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2010 Fiscal Year Final Research Report

Low Friction Properties of Si-Incorporated DLC Coatings Treated with Oxygen Plasma

Research Project

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Project/Area Number 20360073
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Design engineering/Machine functional elements/Tribology
Research InstitutionThe University of Tokyo

Principal Investigator

CHOI Junho  The University of Tokyo, 大学院・工学系研究科, 准教授 (30392632)

Co-Investigator(Renkei-kenkyūsha) NAKAO Setsuo  独立行政法人産業技術総合研究所, サステナブルマテリアル研究部門, 主任研究員 (60357605)
Project Period (FY) 2008 – 2010
Keywordsトライボロジー / 固体薄膜 / 潤滑 / 摩擦 / 表面・界面物性
Research Abstract

In this study, the effects of silicon oxide layer on frictional properties of Si-DLC coatings were investigated by controlling the amount of silicon oxide on Si-DLC coatings. The amount of silicon oxide on the Si-DLC coating was controlled by oxygen plasma treatment for 30-300 s. In a result, the amount of silicon oxide on the top surface of Si-DLC coating increases with the increasing treatment time of oxygen plasma. The friction coefficients of Si-DLC coatings with 3-7at.%Si decrease to 0.02 due to oxygen plasma treatment, which is the lower value than that of Si-DLC coating with 13at.%Si. The surface hardness of Si-DLC coatings is slightly reduced by oxygen plasma treatment due to formation of silicon oxide on the top surface, whereas the hardness of wear track exhibits the same value to Si-DLC coating before oxygen plasma treatment. The Si-rich oxide layer formed on the Si-DLC coating plays roll of scarifying layer to reduce friction coefficient. The oxygen plasma treatment is effective to reduce the friction coefficient without hardness reduction in the entire Si-DLC coating.

  • Research Products

    (44 results)

All 2011 2010 2009 2008 Other

All Journal Article (19 results) (of which Peer Reviewed: 19 results) Presentation (25 results)

  • [Journal Article] Structural and mechanical properties of DLC films prepared by bipolar PBII&D2011

    • Author(s)
      J Choi, K Ishii, T Kato, M Kawaguchi, W Lee
    • Journal Title

      Diamond and Related Materials Vol.20

      Pages: 845-848

    • Peer Reviewed
  • [Journal Article] Nanostructural interpretation for elastic softening of amorphous carbon induced by the incorporation of silicon and hydrogen atoms2010

    • Author(s)
      T Kumagai, S Sawai, J Choi, S Izumi, T Kato
    • Journal Title

      Journal of Applied Physics Vol.107

      Pages: 124315-1-124315-7

    • Peer Reviewed
  • [Journal Article] シリコン含有DLC膜上の自己組織化単分子膜形成および摩擦特性2010

    • Author(s)
      崔〓豪, 桜井健一, 加藤孝久, 川口雅弘
    • Journal Title

      トライボロジスト Vol.55, No.8

      Pages: 44-50

    • Peer Reviewed
  • [Journal Article] Structures and phonon properties ofnanoscale fractional graphitic structuresin amorphous carbon determined bymolecular simulations2010

    • Author(s)
      T Kumagai, J Choi, S Izumi, T Kato
    • Journal Title

      Journal of Applied Physics Vol.107

      Pages: 104307-1-104307-6

    • Peer Reviewed
  • [Journal Article] Observation of self-assembled monolayers on diamond-like carbon films:agglomeration of self-assembled FDTS molecules2010

    • Author(s)
      J Choi, K Sakurai, T Kato
    • Journal Title

      Surface and Interface Analysi Vol.42

      Pages: 1373-1376

    • Peer Reviewed
  • [Journal Article] Effects of nitrogen gas ratio on composition and microstructure of BCN films prepared by RF magnetron sputtering2010

    • Author(s)
      S Nakao, T Soonawa, K Tsugawa, J Choi, T Kato
    • Journal Title

      Vacuum Vol.84

      Pages: 642-647

    • Peer Reviewed
  • [Journal Article] 酸素プラズマ処理によるシリコン添加DLC膜の低摩擦化2009

    • Author(s)
      崔〓豪, 角田篤, 熊谷知久, 加藤孝久,川口雅弘
    • Journal Title

      トライボロジスト Vol.54, No.11

      Pages: 53-61

    • Peer Reviewed
  • [Journal Article] Evaluation of Elastic Properties of DLC Coating on SKD61 Steel by Optical Indentation Microscopy2009

