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2011 Fiscal Year Final Research Report

Establishment of element-specific coherent X-ray diffraction microscopy and 4D nano-meso structural analysis of metallic materials

Research Project

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Project/Area Number 21686060
Research Category

Grant-in-Aid for Young Scientists (A)

Allocation TypeSingle-year Grants
Research Field Physical properties of metals
Research InstitutionOsaka University

Principal Investigator

TAKAHASHI Yukio  大阪大学, 大学院・工学研究科, 准教授 (00415217)

Project Period (FY) 2009 – 2011
KeywordsコヒーレントX線光学 / X線顕微鏡 / 金属ナノ組織解析
Research Abstract

Element-specific high-resolution coherent X-ray diffraction microscopy with energy-tunable X-ray focusing mirrors has been developed at SPring-8 that is the third-generation synchrotron radiation facility and has been applied to nano-meso structural analysis of functional metallic nanoparticles. 2 nm resolution, which is the world record of the spatial resolution of X-ray microscopy, has been achieved at the measurements of a Ag nanocube particle. Three-dimensional electron density mapping of a Au/ Ag nanobox particle has been visualized. In addition, large-field-of-view imaging has been also realized by extending to a scanning scheme.

  • Research Products

    (39 results)

All 2012 2011 2010 2009 Other

All Journal Article (9 results) (of which Peer Reviewed: 9 results) Presentation (29 results) Remarks (1 results)

  • [Journal Article] Multiscale element mapping of buried structures by ptychographic x-ray diffraction microscopy using anomalous scattering2011

    • Author(s)
      Y. Takahashi, A. Suzuki, N. Zettsu, Y. Kohmura, K. Yamauchi and T. Ishikawa
    • Journal Title

      Appl. Phys. Lett.

      Volume: 99 Pages: 131905

    • Peer Reviewed
  • [Journal Article] Towards High-Resolution Ptychographic X-ray Diffraction Microscopy2011

    • Author(s)
      Y. Takahashi, A. Suzuki, N. Zettsu, Y. Kohmura, Y. Senba, H. Ohashi, K. Yamauchi and T. Ishikawa
    • Journal Title

      Phys. Rev. B

      Volume: 83 Pages: 214109

    • Peer Reviewed
  • [Journal Article] High-Resolution Projection Image Reconstruction of Thick Objects by Hard X-ray Diffraction Microscopy2010

    • Author(s)
      Y. Takahashi, Y. Nishino, R. Tsutsumi, N. Zettsu, E. Matsubara, K. Yamauchi and T. Ishikawa
    • Journal Title

      Phys. Rev. B

      Volume: 82 Pages: 214102

    • Peer Reviewed
  • [Journal Article] Three-dimensional electron density mapping of shape-controlled nanoparticle by focused hard x-ray diffraction microscopy2010

    • Author(s)
      Y. Takahashi, N. Zettsu, Y. Nishino, R. Tsutsumi, E. Matsubara, T. Ishikawa and K. Yamauchi
    • Journal Title

      Nano Lett.

      Volume: 10 Pages: 1922-1926

    • Peer Reviewed
  • [Journal Article] Two-dimensional measurement of focused x-ray beam profile using coherent x-ray diffraction of isolated nanoparticle2010

    • Author(s)
      Y. Takahashi, H. Kubo, R. Tsutsumi, S. Sakaki, N. Zettsu, Y. Nishino, T. Ishikawa and K. Yamauchi
    • Journal Title

      Nuclear Instruments and Methods in Physics Research Section A : Accelerators, Spectrometers, Detectors and Associated Equipment

      Volume: 616 Pages: 266-269

    • Peer Reviewed
  • [Journal Article] An experimental procedure for precise evaluation of electron density distribution of a nanostructured material by coherent x-ray diffraction microscopy2010

    • Author(s)
      Y. Takahashi, H. Kubo, Y. Nishino, H. Furukawa, R. Tsutsumi, K. Yamauchi, T. Ishikawa and E. Matsubara
    • Journal Title

      Rev. Sci. Instrum.

      Volume: 81 Pages: 03707

    • Peer Reviewed
  • [Journal Article] High-Resolution Diffraction Microscopy Using the Plane-Wave Field of a Nearly Diffraction-Limited Focusing X ray2009

    • Author(s)
      Y. Takahashi, Y. Nishino, R. Tsutsumi, H. Kubo, H. Furukawa, H. Mimura, S. Matsuyama, N. Zettsu, E. Matsubara, T. Ishikawa and K. Yamauchi
    • Journal Title

      Phys. Rev. B

      Volume: 80 Pages: 054103

    • Peer Reviewed
  • [Journal Article] Observation of electromigration voids in a Cu thin line by in situ coherent x-ray diffraction microscopy2009

