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2020 Fiscal Year Research-status Report

Dissimilar friction welding of titanium alloy and stainless steel and its welding principle elucidation for spinal fixation application

Research Project

Project/Area Number 20K05169
Research InstitutionOsaka University

Principal Investigator

劉 恢弘  大阪大学, 接合科学研究所, 准教授 (40748943)

Project Period (FY) 2020-04-01 – 2023-03-31
KeywordsFriction welding / Titanium alloy / Stainless steel / Microstructural / Mechanical properties
Outline of Annual Research Achievements

Ti-6Al-4V alloy (Ti64) and SUS316L stainless steel rods of 10 mm in diameter were dissimilarly friction welded. The relationship between the processing conditions, weld interface microstructure and its evolution, and mechanical properties of the fabricated joints were systematically investigated in order to obtain a sound dissimilar Ti64/SUS316L joint. The results show that the increased friction pressure unexpectedly decreased the welding temperature, which effectively suppressed the formation of the thick intermetallic compound layers at the weld interface that was supposed to be beneficial for the joint strength improvement. However, high shear strain rate and high temperature rising rate occurred between the faying surfaces caused a formation of the hard and brittle Ti64/SUS316L mechanically mixed layers at the weld interface, which significantly deteriorated the joint quality. Based on the above findings, rotation speed reduction and liquid CO2 cooling were accordingly utilized to reduce the shear strain rate and the temperature increasing rate. As a result, the formation of the harmful mechanically mixed layers was effectively suppressed at the weld interface, and a high-quality dissimilar Ti64/SUS316L friction welded joint was successfully fabricated.

Current Status of Research Progress
Current Status of Research Progress

2: Research has progressed on the whole more than it was originally planned.

Reason

This study aims to elucidate the welding principle for the friction welding of Ti64 and SUS316L and fabricate a sound dissimilar Ti64/SUS316L joint. In the last year, Ti64 and SUS316L rods with the diameter of 10 mm were subjected to the friction welding under various processing parameters. The interface microstructure, microstructural evolution, and mechanical properties of the obtained joints were carefully examined. We found that even though the increased friction pressure acted to effectively lower the welding temperature hence to significantly suppress the brittle intermetallic compound layer formation, the harmful Ti64/SUS316L mechanically mixed layers were generated at the weld interface due to the high shear strain rate and high temperature rising rate between the faying surfaces, that remarkably deteriorated the joint quality. Rotation speed reduction and external cooling were accordingly adopted, which effectively suppressed the mechanically mixed layer formation and successfully improved the joint quality. Based on the above results, we consider that the study is progressing rather smoothly.

Strategy for Future Research Activity

In the last year, we have conducted friction welding on Ti64 and SUS316L rods and carefully investigated the relationship between the processing parameters, interface microstructure and its evolution, and mechanical properties of the fabricated joints. We found that the formation of the harmful Ti64/SUS316L mechanically mixed layers, which closely correlated to the joint quality, was attributed to the high shear strain rate and high temperature rising rate between the faying surfaces and successfully improved the joint quality through suppressing the harmful mechanically mixed layer formation via a series of corresponding parameter optimizations. For the next step, the thermal cycles and material deformation behaviors at the weld interface during friction welding under different processing conditions will be discussed via experimental and simulation methods, so that the processing parameters, temperature/strain/strain-rate evolution, and microstructure/mechanical properties of the joints could be comprehensively analyzed, allowing the welding principle for the friction welding of Ti64 and SUS316L possible to be clarified. Based on the obtained findings, we will further optimize the processing parameters, trying to further improve the joint quality using simpler and easier welding procedures.

  • Research Products

    (25 results)

All 2021 2020

All Journal Article (8 results) (of which Int'l Joint Research: 3 results,  Peer Reviewed: 8 results) Presentation (11 results) (of which Int'l Joint Research: 2 results) Patent(Industrial Property Rights) (6 results) (of which Overseas: 3 results)

  • [Journal Article] In situ observation of solidification crack propagation for type 310S and 316L stainless steels during TIG welding using synchrotron X-ray imaging2021

    • Author(s)
      Tomoya Nagira, Daisuke Yamashita, Masayoshi Kamai, Huihong Liu, Yasuhiro Aoki, Kentaro Uesugi, Akihisa Takeuchi, Hidetoshi Fujii
    • Journal Title

      Journal of Materials Science

      Volume: 56 Pages: 10653-10663

    • DOI

      10.1007/s10853-021-05969-0

    • Peer Reviewed
  • [Journal Article] Ultralow rotation speed produces high-quality joint in dissimilar friction welding of Ti–6Al–4V alloy and SUS316L stainless steel2021

