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2011 Fiscal Year Final Research Report

Growth of High quality Lead Zirconium Titanate Single-crystalline Films and Their Basic Property

Research Project

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Project/Area Number 21360316
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Inorganic materials/Physical properties
Research InstitutionTokyo Institute of Technology

Principal Investigator

FUNAKUBO Hiroshi  東京工業大学, 大学院・総合理工学研究科, 准教授 (90219080)

Co-Investigator(Kenkyū-buntansha) WADA Satoshi  山梨大学, 医学工学総合研究部, 教授 (60240545)
Co-Investigator(Renkei-kenkyūsha) WADA Satoshi  山梨大学, 医学工学総合研究部, 教授 (60240545)
Project Period (FY) 2009 – 2011
Keywords単結晶 / チタン酸ジルコン酸鉛 / 基礎特性
Research Abstract

Fundamental property of Pb(Zr, Ti) O_3 was investigated using high-quality films grown by MOCVD. Orientation dependency and the contribution of non-180°domain on the electrical and electro-mechanical properties were experimentally observed for the first time.

  • Research Products

    (45 results)

All 2012 2011 2010 2009 Other

All Journal Article (20 results) (of which Peer Reviewed: 20 results) Presentation (23 results) Book (1 results) Remarks (1 results)

  • [Journal Article] Non-contact prove method of ferroelectric property estimation of PbTiO_3 based films for micro electro mechanical systems2012

    • Author(s)
      Yoshitaka Ehara, Satoru Utsugi, Mitsumasa Nakajima, Mohamed Tahar, Chentir, Tomokai Yamada, Takashi Iijima, Ken Nishida, Takashi Yamamoto, and Hiroshi Funakubo
    • Journal Title

      J. Mater. Res.

      Volume: (掲載確定)

    • Peer Reviewed
  • [Journal Article] Temperature and Frequency Dependencies of Ferroelectric Properties in Rhombohedral Epitaxial Pb(Zr, Ti) O_3 Films with Perfect(111) Orientations Grown on CaF_2 Substrates2012

    • Author(s)
      Yoshitaka Ehara, Tomoaki Yamada, Takashi Iijima, Valanoor Nagarajan, and Hiroshi Funakubo
    • Journal Title

      Mater. Res. Soc. Symp. Proc.

      Volume: (掲載確定)

    • Peer Reviewed
  • [Journal Article] Spontaneous polarization estimation from the soft mode in strain-free epitaxial polar axis-oriented Pb(Zr, Ti) O_3 thick films with tetragonal symmetry2011

    • Author(s)
      Yoshitaka Ehara, Satoru Utsugi, Mitsumasa Nakajima, Tomoaki Yamada, Takashi Iijima, Hiroki Taniguchi, Mitsuru Itoh, and Hiroshi Funakubo
    • Journal Title

      Appl Phys Lett.

      Volume: 98 Pages: 141914-1-3

    • Peer Reviewed
  • [Journal Article] Enhancement of piezoelectric response in(100)/(001) oriented tetragonal PZT films by controlling tetragonality and volume fraction of the(001) orientation2011

    • Author(s)
      Mitsumasa Nakajima, Syoji Okamoto, Hiroshi Nakaki, Tomoaki Yamada, and Hiroshi Funakubo
    • Journal Title

      J. Appl. Phys.

      Volume: 109 Pages: 091601-1-5

    • Peer Reviewed
  • [Journal Article] TEM Observation on Ferroelectric Domain Structure of PbTiO_3 Epitaxal Films2011

    • Author(s)
      Kenta Aoyagi, Takanori Kiguchi, Yoshitaka Ehara, Hiroshi Funakubo, and Toyohiko Konno
    • Journal Title

      Key Eng. Mater.