    • Author(s)
      Y. Takahashi, Y. Nishino, H. Furukawa, H. Kubo, K. Yamauchi, T. Ishikawa and E. Matsubara
    • Journal Title

      J. Appl. Phys.

      Volume: 105 Pages: 124911

    • Peer Reviewed
  • [Journal Article] Feasibility study of high-resolution coherent diffraction microscopy using synchrotron x rays focused by Kirkpatrick-Baez mirrors2009

    • Author(s)
      Y. Takahashi, Y. Nishino, H. Mimura, R. Tsutsumi, H. Kubo, T. Ishikawa and K. Yamauchi
    • Journal Title

      J. Appl. Phys.

      Volume: 105 Pages: 083106

    • Peer Reviewed
  • [Presentation] X線集光ビームを利用したコヒーレント回折技術の開発と応用2012

    • Author(s)
      高橋幸生
    • Organizer
      アモルファス・ナノ材料第147委員会第112回研究会
    • Place of Presentation
      弘済会館
    • Year and Date
      2012-05-27
  • [Presentation] コヒーレントX線回折による構造可視化の新手法2012

    • Author(s)
      高橋幸生
    • Organizer
      多元物質科学研究所若手交流研究会
    • Place of Presentation
      東北大学多元物質科学研究所
    • Year and Date
      2012-02-24
  • [Presentation] What lies beneath : mapping hidden nanostructures2012

    • Organizer
      RIKEN Research
    • Year and Date
      2012-02-10
  • [Presentation] 高分解能コヒーレントX線回折顕微法の現状と将来展望2012

    • Author(s)
      高橋幸生
    • Organizer
      日本顕微鏡学会の電顕技術開発若手研究部会ワークショップ「様々なイメージング技術の現況と展望」
    • Place of Presentation
      名古屋ファインセラミックスセンター
    • Year and Date
      2012-01-05
  • [Presentation] 高分解能走査型コヒーレントX線回折顕微法の開発と金属材料のナノ組織解析への応用2011

    • Author(s)
      鈴木明大、高橋幸生、山内和人、是津信行、香村芳樹、石川哲也
    • Organizer
      優秀ポスター賞
    • Place of Presentation
      日本金属学会
    • Year and Date
      2011-11-08
  • [Presentation] 高分解能走査型コヒーレントX線回折顕微法の開発と金属材料のナノ組織解析への応用2011

    • Author(s)
      鈴木明大、高橋幸生、山内和人、是津信行、香村芳樹、石川哲也
    • Organizer
      日本金属学会秋期大会
    • Place of Presentation
      沖縄コンベンションセンター
    • Year and Date
      2011-11-07
  • [Presentation] 物質中の電子密度や特定元素の分布観察大視野・高分解能X線顕微鏡阪大、名大、理研の研究グループ開発2011

    • Organizer
      科学新聞
    • Year and Date
      2011-10-14
  • [Presentation] High-resolution coherent diffraction imaging using focused hard x-ray beam at SPring-82011

    • Author(s)
      Y. Takahashi, A. Suzuki, Y. Kohmura, Y. Nishino, K. Yamauchi and Tetsuya Ishikawa
    • Organizer
      CXS Annual Workshop 2011
    • Place of Presentation
      Bio21 Institute Melbourne, Victoria, Australia
    • Year and Date
      2011-10-10
  • [Presentation] 元素識別が可能に大視野、高分解能X線顕微鏡を開発阪大など2011

    • Organizer
      化学工業日報
    • Year and Date
      2011-10-03
  • [Presentation] 大視野で高空間分解能阪大などがX線顕微鏡2011

    • Organizer
      日刊工業新聞
    • Year and Date
      2011-10-03
  • [Presentation] 原子見分ける顕微鏡阪大・理研など開発2011

    • Organizer
      読売新聞
    • Year and Date
      2011-09-29
  • [Presentation] Development and application of high-resolution diffraction microscopy using focused hard x-ray beam2011

    • Author(s)
      Y. Takahashi
    • Organizer
      The 4th International Workshop on FEL Science
    • Place of Presentation
      Peppers Beach Club and Spa, Palm Cove, Cairns, Queensland, Australia
    • Year and Date
      2011-09-01
  • [Presentation] Development of high-resolution coherent X-ray diffraction microscopy and its application in materials science2011

    • Author(s)
      Y. Takahashi
    • Organizer
      International conference on processing & manufacturing of advanced materials
    • Place of Presentation
      Quebec city convention centre, Quebec, Canada
    • Year and Date
      2011-08-03
  • [Presentation] コヒーレントX線散乱イメージング技術の開発と応用の研究2011

    • Author(s)
      高橋幸生
    • Organizer
      文部科学大臣表彰若手科学者賞(科学技術部門)
    • Place of Presentation
      文部科学省
    • Year and Date
      2011-04-20
  • [Presentation] 高分解能コヒーレントX線回折顕微法による金銀ナノボックス粒子の三次元電子密度マッピング2011