    • Author(s)
      Huihong Liu, Hidetoshi Fujii
    • Journal Title

      Materials Science and Engineering: A

      Volume: 800 Pages: 140303

    • DOI

      10.1016/j.msea.2020.140303

    • Peer Reviewed
  • [Journal Article] Principle for obtaining high joint quality in dissimilar friction welding of Ti-6Al-4V alloy and SUS316L stainless steel2020

    • Author(s)
      Huihong Liu, Yo Aoki, Yasuhiro Aoki, Kohsaku Ushioda, Hidetoshi Fujii
    • Journal Title

      Journal of Materials Science & Technology

      Volume: 46 Pages: 211-224

    • DOI

      10.1016/j.jmst.2019.10.037

    • Peer Reviewed
  • [Journal Article] Superplastic deformation mechanism of the friction stir processed fully lamellar Ti-6Al-4V alloy2020

    • Author(s)
      Wenjing Zhang, Huihong Liu, Hua Ding, Hidetoshi Fujii
    • Journal Title

      Materials Science and Engineering: A

      Volume: 785 Pages: 139390

    • DOI

      10.1016/j.msea.2020.139390

    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] The optimal temperature for enhanced low-temperature superplasticity in fine-grained Ti–15V–3Cr–3Sn–3Al alloy fabricated by friction stir processing2020

    • Author(s)
      Wenjing Zhang, Huihong Liu, Hua Ding, Hidetoshi Fujii
    • Journal Title

      Journal of Alloys and Compounds

      Volume: 832 Pages: 154917

    • DOI

      10.1016/j.jallcom.2020.154917

    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Time-resolved X-ray imaging of solidification cracking for Al-Cu alloy at the weld crater2020

    • Author(s)
      T. Nagira, D. Yamashita, M. Kamai, H. Liu, Y. Aoki, H. Fujii, K. Uesugi, A. Takeuchi
    • Journal Title

      Materials Characterization

      Volume: 167 Pages: 110469

    • DOI

      10.1016/j.matchar.2020.110469

    • Peer Reviewed
  • [Journal Article] Dissimilar friction stir welding of pure Ti and carbon fibre reinforced plastic2020

    • Author(s)
      Jeong-Won Choi, Yoshiaki Morisada, Huihong Liu, Kohsaku Ushioda, Hidetoshi Fujii, Kimiaki Nagatsuka, Kazuhiro Nakata
    • Journal Title

      Science and Technology of Welding and Joining

      Volume: 25 Pages: 600-608

    • DOI

      10.1080/13621718.2020.1788814

    • Peer Reviewed
  • [Journal Article] The Deformation Behavior of Oxygen-Modified Ti-29Nb-13Ta-4.6Zr(wt.%)2020

    • Author(s)
      V. Khademi, H. Liu, M. Nakai, M. Niinomi, C.J. Boehlert
    • Journal Title

      MATEC Web of Conferences

      Volume: 321 Pages: 11003

    • DOI

      10.1051/matecconf/202032111003

    • Peer Reviewed / Int'l Joint Research
  • [Presentation] 高炭素鋼の圧力制御通電圧接における 界面接合機構の解明2021

    • Author(s)
      劉 恢弘,宮垣 徹也,釜井 正善,馬 運五,麻 寧緒,藤井 英俊
    • Organizer
      日本金属学会 2021年春期 第168回講演大会(オンライン開催)
  • [Presentation] Superplastic deformation mechanism for fully lamellar Ti-6Al-4V alloy processed by friction stir processing2020

    • Author(s)
      Wenjing Zhang, Huihong Liu, Hua Ding, Hidetoshi Fujii
    • Organizer
      溶接学会 2020年度 春季全国大会
  • [Presentation] ジュール熱大荷重局部変形接合法を利用した高炭素鋼の低温圧接:界面組織観察と接合機構解明2020

    • Author(s)
      劉 恢弘,宮垣 徹也,釜井 正善,馬 運五,麻 寧緒,藤井 英俊
    • Organizer
      溶接学会 2020年度 春季全国大会
  • [Presentation] ジュール熱大荷重局部変形接合法によるTi-6Al-4VとSUS316Lの健全異種継手の作製2020

    • Author(s)
      林 泳錫,劉 恢弘,藤井 英俊
    • Organizer
      溶接学会 2020年度 春季全国大会
  • [Presentation] Fabrication of high-quality joint in dissimilar friction welding of Ti-6Al-4V alloy and SUS316L stainless steel2020

