STEM Imaging System Incorporating Parallel Detection and Processing Techniques Using a Multidetector Array2008

    • Author(s)
      Y. Takai, M. Taya, Y. Kimura, and T. Ikuta
    • Journal Title

      The 9th Asia-Pacific Microscopy Conference(APMC9)

      Volume: 1巻 Pages: 37-38

  • [Journal Article] Aberration-Free Imaging by Dynamic Hollow-cone Illumination in Transmission Electron Microscopy2008

    • Author(s)
      K. Kitade, H. Yoshimori, T. Ikuta, Y. Kimura, and Y. Takai
    • Journal Title

      The 9th Asia-Pacific Microscopy Conference(APMC9)

      Volume: 1巻 Pages: 35-36

  • [Journal Article] Wave Field Reconstruction under Critial Low Electron Dose Conditions : Comparison of SWFM and 3D-FFM2008

    • Author(s)
      Y. Takai, T. Nomaguchi, and Y. Kimura
    • Journal Title

      The 9th Asia-Pacific Microscopy Conference(APMC9)

      Volume: 1巻 Pages: 146-147

  • [Journal Article] Dynamic TEM Observation of Graphite Formation using Transition Metal Oxide Nanocatalysts2008

    • Author(s)
      Y. Takai, T. Yahiro, and T. Kida
    • Journal Title

      The 9th Asia-Pacific Microscopy Conference(APMC9)

      Volume: 1巻 Pages: 191-192

  • [Journal Article] Visulalization of Nanoscaled Organic Multilayer by Low-Voltage STEM2008

    • Author(s)
      T. Ueda, A. Makino, and Y. Takai
    • Journal Title

      The 9th Asia-Pacific Microscopy Conference(APMC9)

      Volume: 1巻 Pages: 736-737

  • [Journal Article] 焦点位置変調電子顕微鏡による収差補正技術の開発とその応用2008

    • Author(s)
      高井義造、木村吉秀
    • Journal Title

      J. Vac. Soc. Jpn

      Volume: 51(11) Pages: 707-713

    • Peer Reviewed
  • [Journal Article] Measurement of Precision for Developing Automatic Transmission Electron Microscope2008

    • Author(s)
      M. Hayashida, Y. Kimura, Y. Takai
    • Journal Title

      Surf. Interface Anal

      Volume: 40(13) Pages: 1777-1780

    • Peer Reviewed
  • [Presentation] 電子顕微鏡像の位相コントラストとその回復2011

    • Author(s)
      高井義造
    • Organizer
      日本顕微鏡学会、超分解能電子顕微鏡分科会
    • Place of Presentation
      東京都中央区
    • Year and Date
      2011-02-25
  • [Presentation] 高分解能電子顕微鏡の現状と今後2010

    • Author(s)
      高井義造
    • Organizer
      第54回日本顕微鏡学会シンポジウム
    • Place of Presentation
      石川県金沢市
    • Year and Date
      20101111-12
  • [Presentation] 傾斜照明下における3次元フーリエフィルタリング法の収差補正機能拡張2010

    • Author(s)
      中谷文弥, 北出晃平, 高井義造
    • Organizer
      第71回応用物理学会学術講演会
    • Place of Presentation
      長崎市
    • Year and Date
      20100914-17
  • [Presentation] 透過型電子顕微鏡による酸化モリブデン内包カーボンナノチューブに関する研究2010

    • Author(s)
      佐川隆亮, 富樫渉, 秋田知樹, 高井義造
    • Organizer
      第71回応用物理学会学術講演会
    • Place of Presentation
      長崎市
    • Year and Date
      20100914-17
  • [Presentation] グラファイト生成過程の高温その場TEM観察2010

    • Author(s)
      八尋孝典, 高井義造
    • Organizer
      第71回応用物理学会学術講演会
    • Place of Presentation
      長崎市
    • Year and Date
      20100914-17
  • [Presentation] 波面再構成法を用いたコバルト触媒微粒子のグラファイト生成海面観察2010

    • Author(s)
      八尋孝典、高井義造
    • Organizer
      日本顕微鏡学会第66回学術講演会
    • Place of Presentation
      名古屋市
    • Year and Date
      20100523-26
  • [Presentation] 傾斜照明下における3次元フーリエフィルタリング法の収差補正機能拡張2010

    • Author(s)
      中谷文弥、北出晃平、高井義造
    • Organizer
      日本顕微鏡学会第66回学術講演会
    • Place of Presentation
      名古屋市
    • Year and Date
      20100523-26
  • [Presentation] 3次元フーリエフィルタリング法の傾斜照明下への適用2009

