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2010 Fiscal Year Final Research Report

Study on how to extract nano fiber clusters from bamboo and their application

Research Project

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Project/Area Number 20360058
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionDoshisha University

Principal Investigator

FUJII Toru  Doshisha University, 理工学部, 教授 (20156821)

Co-Investigator(Kenkyū-buntansha) OKUBO Kazuya  同志社大学, 理工学部, 教授 (60319465)
Project Period (FY) 2008 – 2010
Keywordsナノコンポジット / 竹繊維 / 複合材料 / セルロースミクロフィブリル / ナノファイバークラスター
Research Abstract

Nano fibers called MFC (Micro-Fibrillated Cellulose) were extracted from raw bamboo as well as other plant pulps. When they are mechanically extracted, MFC forms NFC (Nano Fiber Cluster). First, PLA was reinforced with fibrillated bamboo mono-filaments/BNFC. PLA is brittle and less temperature resistance. With an increase of mechanical process for extracting, NFC becomes complicated. The degree of cluster, α was well quantitatively determined by water absorption since the surface of nano fiber cellulose being hydrophilic increased with an increase of fibrillating process. When BNFC was mixed with PLA to form compounds for improving its toughness, strength and thermal resistance, α=3.5 was suitable. Light curing epoxy was well modified in its ductility by adding a small amount of NFC. NFC was hydrophilic, and solvent replacement method such as ethanol was developed. The fracture toughness of light curing epoxy significantly increased due to a small amount of NFC, 0.5~1% dispersion. Finally, epoxy matrix of carbon fiber composites was modified with NFC up to 1% and their high cycle fatigue strength was examined under tension-tension loading. The significant extension of fatigue life was obtained when 0.3wt% NFC was mixed into epoxy resin, where the ethanol replacement method was also applied.

  • Research Products

    (15 results)

All 2011 2010 2009 2008 Other

All Journal Article (5 results) (of which Peer Reviewed: 5 results) Presentation (5 results) Remarks (1 results) Patent(Industrial Property Rights) (4 results)

  • [Journal Article] Interfacial adhesion improvement of plain woven carbon fiber reinforced epoxy filled with micro-fibrillated cellulose by addition liquid rubber2010

    • Author(s)
      Mohamed H.GABR, Mostafa ABDELRAHMAN, 大窪和也, 藤井透
    • Journal Title

      Journal of Materials Science Vol 45

      Pages: 3841-3850

    • Peer Reviewed
  • [Journal Article] Effect of microfibrillated cellulose onmechanical properties of plain woven CFRP reinforced epoxy2010

    • Author(s)
      Mohamed H.GABR, Mostafa ABDELRAHMAN, Kazuya OKUBO, Toru FUJII
    • Journal Title

      Composite Structures Vol 92

      Pages: 1999-2006

    • Peer Reviewed
  • [Journal Article] A Study on mechanical properties of bacterial cellulose/epoxy reinforced by plain woven carbon fiber modified with liquid rubber2010

    • Author(s)
      Mohamed H.GABR, Mostafa ABDELRAHMAN, Kazuya OKUBO, Toru FUJII
    • Journal Title

      COMPOSITE A Vol.41,1

      Pages: 1263-1271

    • Peer Reviewed
  • [Journal Article] 摩砕した竹繊維のフィブリル化度の最適化によるPLA複合材料の機械的特性の改善2009

    • Author(s)
      田中千晶,大窪和也,藤井透
    • Journal Title

      材料 Vol.58, No.15

      Pages: 368-373

    • Peer Reviewed
  • [Journal Article] Improvement of fatigue strength and impact properties of plain-woven CFRP modified with Micro Fibrillated cellulose2008

    • Author(s)
      Norifumi Takagaki, Kazuya OKUBO, Toru FUJII
    • Journal Title

      Advanced Material Research Vols.47-50

      Pages: 133-136

    • Peer Reviewed
  • [Presentation] Can Bio-nano-fibers (MFC) Extend The Fatigue Life of Carbon Fiber/epoxy Composites?2011