    • Author(s)
      M Ikeyama, J Choi, T Miyajima
    • Journal Title

      Surface and Coatings Technology Vol.203

      Pages: 2571-2574

    • Peer Reviewed
  • [Journal Article] Development of empirical bond order-type interatomic potential for amorphous carbon structures2009

    • Author(s)
      T Kumagai, S. Hara, J Choi, S. Izumi, T. Kato
    • Journal Title

      Journal of Applied Physics Vol.105

      Pages: 064310-1- 064310-10

    • Peer Reviewed
  • [Journal Article] Improvement of corrosion protection property of Mg-alloy by DLC and Si-DLC coatings with PBII technique and multi-target DC-RF magnetron sputtering2009

    • Author(s)
      M Ikeyama, S Nakao, S Tsutomu, J Choi
    • Journal Title

      Nuclear Instruments & Methods in Physics Research B Vol.267

      Pages: 1675-1679

    • Peer Reviewed
  • [Journal Article] 臨界せん断応力によるDLC膜の密着強度の評価2009

    • Author(s)
      崔〓豪, 石井啓資, 熊谷知久, 加藤孝久,疋田康弘
    • Journal Title

      トライボロジスト Vol.54, No.2

      Pages: 138-144

    • Peer Reviewed
  • [Journal Article] Effect of Substrate Bias Voltages on Hardness of BCN Films Prepared by RF Magnetron Sputtering2008

    • Author(s)
      S Nakao, J Choi, T Kato
    • Journal Title

      Transaction of the Materials Research Society of Japan Vol.33

      Pages: 1047-1051

    • Peer Reviewed
  • [Journal Article] Effect of Heat Treatment Temperature on PFPE Molecules Bonded on DLC Surface2008

    • Author(s)
      桜井健一, S Aoki, A Mitsuo, J Choi, T Kato
    • Journal Title

      Tribology Online Vol.3, No.5

      Pages: 259-263

    • Peer Reviewed
  • [Journal Article] Thermal Stability of SiBCN Films2008

    • Author(s)
      N Hayashi, J Choi, T Kumagai, T Kato, M Kawaguchi, S Nakao, M Ikeyama
    • Journal Title

      Tribology Online Vol.3, No.5

      Pages: 254-258

    • Peer Reviewed
  • [Journal Article] Estimation of DLC Wear Process by MicroLaser Raman Spectroscopy2008

    • Author(s)
      M Kawaguchi, S Aoki, A Mitsuo, K Morikawa, S Uchida, J Choi, T Kato
    • Journal Title

      Tribology Online Vol.3, No.2

      Pages: 110-115

    • Peer Reviewed
  • [Journal Article] Microstructure of Diamond-Like CarbonFilms Prepared Using Acetylene and Tolueneby Bipolar-Type Plasma Based Ion Implantation2008

    • Author(s)
      S Nakao, J Choi, T Kato
    • Journal Title

      Physica Status Solidi c Vol.5, No.4

      Pages: 973-976

    • Peer Reviewed
  • [Journal Article] Effect of Oxygen Plasma Treatment on theTribological Properties of Si-DLC Coatings2008

    • Author(s)
      J Choi, S Nakao, M Ikeyama, T Kato
    • Journal Title

      Physica Status Solidi c Vol.5, No.4

      Pages: 956-959

    • Peer Reviewed
  • [Journal Article] Effect of Deposition Pressure on theProperties of DLC Coatings Deposited byBipolar-Type PBII&D Surface and Interface2008

    • Author(s)
      J Choi, S Nakao, M Ikeyama, T Kato
    • Journal Title

      Analysis Vol.40

      Pages: 806-809

    • Peer Reviewed
  • [Journal Article] Nitriding of high speed steel by bipolar PBII for improvement in adhesion strength of DLC films

    • Author(s)
      J Choi, K Soejima, T Kato, M Kawaguchi, W Lee
    • Journal Title

      Nuclear Instruments & Methods in Physics Research B in press

    • Peer Reviewed
  • [Presentation] DLC膜におけるラマンパラメータと機械的特性の相関評価2011

    • Author(s)
      日比貴之, 崔〓豪, 加藤孝久,川口雅弘,稲吉成彦
    • Organizer
      日本トライボロジー学会トライボロジー会議予講集
    • Place of Presentation
      東京
    • Year and Date
      2011-05-24
  • [Presentation] バイポーラPBII法によるSKH2表面へのプラズマ窒化処理2010

