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2010 Fiscal Year Final Research Report

Preparation of marine derived bionanofiers and their optically transparent high performance nanocomposites

Research Project

  • PDF
Project/Area Number 20559003
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Polymer/Textile materials
Research InstitutionTottori University

Principal Investigator

IFUKU Shinsuki  Tottori University, 大学院・工学研究科, 講師 (70402980)

Project Period (FY) 2008 – 2010
Keywordsキチン / キトサン / ナノファイバー / 複合材料 / バイオマス
Research Abstract

Chitin nanofibers were prepared from dried crab shells by a simple grinding treatment in a never-dried state under n acidic condition after the removal of proteins and minerals. The obtained nanofibers were observed by FE-SEM and ound to have a uniform width of approximately 10-20 nm and high aspect ratio; both these findings were similar to hose for nanofibers from prawns. Furthermore, it was confirmed that the nanofibers were extracted from the aturalchitin/protein/mineral composites of crab shell in their original state. That is, the N-acetyl group was not emoved and the chitin crystal structure was maintained, as confirmed by elemental analysis data, FT-IR spectra, and X-ray diffraction profiles.
Optically transparent chitin nanofiber composites were fabricated with acrylic resins. Chitin nanofibers rastically increased the Young's moduli and the tensile strengths, and decreased the thermal expansion of all acrylic resins due to the reinforcement effect of chitin nanofibers having an extended crystal structure.

  • Research Products

    (29 results)

All 2011 2010 2009 2008 Other

All Journal Article (9 results) (of which Peer Reviewed: 8 results) Presentation (10 results) Book (1 results) Remarks (2 results) Patent(Industrial Property Rights) (7 results)

  • [Journal Article] Fabrication of uniform cellulose nanofibers from parenchyma cells of pears and apples2011

    • Author(s)
      Shinsuke Ifuku, Masatoshi Adachi, Minoru Morimoto, Hiroyuki Saimoto
    • Journal Title

      繊維学会誌 Vol.67

      Pages: 86-90

    • Peer Reviewed
  • [Journal Article] Simple preparation method of chitin nanofibers with a uniform width of 10 to 20 nm from prawn shell under the neutral conditions2011

    • Author(s)
      Shinsuke Ifuku, M. Iftekhar Shams, , Masaya Nogi, Masafumi Yoshioka, Minoru Morimoto, Hiroyuki Saimoto, Hiroyuki Yano
    • Journal Title

      Carbohydrate Polymers Vol.84

      Pages: 762-764

    • Peer Reviewed
  • [Journal Article] Fabrication of optically transparent chitin nanocomposites2011

    • Author(s)
      Shinsuke Ifuku, Masaya Nogi, Takeshi Oku, Hiroyuki Yano
    • Journal Title

      Applied Physics A. Vol.102

      Pages: 325-331

    • Peer Reviewed
  • [Journal Article] カニ、エビ殻に内包されるキチンナノファイバーの単離技術の開発2010

    • Author(s)
      伊福伸介
    • Journal Title

      日本接着学会誌 Vol.46

      Pages: 385-390

  • [Journal Article] Acetylation of chitin nanofibers and their transparent nanocomposite films2010

    • Author(s)
      Shinsuke Ifuku, Shin Morooka, Minoru, Morimoto, Hiroyuki Saimoto
    • Journal Title

      Biomacromolecules Vol.10

      Pages: 1326-1330

    • Peer Reviewed
  • [Journal Article] Fibrillation of dried chitin into 10-20 nm nanofibers by a simple method under acidic conditions2010

    • Author(s)
      Shinsuke Ifuku, Masaya Nogi, Masafumi Yoshioka, Minoru Morimoto, Hiroyuki Yano, Hiroyuki Saimoto
    • Journal Title

      Carbohydrate Polymers Vol.81

      Pages: 134-139

    • Peer Reviewed
  • [Journal Article] Preparation of chitin nanofibers with a uniform width as α-chitin from crab shells2009

