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2012 Fiscal Year Final Research Report

Development of in-situ X-ray absorption laboratory spectrometer for aqueous metal complexes

Research Project

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Project/Area Number 22550088
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Analytical chemistry
Research InstitutionFukuoka University

Principal Investigator

KURISAKI Tsutomu  福岡大学, 理学部, 助教 (20268973)

Project Period (FY) 2010 – 2012
KeywordsX 線吸収分光法 / 溶存構造 / 金属錯体 / 装置開発
Research Abstract

We started to design and develop our laboratory measurement system for X-ray absorption spectrometer. This spectrometer consists of small X-ray tube, SDD detector and laptop computer. The spectrometer is covered with lead glass case, and X-rays from the tube are shielded with the case at the time of measurement. We performed the spectrum measurement of synthesized copper complexes. The measured spectra analyzed by a DV-Xα method.

  • Research Products

    (19 results)

All 2013 2012 2011 2010

All Journal Article (8 results) (of which Peer Reviewed: 8 results) Presentation (11 results)

  • [Journal Article] Bromo(1,4,7,10,13-pentaazacyclohexa decane)cobalt(III) Bromide2013

    • Author(s)
      T. Kurisaki, M. Hamano, H. Wakita
    • Journal Title

      Dihydrate, Acta Cryst. E

      Volume: 69 Pages: 179-180

    • DOI

      DOI:10.1107/S1600536813004947

    • Peer Reviewed
  • [Journal Article] Visible-light photocatalysis with phosphorus-doped titanium(IV) oxide particlesprepared using a phosphide compound2013

    • Author(s)
      M. Iwase, K. Yamada, T. Kurisaki
    • Journal Title

      Applied Catalysis B

      Volume: 132-133 Pages: 39-44

    • DOI

      DOI:10.1016/j.apcatb.2012.11.014

    • Peer Reviewed
  • [Journal Article] Characterization and photocatalytic activity of nitrogen-doped titanium(IV) oxide prepared by doping titania with TiN powder2013

    • Author(s)
      M. Iwase, K. Yamada, T. Kurisaki, H.Wakita
    • Journal Title

      Applied Catalysis A

      Volume: 455 Pages: 86-91

    • DOI

      DOI:10.1016/j.apcata.2013.01.016

    • Peer Reviewed
  • [Journal Article] The Surface Analysis of Ionic Liquids Using X-ray Photoelectron Spectroscopy2012

    • Author(s)
      T.Kurisaki, D. Tanaka
    • Journal Title

      J. Phys. Chem. B

      Volume: 116 Pages: 10870-10875

    • DOI

      DOI:10.1021/jp301658k

    • Peer Reviewed
  • [Journal Article] 軟X線吸収分光法を用いた水溶液中のナトリウムおよびマグネシウムイオンの溶存構造解析2012

    • Author(s)
      栗崎敏、三木祐典
    • Journal Title

      福岡大学理学集報

      Volume: 42(1) Pages: 29-35

    • Peer Reviewed
  • [Journal Article] 軟X線吸収分光法による固体および溶液中の軽元素の状態分析2011

    • Author(s)
      栗崎敏、三木祐典
    • Journal Title

      X線分析の進歩

      Volume: 42 Pages: 281-290

    • Peer Reviewed
  • [Journal Article] 新規リンドープ酸化チタンのXRD・XPSによる解析2011

    • Author(s)
      岩瀬元希、藤尾侑輝、長濱俊、山田啓二、栗崎敏、脇田久伸
    • Journal Title

      X線分析の進歩

      Volume: 42 Pages: 213-219

    • Peer Reviewed
  • [Journal Article] 軟X線分光スペクトル測定装置用生体試料測定システムの設計・開発・性能評価2010

    • Author(s)
      栗崎敏、迫川泰幸、松尾修司、脇田久伸
    • Journal Title

      X線分析の進歩

      Volume: 41 Pages: 165-170

    • Peer Reviewed
  • [Presentation] 各種トリアザ環銅錯体の溶存構造と触媒能との相関2012

    • Author(s)
      栗崎敏、横山尚平、常住勇弥、脇田久伸
    • Organizer
      日本分析化学会第61年会金沢
    • Place of Presentation
      金沢
    • Year and Date
      2012-09-21
  • [Presentation] DV-Xα法を用いた軽金属イオンの溶存構造解析2012