    • Author(s)
      Huihong Liu, Yo Aoki, Yasuhiro Aoki, Hidetoshi Fujii
    • Organizer
      International Institute of Welding (Commission III Annual Assembly 2020 online)
    • Int'l Joint Research
  • [Presentation] Dissimilar friction stir welding of pure Ti and carbon fiber reinforced plastic2020

    • Author(s)
      Jeong-won Choi, Yoshiaki Morisada, Huihong Liu, Kohsaku Ushioda, Hidetoshi Fujii, Kimiaki Nagatsuka, Kazuhiro Nakata
    • Organizer
      International Institute of Welding (Commission III Annual Assembly 2020 online)
    • Int'l Joint Research
  • [Presentation] 高炭素鋼の圧接制御通電圧接における界面接合機構の解明2020

    • Author(s)
      劉 恢弘,宮垣 徹也,釜井 正善,馬 運五,麻 寧緒,藤井 英俊
    • Organizer
      溶接学会 2020年度 秋季全国大会(WEB開催)
  • [Presentation] ジュール熱大荷重局部変形接合法を利用した高炭素鋼の低温圧接:界面組織観察と接合機構解明2020

    • Author(s)
      劉 恢弘,宮垣 徹也,釜井 正善,馬 運五,麻 寧緒,藤井 英俊
    • Organizer
      溶接学会 2020年度 秋季全国大会(WEB開催)
  • [Presentation] Ti-CFRP摩擦攪拌接合継手の機械的性質に及ぼす接合温度の影響2020

    • Author(s)
      崔 正原,森貞 好昭,劉 恢弘,潮田 浩作,藤井 英俊,永塚 公彬,中田 一博
    • Organizer
      溶接学会 2020年度 秋季全国大会(WEB開催)
  • [Presentation] 圧力制御通電圧接Ti-6Al-4V/SUS316L異材継手における接合界面形成機構の解明2020

    • Author(s)
      林 泳錫,劉 恢弘,森貞 好昭,藤井 英俊
    • Organizer
      溶接学会 2020年度 秋季全国大会(WEB開催)
  • [Presentation] 極低回転速度による健全なTi-6Al-4V/SUS316L摩擦圧接継手の作製2020

    • Author(s)
      劉 恢弘,藤井 英俊
    • Organizer
      日本金属学会 2020年秋期 第167回講演大会(オンライン開催)
  • [Patent(Industrial Property Rights)] 異材摩擦攪拌接合方法及び異材摩擦攪拌接合部材2020

    • Inventor(s)
      藤井 英俊, 森貞 好昭, 劉 恢弘
    • Industrial Property Rights Holder
      藤井 英俊, 森貞 好昭, 劉 恢弘
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      特願2020-149882
  • [Patent(Industrial Property Rights)] 摩擦圧接方法2020

    • Inventor(s)
      藤井 英俊,劉 恢弘,森貞 好昭
    • Industrial Property Rights Holder
      藤井 英俊,劉 恢弘,森貞 好昭
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      特願2020-160467
  • [Patent(Industrial Property Rights)] 金属材の固相接合方法及び固相接合装置2020

    • Inventor(s)
      藤井 英俊, 森貞 好昭, 劉 恢弘, 青木 祥宏,釜井 正善
    • Industrial Property Rights Holder
      藤井 英俊, 森貞 好昭, 劉 恢弘, 青木 祥宏,釜井 正善
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      1970353.1
    • Overseas
  • [Patent(Industrial Property Rights)] 金属材の固相接合方法及び固相接合装置2020

    • Inventor(s)
      藤井 英俊, 森貞 好昭, 劉 恢弘, 青木 祥宏,釜井 正善
    • Industrial Property Rights Holder
      藤井 英俊, 森貞 好昭, 劉 恢弘, 青木 祥宏,釜井 正善
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      16/981.001
    • Overseas
  • [Patent(Industrial Property Rights)] 金属材の固相接合方法及び固相接合装置2020

    • Inventor(s)
      藤井 英俊, 森貞 好昭, 劉 恢弘, 青木 祥宏,釜井 正善
    • Industrial Property Rights Holder
      藤井 英俊, 森貞 好昭, 劉 恢弘, 青木 祥宏,釜井 正善
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      201980037370.3
    • Overseas
  • [Patent(Industrial Property Rights)] 金属材の固相接合方法及び固相接合装置2020

    • Inventor(s)
      藤井 英俊, 森貞 好昭, 劉 恢弘, 青木 祥宏,釜井 正善
    • Industrial Property Rights Holder
      藤井 英俊, 森貞 好昭, 劉 恢弘, 青木 祥宏,釜井 正善
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      特願2020-507455

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Published: 2021-12-27  

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