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2010 Fiscal Year Final Research Report

Deve I opment of next-enerat i on e I ectron tomography for 3D mesa-ea I e structural analysisDeve I opment of next-enerat i on e I ectron tomography for 3D mesa-ea I e structural analysisDeve I opment of next-enerat i on e I ectron tomography for 3D mesa-ea I e structural analysis

Research Project

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Project/Area Number 21241030
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Nanomaterials/Nanobioscience
Research InstitutionKyushu University (2010-2011)
Kyoto Institute of Technology (2009)

Principal Investigator

JINNAI Hiroshi  九州大学, 先導物質化学研究所, 特任教授 (20303935)

Project Period (FY) 2009 – 2011
Keywordsナノ材料解析 / 評価
Research Abstract

In this project, we have developed next generation transmission electron microtomography that enables us to observe very thick(on the order of micron) polymeric(or biological) specimens with 200 kV transmission electron microscope(TEM). The developments include newly designed high contrast pole piece with scanning optics with wider gap, and corresponding energy filtering system. Lowering the focusing angle of the scanning electron beam, and thus larger depth of focus, it is now possible to observe 1 to 2 gm thick polymeric specimen with resolution varying from a few nm to a few tens of nm in three dimension.

  • Research Products

    (29 results)

All 2012 2011 2010 2009 Other

All Journal Article (11 results) (of which Peer Reviewed: 2 results) Presentation (17 results) Remarks (1 results)

  • [Journal Article] Morphological Transition of Triblock Copolymer Cylindrical Micelles Responding to Solvent Change2012

    • Author(s)
      D.Han, et al
    • Journal Title

      Soft Matter

      Volume: 8 Pages: 2144-2151

    • DOI

      10.1039/C2SM07020K

    • Peer Reviewed
  • [Journal Article] Tilt-angle measurement of a sample stage using a capacitive liquid-based inclinometer2012

    • Author(s)
      K. Matoba, J. Takagi, T. Yasunaga, H. Jinnai, K. Iwasaki
    • Journal Title

      J. Electron. Microsc

      Volume: (未定)

  • [Journal Article] Creating Suprapolymer Assemblies : Nanowires, Nanorings, and Nanospheres Prepared from Symmetric BlockCopolymers Confined in Spherical Particles2012

    • Author(s)
      H. Yabu, S. Sateo, T. Higuchi, H. Jinnai, M. Shimomura
    • Journal Title

      J. Mater. Chem

      Volume: 22 Pages: 7672-7675

  • [Journal Article] Threedimensional observation of confined phaseseparated structures in block copolymer nanoparticles2012

    • Author(s)
      T. Higuchi, K. Motoyoshi, H. Sugimori, H. Jinnai, H. Yabu*, M. Shimomura
    • Journal Title

      Soft Matter

      Volume: 8 Pages: 3791-3797

  • [Journal Article] Structural characterization of the Fddd phase in a diblock copolymer thin film by electron microtomography2011

    • Author(s)
      J.Jung, et al
    • Journal Title

      Soft Matter

      Volume: 7 Pages: 10424-10428

    • DOI

      10.1039/clsm06236k

    • Peer Reviewed
  • [Journal Article] Single chain distribution analysis near a substrate using a combined method of threedimensional imaging and SCF simulation2011

    • Author(s)
      H. Maritaa, H. Sugimori, M. Doli, H. Jinnai
    • Journal Title

      Eur. Polymer J

      Volume: 47 Pages: 685-691

  • [Journal Article] Solvent-Driven Evolution of Block Copolymer Morphology under 3D Confinement2010

    • Author(s)
      L. Li, K. Matsunaga, J. Zhu, T. Higuchi, H. Yabu, M. Shimomura, H. Jinnai, R. C. Hayward*, T. P. Russell
    • Journal Title

      Macromolecules

      Volume: 43(18) Pages: 7807-7812

  • [Journal Article] Dependence of beam broadening on detection angle in scanning transmission electron microtomography2010

    • Author(s)
      S. Motoki, T. Kaneko, Y. Aoyama, H. Nishioka, Y. Okura, Y. Kondo, H. Jinnai
    • Journal Title

      J. Electron. Microsc

      Volume: 59 Pages: S45-S53

  • [Journal Article] Transmission Electron Microtomography and Polymer Nanostructures2010

    • Author(s)
      H. Jinnai*, R. J. Spontak, T. Nishi
    • Journal Title

      Macromolecules

      Volume: 43(4) Pages: 1675-1688

  • [Journal Article] Self-Assembled ABC Triblock Copolymer Double and Triple Helices2009

    • Author(s)
      J. Dupont, G. Lin*, K. Niihara, R. Kimoto, H. Jinnai
    • Journal Title

      Angew. Chem

      Volume: 48(33) Pages: 6144-6147

  • [Journal Article] Small-Molecule-Directed Nanoparticle Assembly Toward Stimuliresponsive Nanocomposites2009

    • Author(s)
      Y. Zhao, K. Thorkelsson, A. J. Mastroianni, T. Schilling, J. M. Luther, B. J. Rancatore, K. Matsunaga, H. Jinnai, Y. We, D. Poulsen, J. M. J. Frechet, A. P. Alivisatos, T. Xu*
    • Journal Title

      Nat. Mater

      Volume: 8(12) Pages: 979-985

  • [Presentation] Recent Development of Electron Tomography for Polymeric Nano and MesoStructures2010