    • Author(s)
      高橋幸生、是津信行、西野吉則、堤良輔、松原英一郎、石川哲也、山内和人
    • Organizer
      第61回金属組織写真賞奨励賞(顕微鏡関連部門)
    • Place of Presentation
      日本金属学会
    • Year and Date
      2011-03-25
  • [Presentation] 試料厚さの効果を考慮した高分解能コヒーレントX線回折顕微法2011

    • Author(s)
      高橋幸生、堤良輔、西野吉則、是津信行、松原英一郎、山内和人、石川哲也
    • Organizer
      第24回日本放射光学会年会
    • Place of Presentation
      エポカルつくば
    • Year and Date
      2011-01-08
  • [Presentation] Development and application of high-resolution X-ray diffraction microscopy using advanced mirror optics2010

    • Author(s)
      Y. Takahashi
    • Organizer
      International Global COE Symposium on Atomically Controlled Fabrication Technology 2010
    • Place of Presentation
      Osaka University Nakanoshima Center, Osaka, Japan
    • Year and Date
      2010-11-24
  • [Presentation] 高分解能コヒーレントX線回折顕微法による金属ナノ粒子の三次元電子密度マッピング2010

    • Author(s)
      高橋幸生、是津信行、堤良輔、山内和人、西野吉則、石川哲也、松原英一郎
    • Organizer
      日本金属学会秋期大会
    • Place of Presentation
      北海道大学
    • Year and Date
      2010-09-25
  • [Presentation] Development and application of high-resolution diffraction microscopy using focused hard X-ray beam2010

    • Author(s)
      Y. Takahashi, Y. Nishino, E. Matsubara, T. Ishikawa and Kazuto Yamauchi
    • Organizer
      the 10th International Conference of X-ray Microscopy
    • Place of Presentation
      chicago, illinois, USA
    • Year and Date
      2010-08-16
  • [Presentation] Development of coherent x-ray diffraction microscopy and its application in materials science2010

    • Author(s)
      Y. Takahashi
    • Organizer
      The 7th International Conference on Synchrotron Radiation in Materials Science
    • Place of Presentation
      Oxford, UK
    • Year and Date
      2010-07-12
  • [Presentation] 10ナノのくぼみはっきり新型のX線顕微鏡阪大グループ開発2010

    • Organizer
      朝日新聞
    • Year and Date
      2010-05-11
  • [Presentation] X線顕微鏡観察精度10ナノ以下阪大などSPring-8活用2010

    • Organizer
      日経産業新聞
    • Year and Date
      2010-04-21
  • [Presentation] Development of coherent x-ray diffraction microscopy and its application in materials science2010

    • Author(s)
      Y. Takahashi
    • Organizer
      TMS annual meeting
    • Place of Presentation
      Seattle, Washington, USA
    • Year and Date
      2010-02-16
  • [Presentation] 2010 JIM/ TMS Young Leader International Scholar2010

    • Author(s)
      Y. Takahashi
    • Organizer
      The Minerals, Metals & Materials Society The Minerals, Metals & Materials Society
    • Year and Date
      2010-02-14
  • [Presentation] コヒーレントX線散乱・回折イメージング技術の開発と応用2010

    • Author(s)
      高橋幸生
    • Organizer
      第14回日本放射光学会奨励賞
    • Place of Presentation
      日本放射光学会
    • Year and Date
      2010-01-07
  • [Presentation] コヒーレントX線回折・散乱イメージング技術の開発とその応用2010

    • Author(s)
      高橋幸生
    • Organizer
      第23回日本放射光学会年会
    • Place of Presentation
      イーグレ姫路
    • Year and Date
      2010-01-06
  • [Presentation] Development and application of coherent x-ray diffraction microscopy at SPring-82009

    • Author(s)
      Y. Takahashi
    • Organizer
      X-ray coherent diffraction" Workshop & XFEL Meeting, SOLEIL Synchrotron facility
    • Place of Presentation
      France
    • Year and Date
      2009-12-14
  • [Presentation] 硬X線集光ビームを用いた高分解能回折顕微法の開発2009

    • Author(s)
      高橋幸生
    • Organizer
      第10回X線結像光学シンポジウム
    • Place of Presentation
      つくばエポカル
    • Year and Date
      2009-11-07
  • [Presentation] 集光X線を利用した高分解能回折顕微法の開発2009

    • Author(s)
      高橋幸生
    • Organizer
      日本放射光学会第一回若手研究会「X線ナノ集光技術研究会」
    • Place of Presentation
      大阪大学
    • Year and Date
      2009-08-10
  • [Remarks]

    • URL

      http://www-up.prec.eng.osaka-u.ac.jp/takahashi/

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Published: 2013-07-31  

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