2012 Fiscal Year Final Research Report
Automatic separation technique of ultra-trace multi-elements to analyze the origin of trace environmental materials
| Project/Area Number |
22550143
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| Research Category |
Grant-in-Aid for Scientific Research (C)
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| Allocation Type | Single-year Grants |
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| Section | 一般 |
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| Research Field |
Environmental chemistry
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| Research Institution | Japan Atomic Energy Agency |
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Principal Investigator |
MIYAMOTO Yutaka 独立行政法人日本原子力研究開発機構, 原子力基礎工学研究部門, 研究副主幹 (60219821)
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| Co-Investigator(Renkei-kenkyūsha) |
YASUDA Kenichiro 独立行政法人日本原子力研究開発機構, 原子力基礎工学研究部門, 研究副主幹 (20354871)
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| Project Period (FY) |
2010 – 2012
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| Keywords | ミクロ化学手法 / イオン交換分離 / 環境試料 / ウラン / 鉛 / トリウム |
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| Research Abstract |
The objective of this study is to develop an automatic separation technique of ultra-trace multi-elements. The experimental conditions of sequential separation with a single anion-exchange column were optimized. An automatic separation system was assembled. A reference environmental sample was separated and quantitatively analyzed with the optimized system, and the features of this system were evaluated. The elements of interest were sequentially and completely separated within 6 hours. The chemical recovery yield was more than 95%. This evaluation suggests that a sample in more than 500 micro grams (equivalent to several micro meters in diameter) of sample can be analyzed.
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