      Volume: 485 Pages: 179-182

    • Peer Reviewed
  • [Journal Article] Intrinsic Characteristics of Bi(Zn_<1/2> Ti_<1/2>) O_3-substituted Pb(Zr_<0. 4> Ti_<0. 6>) O_3 Thin Films2011

    • Author(s)
      M. T. Chentir, Yoshitaka Ehara, Y. Sugiyama, Y. Tasaki, H. Ishiwara, and H. Funakubo
    • Journal Title

      Materials Science and Engineering

      Volume: 18 Pages: 092008-1-4

    • Peer Reviewed
  • [Journal Article] Ultrafast switching of ferroelastic nanodomains in bilayered ferroelectric thin films2011

    • Author(s)
      Y. Ehara, S. Yasui, J. Nagata, D. Kan, V. Anbusathaiah, T. Yamada, O. Sakata, H. Funakubo, and V. Nagarajan
    • Journal Title

      Appl. Phys. Lett.

      Volume: 99 Pages: 182906-1-3

    • Peer Reviewed
  • [Journal Article] Configuration and local elastic interaction of ferroelectric domains and misfit dislocation in PbTiO_3/SrTiO_3 epitaxial thin films2011

    • Author(s)
      Takanori Kiguchi, Kenta Aoyagi, Yoshitaka Ehara, Hiroshi Funakubo, Tomoaki Yamada, Noritaka Usami, and Toyohiko J Konno
    • Journal Title

      Sci. Technol. Adv. Mater.

      Volume: 12 Pages: 034413-1-9

    • Peer Reviewed
  • [Journal Article] Diffraction contrast analysis of 90°and 180°ferroelectric domain structures of PbTiO3 thin films2011

    • Author(s)
      Kenta Aoyagi, Takanori Kiguchi, Yoshitaka Ehara, Tomoaki Yamada, Hiroshi Funakubo, and Toyohiko J Konno
    • Journal Title

      Sci. Technol. Adv. Mater.

      Volume: 12 Pages: 0344031-6

    • Peer Reviewed
  • [Journal Article] Determination Factors of Strain-relaxed Complex Domain Structure Observed in Thick Epitaxial Pb(Zr, Ti) O_3 Films2010

    • Author(s)
      Hiroshi Nakaki, Satoru Utsugi, Takashi Fujisawa, Mitsumasa Nakajima, Yoshitaka Ehara, Tomoaki Yamada, Hitoshi Morioka, Toshihiro Ifuku, and Hiroshi Funakubo
    • Journal Title

      Mater. Res. Soc. Symp. Proc.

      Volume: 1199 Pages: 1199-F08-08

    • Peer Reviewed
  • [Journal Article] Geometric Phase Analysis of Nano-Scale Strain Fields Around 90°Domains in PbTiO3/SrTiO3 Epitaxial Thin Film2010

    • Author(s)
      Takanori Kiguchi, Kenta Aoyagi, Toyohiko J. Konno, Satoru Utsugi, Tomoaki Yamada, and Hiroshi Funakubo
    • Journal Title

      Mater. Res. Soc. Symp. Proc.

      Volume: 1199 Pages: 1199-F09-08

    • Peer Reviewed
  • [Journal Article] Orientation control of(001) and(101) in epitaxial tetragonal Pb(Zr, Ti) O_3 films with(100)/(001) and(110)/(101) mixture orientations2010

    • Author(s)
      Satoru Utsugi, Takashi Fujisawa, Yoshitaka Ehara, Tomoaki Yamada, Shintaro Yasui, Mohamed-Tahar Chentir, Hitoshi Morioka, Takashi Iijima, and Hiroshi Funakubo
    • Journal Title

      J. Ceram. Soc. Jpn.

      Volume: 118[ 8] Pages: 627-630

    • Peer Reviewed
  • [Journal Article] Single crystal-like selection rules for unipolar-axis oriented tetragonal Pb(Zr, Ti) O_3 thick epitaxial films2010

    • Author(s)
      Mitsumasa Nakajima, Takashi Fujisawa, Yoshitaka Ehara, Tomoaki Yamada, Hiroshi Funakubo, Hiroshi Naganuma, Soichiro Okamura, Ken Nishida, Takashi Yamamoto, and Minoru Osada
    • Journal Title

      Appl. Phys. Lett.