    • Author(s)
      Shinsuke Ifuku, Masaya Nogi, Kentaro Abe, Masafumi Yoshioka Minoru Morimoto, Hiroyuki Saimoto, Hiroyuki Yano
    • Journal Title

      Biomacromolecules Vol.10

      Pages: 1584-1588

    • Peer Reviewed
  • [Journal Article] Preparation of chemoselective N-phthaloyl chitosan in aqueous media

    • Author(s)
      Shinsuke Ifuku, Takeshi Miwa, Minoru Morimoto, Hiroyuki Saimoto
    • Journal Title

      Green Chemistry in press.

    • Peer Reviewed
  • [Journal Article] Preparation of highly regioselective chitosan derivatives via "click chemistry"

    • Author(s)
      Shinsuke Ifuku, Masahiro Wada, Minoru Morimoto, Hiroyuki Saimoto
    • Journal Title

      Carbohydrate Polymers in press.

    • Peer Reviewed
  • [Presentation] Preparation of Chitin Nanofibers from crab shell and their transparent nanocomposite films2011

    • Author(s)
      伊福伸介
    • Organizer
      Chitin & chitosan symposium 2010 2^<nd> international and cross-strait chitin and chitosan symposium & the 7^<th> national academic conference on chitin and chitosan
    • Place of Presentation
      Qianjiang, China
    • Year and Date
      20111100
  • [Presentation] キチンナノファイバーで補強した透明フレキシブルプラスチックフィルムの調製2011

    • Author(s)
      伊福伸介
    • Organizer
      日本化学会
    • Year and Date
      20110300
  • [Presentation] Fibrillation of dried chitin into 10-20 nm nanofibers by a simple grinding method under acidic conditions and their transparent nanocomposite films2010

    • Author(s)
      伊福伸介
    • Organizer
      2010 International Chemical Congress of Pacific Basin Societies.PACIFICHEM 2010
    • Place of Presentation
      Honolulu, Hawaii, USA
    • Year and Date
      20101200
  • [Presentation] 乾燥キチンからの簡便なナノファイバー製造技術とその透明複合フィルムの開発2010

    • Author(s)
      伊福伸介
    • Organizer
      第24回キチン・キトサンシンポジウム
    • Place of Presentation
      東京
    • Year and Date
      20100700
  • [Presentation] 廃棄果実から単離されるセルロースナノファイバー2010

    • Author(s)
      伊福伸介
    • Organizer
      セルロース学会
    • Place of Presentation
      香川
    • Year and Date
      20100700
  • [Presentation] 乾燥キチンを原料とした効率的なナノファイバー化技術の開発2010

    • Author(s)
      伊福伸介
    • Organizer
      第59回高分子学会年次大会
    • Place of Presentation
      横浜
    • Year and Date
      20100500
  • [Presentation] カニ、エビ殻より抽出される天然繊維「キチンナノファイバー」2009

    • Author(s)
      伊福伸介
    • Organizer
      日本化学会西日本大会2009日本化学会西日本大会
    • Place of Presentation
      愛媛
    • Year and Date
      20091100
  • [Presentation] Simple Preparation method of chitin nanofibers from prawn shell under neutral conditions2009

    • Author(s)
      伊福伸介
    • Organizer
      The 11^<th> International Conference on Chitin and Chitosan & The 8^<th> Asia-Pacific Chitin and Chitosan Symposium
    • Place of Presentation
      Taipei, Taiwan
    • Year and Date
      20090900
  • [Presentation] Preparation of chitin nanofaibers from crab shell and optically transparent composites reinforced with the nanofibers2009

    • Author(s)
      伊福伸介
    • Organizer
      237 th ACS National Meeting
    • Place of Presentation
      Salt Lake City, UT
    • Year and Date
      20090322-20090326
  • [Presentation] キチンナノファイバー補強プラスチックの開発2008