    • Author(s)
      Toru FUJII
    • Organizer
      Changwon National Univ., The 5th International Symposium on Advanced Mechatronics Engineering
    • Place of Presentation
      Changwon National Univ., Korea
    • Year and Date
      2011-01-06
  • [Presentation] An Application of Bamboo Fiber in Japan : Effect of Needle Punching and Spring Back Molding On Stiffness of Stampable Bamboo Fiber Sheet Processed with Pressed Mat2010

    • Author(s)
      Kazuya OKUBO, Toru FUJII, XIAOCHEN FU
    • Organizer
      5^<th> Vietnam conference on Chemical Science Hanoi University of Tecnology
    • Year and Date
      2010-11-16
  • [Presentation] Improvement of Strength of Bamboo Fiber Paper by Addition of MFC (Micro Fibrillated cellulose)2010

    • Author(s)
      Keisuke WAKASUGI, Kazuya OKUBO, Toru FUJII
    • Organizer
      The Sixth International Workshop on Green Composites (IWGC-6)
    • Place of Presentation
      Geumosan Hotel
    • Year and Date
      2010-09-10
  • [Presentation] Application of natural MFC (Micro Fibrillated cellulose) to improve fatigue life of plain CFRP2009

    • Author(s)
      Tomoya YASHIRO, Kazuya Okubo, Toru Fujii
    • Organizer
      JISSE-11 (11th Japan International SAMPE Sympo.& Exhibition, "Advanced Material Technology for Sustainable Development"
    • Place of Presentation
      Tokyo
    • Year and Date
      2009-11-27
  • [Presentation] Application of High Homogenization Technique to Fabrication of Electric Testing Prove Disk Using Micro-Fibrillated Bacteria Cellulose2008

    • Author(s)
      Kaho MATSUOKA, Kazuya OKUBO, Toru FUJII
    • Organizer
      the Third International Conference on Material and Processing MSEC ICMP2008-72473
    • Place of Presentation
      Northwestern University, Evanston, Illinois, USA
    • Year and Date
      20081007-20081010
  • [Remarks] ホームページ等

    • URL

      http://engineering.doshisha.ac.jp/kenkyu/labo/mech/me_02/index.html

  • [Patent(Industrial Property Rights)] 炭素繊維強化複合材料及びその製造方法2010

    • Inventor(s)
      藤井透.大窪和也.小武内清貴.竹内康徳.中辻毅
    • Industrial Property Rights Holder
      学校法人同志社サンスター技研株式会社
    • Industrial Property Number
      特許出願,特願2010-188976
    • Filing Date
      2010-08-25
  • [Patent(Industrial Property Rights)] 樹脂組成物の製造方法及び混練押出機2010

    • Inventor(s)
      藤井透、大窪和也、植松峻一、大森一寛、御園和則
    • Industrial Property Rights Holder
      学校法人同志社株式会社神戸製鋼所
    • Industrial Property Number
      特許出願,2010-008092
    • Filing Date
      2010-01-18
  • [Patent(Industrial Property Rights)] 繊維強化複合体2010

    • Inventor(s)
      藤井透、大窪和也、植松峻一、大森一寛、御園和則
    • Industrial Property Rights Holder
      学校法人同志社美津濃株式会社
    • Industrial Property Number
      特許出願,2010-012030
    • Filing Date
      2010-01-22
  • [Patent(Industrial Property Rights)] 炭素繊維強化炭素複合材料及びその製造方法2009

    • Inventor(s)
      藤井透.大窪和也.小武内清貴.竹内康徳.中辻毅
    • Industrial Property Rights Holder
      学校法人同志社サンスター技研株式会社
    • Industrial Property Number
      特許出願,特願2009-194259
    • Filing Date
      2009-08-25

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Published: 2012-01-26   Modified: 2016-04-21  

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