      Volume: 97 Pages: 111901-1-3

    • Peer Reviewed
  • [Journal Article] Growth of polar axis-oriented tetragonal Pb(Zr, Ti) O3 films on CaF2 substrates with transparent(La_<0. 07> Sr_<0. 93>) SnO_32010

    • Author(s)
      Satoru Utsugi, Yoshitaka Ehara, Hidenori Tanaka, Tomoaki Yamada, Hiroshi Funakubo, and Hiroshi Uchida
    • Journal Title

      J. Crystal Growth

      Volume: 312 Pages: 3127-3130

    • Peer Reviewed
  • [Journal Article] In-situ Raman spectroscopy for characterization of the domain contributions to electrical and piezoelectric responses in Pb(Zr, Ti) O_3 films2010

    • Author(s)
      Mitsumasa Nakajima, Hiroshi Nakaki, Yoshitaka Ehara, Tomoaki Yamada, Ken Nishida, Takashi Yamamoto, Minoru Osada, and Hiroshi Funakubo
    • Journal Title

      Appl. Phys. Lett.

      Volume: 97 Pages: 181907-1-3

    • Peer Reviewed
  • [Journal Article] Investigation of Oxygen vacancies in Micro-patterned PZT Thin Films using Raman spectroscopy2010

    • Author(s)
      Ken Nishida, Minoru Osada, Shintaro Yokoyama, Takafumi Kamo, Takashi Fujisawa, Keisuke Saito, Hiroshi Funakubo, Takashi Katoda, and Takashi Yamamoto
    • Journal Title

      Key Eng. Mater.

      Volume: 421-422 Pages: 135-138

    • Peer Reviewed
  • [Journal Article] Experimental evidence for orientation property of Pb(Zr_<0. 35> Ti_<0. 65>) O_3 by manipulating polar axis angle using CaF_2 substrate2010

    • Author(s)
      Satoru Utsugi, Takashi Fujisawa, Yoshitaka Ehara, Tomoaki Yamada, Masaaki Matsushima, Hitoshi Morioka, and Hiroshi Funakubo
    • Journal Title

      Appl. Phys. Lett.

      Volume: 96 Pages: 1029051-1-3

    • Peer Reviewed
  • [Journal Article] Strain-relaxed structure in(001)/(100)-oriented epitaxial Pb(Zr, Ti) O_3 films grown on(100) SrTiO_3 substrates by metal organic chemical vapor deposition2009

    • Author(s)
      Hiroshi Nakaki, Yong Kwan Kim, Shintaro Yokoyama, Rikyu Ikariyama, Hiroshi Funakubo, Ken Nishida, Keisuke Saito, Hitoshi Morioka, Osami Sakata, Hee Han, and Sunggi Baik
    • Journal Title

      J. Appl. Phys.

      Volume: 105 Pages: 014107-1-5

    • Peer Reviewed
  • [Journal Article] Electric-Field-Induced Transverse Displacement in Pt/Pb(Zr, Ti) O_3 Film/Pt/Si Structure2009

    • Author(s)
      Takashi Yamamoto, Mitsutaka Yamamoto, Ken Nishida, Hiroshi Funakubo, Takashi Iijima, Toru Aiso, and Yasuko Ichikawa
    • Journal Title

      Jpn. J. Appl. Phys.

      Volume: 48 Pages: 09KA04-1-4

    • Peer Reviewed
  • [Journal Article] Composition dependency of epitaxial Pb(Zr, Ti) O_3 films with different film thickness2009

    • Author(s)
      Shintaro Yokoyama, Hiroshi Funakubo, Hitoshi Morioka, Keisuke Saito, Tomoaki Yamada, and Mutsuo Ishikawa
    • Journal Title

      Ferroelectrics

      Volume: 389[ 1] Pages: 10-17

    • Peer Reviewed
  • [Presentation] 分極軸配向エピタキシャルPb(Zr, Ti) O_3膜の強誘電特性2012

    • Author(s)
      江原祥隆・安井伸太郎・及川貴弘・山田智明・飯島高志・坂田修身・舟窪浩
    • Organizer
      日本セラミックス協会2012年年会(招待講演)
    • Place of Presentation
      京都大学吉田キャンパス
    • Year and Date
      20120319-21
  • [Presentation] PbTiO_3薄膜における90°ドメイン底部境界構造の解明2012