    • Author(s)
      崔〓豪, 副島広志, 加藤孝久, 川口雅弘
    • Organizer
      日本トライボロジー学会トライボロジー会議予講集
    • Place of Presentation
      福井
    • Year and Date
      2010-09-15
  • [Presentation] バイポーラPBII法により作成したDLC膜の構造および機械的特性評価2010

    • Author(s)
      崔〓豪, 石井啓資, 熊谷知久, 加藤孝久,稲吉成彦, 芹澤一史
    • Organizer
      日本トライボロジー学会トライボロジー会議予講集 pp.83-84
    • Place of Presentation
      東京
    • Year and Date
      2010-05-17
  • [Presentation] 塩水中におけるDLC膜の保護特性第二報防食特性2010

    • Author(s)
      川口雅弘, 清水綾, 崔〓豪, 加藤孝久
    • Organizer
      日本トライボロジー学会トライボロジー会議予講集 pp.81-82
    • Place of Presentation
      東京
    • Year and Date
      2010-05-17
  • [Presentation] 塩水中におけるDLC膜の保護特性第1報:トライボロジー特性2010

    • Author(s)
      清水綾, 遊馬なつみ, 川口雅弘, 崔〓豪, 加藤孝久
    • Organizer
      日本トライボロジー学会トライボロジー会議予講集 pp.79-80
    • Place of Presentation
      東京
    • Year and Date
      2010-05-17
  • [Presentation] シリコン含有DLC膜上の自己組織化単分子膜形成2009

    • Author(s)
      崔〓豪, 桜井健一, 加藤孝久
    • Organizer
      摩擦の科学 pp.147
    • Place of Presentation
      名古屋
    • Year and Date
      2009-12-03
  • [Presentation] Observation of Self-Assembled Monolayers on Diamond-Like Carbon Films2009

    • Author(s)
      J Choi, K Sakurai, T Kato
    • Organizer
      13th European Conference on Applications of Surface and Interface Analysis (ECASIA) pp.339
    • Place of Presentation
      Antalya, Turkey
    • Year and Date
      2009-10-22
  • [Presentation] 原子スケールシミュレーションによるシリコン添加ダイヤモンドライクカーボン膜の構造・特性評価2009

    • Author(s)
      澤井周, 熊谷知久, 崔〓豪, 加藤孝久
    • Organizer
      日本機械学会第21回計算力学講演会
    • Place of Presentation
      金沢(CD-ROM論文集 pp.298-299)
    • Year and Date
      2009-10-11
  • [Presentation] タイトバインディング法を用いたDLC 膜のフォノンモードの解析2009

    • Author(s)
      熊谷知久, 崔〓豪, 加藤孝久
    • Organizer
      日本機械学会第21回計算力学講演会
    • Place of Presentation
      金沢(CD-ROM論文集 pp.296-297)
    • Year and Date
      2009-10-11
  • [Presentation] Formation of Carbon Mixing Layer on Silicon Surface by PBII&D2009

    • Author(s)
      M Kawaguchi, A Shimizu, S Nakanishi, A Monkawa, J Choi, T Kato
    • Organizer
      16th International Conference on Surface Modification of Materials by Ion Beams pp.116
    • Place of Presentation
      Tokyo, Japan
    • Year and Date
      2009-09-15
  • [Presentation] Structural Transformation of Diamond-Like Carbon Films under Various Sliding Conditions2009

    • Author(s)
      川口雅弘, 青木才子, A Mitsuo, J Choi, T Kato
    • Organizer
      World Tribology Congress pp.443. 12
    • Place of Presentation
      Kyoto, Japan
    • Year and Date
      2009-09-09
  • [Presentation] Development of Si-DLC Coatings with Ultra-Low Friction and High Hardness2009

    • Author(s)
      J Choi, A Tsunoda, T Kumagai, T Kato, M Kawaguchi
    • Organizer
      World Tribology Congress pp.403. 13
    • Place of Presentation
      Kyoto, Japan
    • Year and Date
      2009-09-09
  • [Presentation] Ab-Initio Investigations of the Atomic Structures of Si-DLC Films2009

    • Author(s)
      T Kumagai, S Sawai, J Choi, T Kato
    • Organizer
      World Tribology Congress pp.259. 14
    • Place of Presentation
      Kyoto, Japan
    • Year and Date
      2009-09-08
  • [Presentation] Critical Shear Stress of DLC Films with Different Film Thickness2009