    • Author(s)
      栗崎敏、脇田久伸
    • Organizer
      第25回DV-Xα研究会
    • Place of Presentation
      福岡
    • Year and Date
      2012-08-06
  • [Presentation] 軟X線吸収分光法を用いた塩化ナトリウムおよび臭化ナトリウム水溶液中のナトリウムイオンの溶存構造解析2012

    • Author(s)
      栗崎敏、南慧多、横山尚平、岩瀬元希、脇田久伸
    • Organizer
      第72回分析化学討論会
    • Place of Presentation
      鹿児島
    • Year and Date
      2012-05-20
  • [Presentation] ポリキャピラリー集光レンズを導入した生体試料測定システムを用いる水溶液中の軽金属イオンの溶存構造解析2011

    • Author(s)
      栗崎敏,横山尚平、南慧多、岩瀬元希、脇田久伸
    • Organizer
      第47回X線分析討論会
    • Place of Presentation
      福岡
    • Year and Date
      2011-10-29
  • [Presentation] The Characterization of Light Element Ions in Aqueous Solution by Soft X-ray Absorption Spectral Measurement Apparatus using Polycapillary X-ray Optics2011

    • Author(s)
      T. Kurisaki、Y. Sakogawa, Y. Miki, S.Kokubu, K. Minami, S. Yokoyama, and H. Wakita
    • Organizer
      International Congress on Analytical Sciences 2011
    • Place of Presentation
      京都
    • Year and Date
      2011-05-24
  • [Presentation] X-ray absorption spectroscopic characterization of Phosphorus-doped TiO2 with visible-light photocatalytic activity2010

    • Author(s)
      M. Iwase, K. Yamada, T. Kurisaki, H.Wakita
    • Organizer
      Pacifichem
    • Place of Presentation
      Honolulu、USA
    • Year and Date
      2010-12-19
  • [Presentation] Characterization of minerals and archeological samples by soft X-ray spectroscopy2010

    • Author(s)
      T. Kurisaki, D. Tanaka, S. Kokubu, H.Wakita
    • Organizer
      Pacifichem
    • Place of Presentation
      Honolulu、USA
    • Year and Date
      2010-12-18
  • [Presentation] X線吸収スペクトル測定装置の開発と各種金属イオンおよび金属錯体の溶存構造解析2010

    • Author(s)
      栗崎敏
    • Organizer
      第46回X線分析討論会
    • Place of Presentation
      広島
    • Year and Date
      2010-10-22
  • [Presentation] Characterization of Light Element Ions in Aqueous Solution by Soft X-ray Absorption Spectroscopy using Liquid Cell System2010

    • Author(s)
      T. Kurisaki、Y. Sakogawa、H. Wakita
    • Organizer
      6th International Conference on DV-Xα and the 23rd DV-Xα Annual Meeting
    • Place of Presentation
      Daejeon、Korea
    • Year and Date
      2010-08-04
  • [Presentation] Electronic Structure of Phosphorus-doped TiO2with visible-light photocatalytic activity2010

    • Author(s)
      M. Iwase, S. Kokubu, K. Yamada, T.Kurisaki, H. Wakita
    • Organizer
      6th International Conference on DV-Xα and the 23rd DV-Xα Annual Meeting
    • Place of Presentation
      Daejeon、Korea
    • Year and Date
      2010-08-04
  • [Presentation] Characterization of Iron Slags and Lump Found from Reverberatory Furnace Vacant Lot by X-ray Absorption Spectroscopy (2)2010

    • Author(s)
      S. Kokubu, T. Kurisaki, H. Wakita
    • Organizer
      6th International Conference on DV-Xα and the 23rdDV-Xα Annual Meeting
    • Place of Presentation
      Daejeon、Korea
    • Year and Date
      2010-08-04

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Published: 2014-08-29  

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