    • Author(s)
      木口賢紀、青柳健大、今野豊彦、江原祥隆、舟窪浩
    • Organizer
      第37回セラミックスに関する顕微鏡写真展(日本セラミックス協会2012年年会)(招待講演)
    • Place of Presentation
      京都大学吉田キャンパス
    • Year and Date
      20120319-21
  • [Presentation] MPB近傍PZT圧膜におけるインコメンシュレート相の発見2012

    • Author(s)
      青柳健大・木口賢紀・今野豊彦・和田亜由美・江原祥隆・舟窪浩
    • Organizer
      第37回セラミックスに関する顕微鏡写真展(日本セラミックス協会2012年年会)(招待講演)
    • Place of Presentation
      京都大学吉田キャンパス
    • Year and Date
      20120319-21
  • [Presentation] MPB近傍PZT薄膜の90°ドメインと帯電した菱面体晶ドメイン境界2012

    • Author(s)
      青柳健大・木口賢紀・今野豊彦・和田亜由美・江原祥隆・舟窪浩
    • Organizer
      第37回セラミックスに関する顕微鏡写真展(日本セラミックス協会2012年年会)(招待講演)
    • Place of Presentation
      京都大学吉田キャンパス
    • Year and Date
      20120319-21
  • [Presentation] CaF_2基板上の作製したエピタキシャルPb(Zr, Ti) O_3膜の結晶構造および強誘電特性のZr/(Zr+ Ti)比依存性2012

    • Author(s)
      江原祥隆,安井伸太郎,森岡仁,山田智明,舟窪浩
    • Organizer
      2012年春季第59回応用物理学関係連合講演会(招待講演)
    • Place of Presentation
      早稲田大学早稲田キャンパス
    • Year and Date
      20120315-18
  • [Presentation] Crystal Structure and Ferroelectric property of Epitaxial Rhombonedral Pb(Zr, Ti) O_3 Films2012

    • Author(s)
      Yoshitaka Ehara, Shintaro Yasui, Takahiro Oikawa, Mitsumasa Nakajima, Tomoaki Yamada, and Hiroshi Funakubo
    • Organizer
      Electronic Materials and Applications(EMA) 2012(招待講演)
    • Place of Presentation
      Double Tree by Hilton Orlando at Sea World, Orlando, FL, USA
    • Year and Date
      20120118-20
  • [Presentation] Proving of the Ferroelectric and Piezoelec tricProperties of Pb(Zr, Ti) O_3 Films by Raman Spectroscopy2011

    • Author(s)
      Hiroshi Funakubo, Mitsumasa Nakajima,Yoshitaka Ehara, Ayumi Wada, Tomoaki Yamada, Nobuyasu Mizutani, Takashi Iijima, Hiroki Taniguchi, Mitsuru Itoh,Ken Nishida, Takashi Yamamoto, and Minoru Osada
    • Organizer
      2011 MRS Fall Meeting(招待講演)
    • Place of Presentation
      Hynes Conven tionCenter, Boston, MA, USA
    • Year and Date
      20111128-1202
  • [Presentation] Proving of Strain Relaxation by and under Applying Electric Field in Pb(Zr, Ti) O_3 Thick Films2011

    • Author(s)
      Ayumi Wada, Yoshitaka Ehara, Shintaro Yasui, Mitsumasa Nakajima, Megu Wada, Soichiro Okamura, Ken Nishida, Takashi Yamamoto, Takeshi Kobayashi, Hitoshi Morioka, and Hiroshi Funakubo
    • Organizer
      15th US-Japan Seminar on Dielectric and Piezoelectric Ceramics(招待講演)
    • Place of Presentation
      Shiroyama Kanko Hotel, Kagoshima
    • Year and Date
      20111106-09
  • [Presentation] PbTiO_3厚膜における格子欠陥のTEM解析2011