    • Author(s)
      H. Jinnai
    • Organizer
      International Microscopy Congress 17(IMC17)
    • Place of Presentation
      Windsor Barra Convention Center, Rio de Janeiro, Brazil
    • Year and Date
      2010-09-24
  • [Presentation] Electron Tomography of Soft Polymeric Materials2010

    • Author(s)
      H. Jinnai
    • Organizer
      SofTEAM Workshop
    • Place of Presentation
      Berkeley, CA, U SA
    • Year and Date
      2010-03-08
  • [Presentation] Electron tomography for thick polymeric s amples of the order of micrometer2010

    • Author(s)
      H. Jinnai
    • Organizer
      10-th International Symposium on Biomimeti c Materials Processing(BMMP-10)
    • Place of Presentation
      Nagoya, Japan
    • Year and Date
      2010-01-28
  • [Presentation] 高分子材料の3次元構造解析一最新の技術と可能性一2010

    • Author(s)
      陣内浩司
    • Organizer
      日本接着学会粘着研究会1.月度例会
    • Place of Presentation
      大阪市立工業研究所
    • Year and Date
      2010-01-22
  • [Presentation] ポリマー材料の定量的3D解析2010

    • Author(s)
      陣内浩司
    • Organizer
      階層的3D4Dフォーラム
    • Place of Presentation
      九州大学伊都キャンパス鉄鋼リサーチセンター
    • Year and Date
      2010-01-12
  • [Presentation] Microphaseseparated structure in a cylind erforming block copolymer thin film studied by neutron reflectivity aided by transmission electron microtomography2009

    • Author(s)
      H. Jinnai et al
    • Organizer
      St ructure of Nanophase Materials
    • Place of Presentation
      SAS
    • Year and Date
      20090000
  • [Presentation] 3D Elemental Mapping of Soft Materials using Transmission Electron Microtomography2009

    • Author(s)
      H. Jinnai
    • Organizer
      7th International Symposium on Atomic Level Characterizations for New Mate rials and Devices' 09(ALC' 09)
    • Place of Presentation
      The Westin Maui Reso rt & Spa, Maui, Hawaii, USA
    • Year and Date
      2009-12-10
  • [Presentation] ソフトマテリアル機能材料の3次元構造観察と解析2009

    • Author(s)
      陣内浩司
    • Organizer
      第29回水素エネルギー協会大会
    • Place of Presentation
      タワーホール船堀5階小ホール
    • Year and Date
      2009-12-03
  • [Presentation] トモグラフィから何が測れるか?(3次元測定の種類と阻害要因)2009

    • Author(s)
      陣内浩司
    • Organizer
      日本顕微鏡学会3次元電子線トモグラフィ法のマテリアルへの展開研究部会講演会
    • Place of Presentation
      工学院大学
    • Year and Date
      2009-11-28
  • [Presentation] 電子線トモグラフィー法による観察・評価の現状と今後2009

    • Author(s)
      陣内浩司
    • Organizer
      半導体計測・評価技術ネットワーク」ワークショップ
    • Place of Presentation
      茨城県つくば市国際会議場
    • Year and Date
      2009-11-24
  • [Presentation] 電子線トモグラフィー法のソフトマテリアルへの応用2009

    • Author(s)
      陣内浩司
    • Organizer
      日本顕微鏡学会第53回シンポジウム
    • Place of Presentation
      東京工業大学大岡山キャンパス
    • Year and Date
      2009-10-31
  • [Presentation] Self-assembled polymer nanostructures2009

    • Author(s)
      H. Jinnai
    • Organizer
      International Conference on Supercrit ical Fluids(Supergreen2009)
    • Place of Presentation
      Sendai, Japan
    • Year and Date
      2009-10-17
  • [Presentation] Helical structures formed from an amorph ous, achiral ABC triblock terpolymer2009

    • Author(s)
      H. Jinn
    • Organizer
      International Symposium on Nano S tructured Polymeric Materials : Synthesis, Cha racterization and Application
    • Place of Presentation
      Gwangju, Korea
    • Year and Date
      2009-10-07
  • [Presentation] 高分子ブロック共重合体の自己秩序化するメソスケール構造2009

    • Author(s)
      陣内浩司
    • Organizer
      日本化学会第3回関東支部大会
    • Place of Presentation
      早稲田大学理工キャンパス
    • Year and Date
      2009-09-05
  • [Presentation] ACA(American Crystallographic Associati on)2009

    • Author(s)
      H. Jinnai
    • Organizer
      Meeting
    • Place of Presentation
      Toronto, Canada
    • Year and Date
      2009-07-29
  • [Presentation] 電子線トモグラフィー法とエックス線CTによる高分子材料の三次元観察・解析2009

    • Author(s)
      陣内浩司
    • Place of Presentation
      東京大学先端科学技術センター
    • Year and Date
      2009-05-15
  • [Presentation] Science for Future Molecul ar Systems2009

    • Author(s)
      陣内浩司
    • Organizer
      ブロック共重合体の自己秩序化に関する最近の進展,陣内浩司
    • Place of Presentation
      九州大学伊都キャンパス
    • Year and Date
      2009-04-30
  • [Remarks]

    • URL

      http://muse.ifoc.kyushu-.ac.jp/JLAB/JINNAILABORATORY/Welcome.html

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Published: 2013-07-31  

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