    • Author(s)
      J Choi, K Ishii, T Kumagai, T Kato
    • Organizer
      ECOTRIB 2009 pp. 803-808
    • Place of Presentation
      Pisa, Italy
    • Year and Date
      2009-07-09
  • [Presentation] Study of Change in Structure of a-C:H Films Using Laser Raman Spectroscopy2009

    • Author(s)
      M Kawaguchi, S Aoki, A Mitsuo, J Choi, T Kato
    • Organizer
      ECOTRIB 2009 pp.505-510
    • Place of Presentation
      Pisa,Italy
    • Year and Date
      2009-06-09
  • [Presentation] 分子シミュレーションによるアモルファスカーボンのフォノンモード解析2009

    • Author(s)
      熊谷知久, 崔〓豪, 加藤孝久
    • Organizer
      日本トライボロジー学会トライボロジー会議予講集 pp.265-266
    • Place of Presentation
      東京
    • Year and Date
      2009-05-20
  • [Presentation] ダイヤモンドライクカーボン膜上の自己組織化単分子膜形成及び熱安定性2009

    • Author(s)
      崔〓豪, 桜井健一, 加藤孝久, 川口雅弘
    • Organizer
      日本トライボロジー学会トライボロジー会議予講集 pp.259-260
    • Place of Presentation
      東京
    • Year and Date
      2009-05-20
  • [Presentation] 原子シミュレーションによるアモルファスカーボンにおけるクラスター構造の検討2008

    • Author(s)
      熊谷知久, 澤井周, 崔〓豪, 泉聡志, 加藤孝久
    • Organizer
      日本機械学会第21回計算力学講演会
    • Place of Presentation
      沖縄(CD-ROM論文集 pp.438-439)
    • Year and Date
      2008-11-02
  • [Presentation] ダイヤモンドライクカーボン膜上の自己組織化単分子膜形成および熱安定性2008

    • Author(s)
      桜井健一, 崔〓豪, 加藤孝久
    • Organizer
      日本トライボロジー学会トライボロジー会議予講集 pp.403-404
    • Place of Presentation
      名古屋
    • Year and Date
      2008-09-16
  • [Presentation] 原子シミュレーションを用いたシリコンを含むアモルファスカーボン構造の検討2008

    • Author(s)
      熊谷知久, 澤井周, 蘭恵清, 崔〓豪, 加藤孝久
    • Organizer
      日本トライボロジー学会トライボロジー会議予講集 pp.399-400
    • Place of Presentation
      名古屋
    • Year and Date
      2008-09-16
  • [Presentation] Si-DLC 膜の摩擦特性に対する酸素プラズマ処理の影響2008

    • Author(s)
      角田篤史, 崔〓豪, 川口雅弘, 熊谷知久,加藤孝久, 中尾節男, 池山雅美
    • Organizer
      日本トライボロジー学会トライボロジー会議予講集 pp.181-182
    • Place of Presentation
      名古屋
    • Year and Date
      2008-09-16
  • [Presentation] PBII&D法により成膜したDLC 膜の摩擦熱の解析2008

    • Author(s)
      川口雅弘, 青木才子, 三尾淳, 崔〓豪,加藤孝久
    • Organizer
      日本トライボロジー学会トライボロジー会議予講集 pp.179-180
    • Place of Presentation
      名古屋
    • Year and Date
      2008-09-16
  • [Presentation] DLC膜上の自己組織化単分子膜形成と熱安定性評価2008

    • Author(s)
      崔〓豪, 桜井健一, 加藤孝久
    • Organizer
      摩擦の科学2008 pp.25
    • Place of Presentation
      刈谷
    • Year and Date
      2008-09-12
  • [Presentation] Low Friction Mechanism of Si-Incorporated Diamond-Like CarbonCoatings2008

    • Author(s)
      A Tsunoda, J Choi, T Kato,S Nakao, MIkeyama
    • Organizer
      63rd STLE Annual Meeting pp.1-6 (CDROM)
    • Place of Presentation
      Cleveland, OH
    • Year and Date
      2008-05-19
  • [Presentation] DLC薄膜の剥離荷重に及ぼす膜厚の影響2008

    • Author(s)
      石井啓資, 崔〓豪, 疋田康弘, 熊谷知久, 加藤孝久
    • Organizer
      日本トライボロジー学会トライボロジー会議予講集 pp.123-124
    • Place of Presentation
      東京
    • Year and Date
      2008-05-14

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Published: 2012-01-26   Modified: 2016-04-21  

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