    • Author(s)
      青柳健大、木口賢紀、今野豊彦、江原祥隆、舟窪浩
    • Organizer
      第31回エレクトロセラミックス研究討論会(招待講演)
    • Place of Presentation
      東京大学駒場IIリサーチキャンパス
    • Year and Date
      20111028-29
  • [Presentation] PbTiO_3薄膜の90°ドメイン境界の構造とミスフィット転位との弾性相互作用2011

    • Author(s)
      木口賢紀、青柳健大、江原祥隆、舟窪浩、山田智明、宇佐美徳隆、今野豊彦
    • Organizer
      第31回エレクトロセラミックス研究討論会(招待講演)
    • Place of Presentation
      東京大学駒場IIリサーチキャンパス
    • Year and Date
      20111028-29
  • [Presentation] 積層欠陥を含むPbTiO_3厚膜の組織解析2011

    • Author(s)
      青柳健大、兒玉裕美子、木口賢紀、宇佐美徳隆、今野豊彦、江原祥隆、舟窪浩、山田智明
    • Organizer
      日本セラミックス協会第24回秋季シンポジウム(招待講演)
    • Place of Presentation
      北海道大学、札幌キャンパス
    • Year and Date
      20110907-09
  • [Presentation] ミスフィット転位との弾性相互作用によるPbTiO_3薄膜90°ドメインの核生成・成長メカニズム2011

    • Author(s)
      木口賢紀、青柳健大、江原祥隆、舟窪浩、山田智明、宇佐美徳隆、今野豊彦
    • Organizer
      日本セラミックス協会第24回秋季シンポジウム(招待講演)
    • Place of Presentation
      北海道大学、札幌キャンパス
    • Year and Date
      20110907-09
  • [Presentation] 菱面体晶Pb(Zr, Ti) O_3エピタキシャル膜の結晶構造と強誘電特性2010

    • Author(s)
      江原祥隆、宇津木覚、中島光雅、山田智明、飯島高志、舟窪浩
    • Organizer
      第71回応用物理学会学術講演会
    • Place of Presentation
      長崎大学文教キャンパス(長崎市)
    • Year and Date
      20100914-17
  • [Presentation] Domain Density Control of PZT Thick Films and Their Piezoelectricity Enhancement2010

    • Author(s)
      Hiroshi Funakubo, Mitsumasa Nakajima, Satoru Utsugi, Yoshitaka Ehara, Hiroshi Nakaki, Tomoaki Yamada, and Hitoshi Morioka
    • Organizer
      The 8th Japan-Korea Conference on Ferroelectrics(JKC-FE08)
    • Place of Presentation
      Egret Himeji, Himeji, Japan
    • Year and Date
      20100803-06
  • [Presentation] 歪みの少ないエピタキシャル正方晶分極軸配向Pb(Zr, Ti) O_3厚膜を用いたソフトモードによる強誘電性の見積もり2010

    • Author(s)
      江原祥隆、宇津木覚、中島光雅、山田智明、舟窪浩、飯島高志、木口賢紀、今野豊彦
    • Organizer
      第27回強誘電体応用会議(FMA-27)
    • Place of Presentation
      コープイン京都(京都市)
    • Year and Date
      20100526-29
  • [Presentation] Enhancement of Piezoelectric response in tetragonal Pb(Ti, Zr) O_3 thick films by 90°-domain wall density control2010

    • Author(s)
      Hiroshi Funakubo, Mitsumasa Nakajima, Hiroshi Nakaki, Tomoaki Yamada and Hitoshi Morioka
    • Organizer
      2010 U. S. Navy Workshop on Acoustic Transduction Materials and Devices
    • Place of Presentation
      The Penn State Conference Center Hotel, State College, Pennsylvania, USA
    • Year and Date
      20100511-13
  • [Presentation] PbTiO_3/SrTiO_3薄膜における90°ドメイン構造の歪み場イメージング2010