    • Author(s)
      伊福伸介
    • Organizer
      キチンキトサン学会2008第22回キチン・キトサンシンポジウム
    • Place of Presentation
      新潟
    • Year and Date
      20080800
  • [Book] Preparation of chitin nanofibers with a uniform width of 10-20 nm from crab and prawn shells and their transparent nanocomposite films

    • Author(s)
      Shinsuke Ifuku, Antonio N. Nakagaito, Hiroyuki Saimoto
    • Publisher
      Nova Science Publishers, Inc., NY, In Optical Networks.
  • [Remarks] ホームページ

    • URL

      http://saimotolab.sakura.ne.jp/index.html

  • [Remarks]

    • URL

      http://space.geocities.jp/s_s_ifuku/top.html

  • [Patent(Industrial Property Rights)] キチンナノファイバーまたはキトサンナノファイバーを含む塗料組成物2010

    • Inventor(s)
      斎本博之、伊福伸介、森本稔、大村善彦、米田敏和
    • Industrial Property Rights Holder
      国立大学法人鳥取大学 外1名
    • Industrial Property Number
      特許,特願2010-270662
    • Acquisition Date
      2010-12-03
  • [Patent(Industrial Property Rights)] キチンナノファイバーを含む化粧品、入浴剤および医薬組成物2010

    • Inventor(s)
      南三郎、今川智敬、岡本芳晴、柄武志、斎本博之、伊福伸介、工藤祐司
    • Industrial Property Rights Holder
      国立大学法人鳥取大学 外1名
    • Industrial Property Number
      特許,特願2010-207802
    • Acquisition Date
      2010-09-16
  • [Patent(Industrial Property Rights)] ナノファイバー強化タンパク質多孔膜2010

    • Inventor(s)
      山口修、斎本博之、伊福伸介
    • Industrial Property Rights Holder
      国立大学法人鳥取大学 外1名
    • Industrial Property Number
      特許,特願2010-221417
    • Filing Date
      20100931
  • [Patent(Industrial Property Rights)] 繊維複合材及びその製造方法2010

    • Inventor(s)
      古賀真、伊福伸介、斎本博之
    • Industrial Property Rights Holder
      国立大学法人鳥取大学 外1名
    • Industrial Property Number
      特許,特願2010-181946
    • Filing Date
      2010-08-16
  • [Patent(Industrial Property Rights)] ナノファイバー補強透明複合材2010

    • Inventor(s)
      伊福伸介、斎本博之、金谷慎吾、山口善之、細見哲也
    • Industrial Property Rights Holder
      国立大学法人鳥取大学 外1名
    • Industrial Property Number
      特許,特願2010-181572
    • Filing Date
      2010-08-16
  • [Patent(Industrial Property Rights)] マリンナノファイバー2009

    • Inventor(s)
      斎本博之、伊福伸介
    • Industrial Property Rights Holder
      国立大学法人鳥取大学
    • Industrial Property Number
      商願2009-094569
    • Filing Date
      2009-12-15
  • [Patent(Industrial Property Rights)] PROCESS FOR PRODUCING CHITIN NANOFIBER, COMPOSITE MATERIAL AND COATING COMPOSITION BOTH CONTAINING CHITIN NANOFIBER, PROCESS FOR PRODUCING CHITOSAN NANOFIBER, AND COMPOSITE MATERIAL AND COATING COMPOSITION BOTH CONTAINING CHITOSAN NANOFIBER2009

    • Inventor(s)
      Ifuku Shinsuke, Saimoto Hiroyuki, Yano Hiroyuki, Omura Yoshihiko
    • Industrial Property Rights Holder
      国立大学法人鳥取大学 外1名
    • Industrial Property Number
      特許,WO/2010/073758
    • Filing Date
      2009-06-30

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Published: 2012-01-26   Modified: 2016-04-21  

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