    • Author(s)
      中谷文弥, 北出晃平, 高井義造
    • Organizer
      第70回応用物理学会学術講演会
    • Place of Presentation
      富山大学
    • Year and Date
      20090908-11
  • [Presentation] 透過型電子顕微鏡における動的ホローコーン照明の高精度化2009

    • Author(s)
      北出晃平, 生田孝, 木村吉秀, 高井義造
    • Organizer
      第70回応用物理学会学術講演会
    • Place of Presentation
      富山大学
    • Year and Date
      20090908-11
  • [Presentation] 酸化コバルト微粒子を用いたグラファイト生成過程のその場TEM観察II2009

    • Author(s)
      八尋孝典、高井義造
    • Organizer
      第70回応用物理学会学術講演会
    • Place of Presentation
      富山大学
    • Year and Date
      20090908-11
  • [Presentation] 酸化コバルト微粒子を用いたグラファイト生成過程のその場TEM観察22009

    • Author(s)
      八尋孝典, 高井義造
    • Organizer
      日本顕微鏡学会第65回学術講演会
    • Place of Presentation
      仙台市
    • Year and Date
      20090526-29
  • [Presentation] 3次元フーリエフィルタリング法の傾斜照明下への適用2009

    • Author(s)
      中谷文弥, 北出晃平, 高井義造
    • Organizer
      日本顕微鏡学会第65回学術講演会
    • Place of Presentation
      仙台市
    • Year and Date
      20090526-29
  • [Presentation] 動的ホローコーン照明による無収差結像2008

    • Author(s)
      高井義造
    • Organizer
      日本顕微鏡学会第52回シンポジウム
    • Place of Presentation
      千葉
    • Year and Date
      20081017-18
  • [Presentation] 収差補正TEM位相像による金/酸化チタン界面構造の解析2008

    • Author(s)
      川崎忠寛, 高井義造
    • Organizer
      日本顕微鏡学会日本顕微鏡学会第64回学術講演会
    • Place of Presentation
      京都市
    • Year and Date
      20080521-23
  • [Presentation] 走査型透過電子顕微鏡における輪帯照明システムの開発2008

    • Author(s)
      松谷貴臣, 田屋昌樹, 生田孝, 田中武雄, 木村吉秀, 高井義造, 川崎忠寛
    • Organizer
      日本顕微鏡学会第64回学術講演会
    • Place of Presentation
      京都市
    • Year and Date
      20080521-23
  • [Presentation] 輪帯対物絞りを用いた傾斜照明TEM像の無収差成分の抽出2008

    • Author(s)
      北出晃平, 吉森宏雅, 生田孝, 田中武雄, 高井義造
    • Organizer
      日本顕微鏡学会第64回学術講演会
    • Place of Presentation
      京都市
    • Year and Date
      20080521-23
  • [Presentation] 酸化コバルト微粒子を用いたグラファイト生成過程のその場TEM観察2008

    • Author(s)
      八尋孝典, 高井義造
    • Organizer
      日本顕微鏡学会第64回学術講演会
    • Place of Presentation
      京都市
    • Year and Date
      20080521-23
  • [Presentation] 3次元フーリエフィルタリング法とSchiske' s Wiener filtering法の比較2008

    • Author(s)
      野間口恒典, 高井義造
    • Organizer
      日本顕微鏡学会第64回学術講演会
    • Place of Presentation
      京都市
    • Year and Date
      20080521-23
  • [Presentation] 電子顕微鏡自動化におけるコンデンサーレンズのヒステリシス対策2008

    • Author(s)
      林田美咲, 木村吉秀
    • Organizer
      日本顕微鏡学会第64回学術講演会
    • Place of Presentation
      京都市
    • Year and Date
      20080521-23
  • [Presentation] 動的ホローコーン照明を用いた無収差結像2008

    • Author(s)
      高井義造, 吉森宏雅, 北出昇平, 木村吉秀
    • Organizer
      日本顕微鏡学会第64回学術講演会
    • Place of Presentation
      京都市
    • Year and Date
      20080521-23
  • [Remarks]

    • URL

      http://www-atom.mls.eng.osaka-u.ac.jp/jp/index.html

  • [Patent(Industrial Property Rights)] 遷移金属酸化物内包カーホ"ンナノチューフ"及びその製造方法2010

    • Inventor(s)
      高井義造
    • Industrial Property Rights Holder
      高井義造
    • Industrial Property Number
      特許、特願2010-124074
    • Filing Date
      2010-04-13

URL: 

Published: 2013-07-31  

Information User Guide FAQ News Terms of Use Attribution of KAKENHI

Powered by NII kakenhi