    • Author(s)
      木口賢紀、青柳健大、今野豊彦、宇津木覚、山田智明、舟窪浩
    • Organizer
      日本セラミックス協会2010年年会
    • Place of Presentation
      東京農工大
    • Year and Date
      2010-03-22
  • [Presentation] 幾何学的位相解析によるPbTiO_3薄膜90ドメインの局所歪み場解析2010

    • Author(s)
      木口賢紀、今野豊彦、青柳健大、宇津木覚、山田智明、舟窪浩
    • Place of Presentation
      東海大学
    • Year and Date
      2010-03-19
  • [Presentation] CaF_2基板上の作製した菱面体組成エピタキシャルPb(Zr, Ti) O_3膜の結晶構造および強誘電特性2010

    • Author(s)
      江原祥隆、宇津木覚、中島光雅、森岡仁、山田智明、舟窪浩
    • Organizer
      2010年春季第57回応用物理学関係連合講演会
    • Place of Presentation
      東海大学
    • Year and Date
      2010-03-18
  • [Presentation] 分極軸単一配向した歪みの少ないエピタキシャル正方晶Pb(Zr, Ti) O_3厚膜を用いたソフトモードによる強誘電性の見積もり2010

    • Author(s)
      江原祥隆、宇津木覚、中島光雅、山田智明、飯島高志、舟窪浩
    • Organizer
      2010年春季第57回応用物理学関係連合講演会
    • Place of Presentation
      東海大学
    • Year and Date
      2010-03-17
  • [Presentation] (001),(101),(111)-Single-oriented Epitaxial Pb(Zr, Ti) O_3 Films Grown on CaF_2 Substrates and their Characterization2009

    • Author(s)
      Satoru Utsugi, Takashi Fujisawa, Yoshitaka Ehara, Tomoaki Yamada, Shintaro Yasui, Hitoshi Morioka, Takashi Iijima, and Hiroshi Funakubo
    • Organizer
      2009 MRS Fall Meeting
    • Place of Presentation
      Hynes Convention Center and Sheraton Boston Hotel, Boston, MA, U. S. A
    • Year and Date
      2009-11-30
  • [Presentation] Characterization of Tetragonal and Rhombohedral Pb(Zr, Ti) O_3 Phase in MPB Using Raman Spectroscopy-In-depth profile of Volume Fraction on Epitaxial Pb(Zr, Ti) O_3 Thick Films2009

    • Author(s)
      Masamichi Nishide, Hiroshige Takeuchi, Ken Nishida, Takashi Yamamoto, Shintaro Yokoyama, Shintaro Yasui, Hiroshi Funakubo, and Takashi Katoda
    • Organizer
      ISIF^2 2009
    • Place of Presentation
      Antlers Hilton Colorado Springs, Colorado Springs, CO, USA.
    • Year and Date
      2009-09-29
  • [Presentation] CaF_2基板上に作製したエピタキシャルPb(Zr, Ti) O_3膜の強誘電特性の組成依存2009

    • Author(s)
      江原祥隆、宇津木覚、中島光雅、森岡仁、山田智明、舟窪浩
    • Organizer
      2009年秋季第70回応用物理学会学術講演会
    • Place of Presentation
      富山大学
    • Year and Date
      2009-09-11
  • [Book] edited by Mickael Lallert, Chapter 12,"Change of CrystalStructure and Electrical Propertieswith Zr/(Zr+ Ti) Ratio for Epitaxial Pb(Zr, Ti) O_3 films Grown on(100) cSrRuO_3//(100) SrTiO_3 Substrates by Metal Organic Chemical VaporDeposition"2011

    • Author(s)
      Chentir Mohamed-Tahar, Hitoshi Morioka, Keisuke Saito, Yoshitaka Ehara, Shintaro Yokoyama Takahiro Oikawa, andHiroshi Funakubo
    • Total Pages
      229-244
    • Publisher
      INTECH,"Ferroelectrics, Characterization andModeling"
  • [Remarks]

    • URL

      http://f-lab.iem.titech.ac.jp/f-lab.htm

URL: 

Published: 2013-07-31  

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