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2012 Fiscal Year Final Research Report

Understanding of the high-speed sintering mechanisms and improvement of the technical construction in the pulsed-current-sintering (PCS) processing

Research Project

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Project/Area Number 22560675
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Inorganic materials/Physical properties
Research InstitutionNational Institute for Materials Science

Principal Investigator

MORITA Koji  独立行政法人物質・材料研究機構, 先端材料プロセスユニット, 主幹研究員 (20354186)

Co-Investigator(Renkei-kenkyūsha) KIM Byung-nam  独立行政法人物質・材料研究機構, 先端材料プロセスユニット, 主席研究員 (50254149)
SAKKA Yoshio  独立行政法人物質・材料研究機構, 先端材料プロセスユニット, ユニット長 (00354217)
Project Period (FY) 2010 – 2012
Keywordsパルス通電焼結 / 構造用セラミックス / スピネル / 透光性
Research Abstract

In order to achieve an advanced pulsed-current-sintering (PCS) technique, this work was performed to understand the sintering mechanisms and to clarify the effect of the sintering parameters, such as heating rate, sintering temperature, dwelling time, loading schedule and so on, on PCS processing of MgAl2O4 spinel. It is found that the sintering behavior changes sensitively with the parameters and dense fine-grained ceramics can be fabricated by carefully optimizing the parameters. Loading at high temperatures, for example, can attain high density spinel even at a high heating rate of 100°C/min, and hence, can save the total processing time.

  • Research Products

    (26 results)

All 2013 2012 2011 2010

All Journal Article (13 results) (of which Peer Reviewed: 13 results) Presentation (13 results)

  • [Journal Article] Development of high-strain-rate superplastic oxide ceramics based on flow mechanism2013

    • Author(s)
      K. Morita, B.-N. Kim, H. Yoshida, Y. Sakka and K. Hiraga
    • Journal Title

      Mat. Sci. Forum

      Volume: 735 Pages: 9-14

    • Peer Reviewed
  • [Journal Article] Effect of Loading Schedule on Densification of MgAl_2O_4 Spinel during Spark Plasma Sintering (SPS) Processing2012

    • Author(s)
      K. Morita, B.-N. Kim, H. Yoshida, H. Zhang, K. Hiraga and Y. Sakka
    • Journal Title

      J Eur. Ceram. Soc.,

      Volume: 32 Pages: 2303-2309

    • Peer Reviewed
  • [Journal Article] Optical Properties and Microstructure of Nanocrystalline Cubic Zirconia Prepared by High-Pressure Spark Plasma Sintering2011

    • Author(s)
      H. Zhang, B.-N. Kim, K. Morita, H. Yoshida, J. Lim, K. Hiraga
    • Journal Title

      J. Am. Ceram. Soc.

      Volume: 94 Pages: 2981-2986

    • Peer Reviewed
  • [Journal Article] Diffusive model of pore shrinkage in final-stage sintering under hydrostatic pressure2011

    • Author(s)
      B.-N. Kim, K. Hiraga, K. Morita, H. Yoshida and H. Zhang
    • Journal Title

      Acta Mater

      Volume: 59[10] Pages: 4079-4087

    • Peer Reviewed
  • [Journal Article] Highly Infrared Transparent Nanometric Tetragonal Zirconia Prepared by High-Pressure Spark Plasma Sintering2011

    • Author(s)
      H. Zhang, Z. Li, B.-N. Kim, K. Morita, H. Yoshida, K. Hiraga, Y. Sakka and J. Blendell
    • Journal Title

      J. Am. Ceram. Soc.

      Volume: 94[9] Pages: 2739-2741

    • Peer Reviewed
  • [Journal Article] Fabrication of Transparent Yttria by High-Pressure Spark Plasma Sintering2011

    • Author(s)
      H. Zhang, B.-N. Kim, K. Morita, H. Yoshida, K. Hiraga, Y. Sakka and J. Ballato
    • Journal Title

      J. Am. Ceram. Soc.

      Volume: 94[10] Pages: 3206-3210

    • Peer Reviewed
  • [Journal Article] Effects of Preheating of Powder Before Spark Plasma Sintering of Transparent MgAl2O4 Spinel2010

    • Author(s)
      B.-N. Kim, K. Morita, J.-H. Lim, K. Hiraga, H. Yoshida
    • Journal Title

      J. Am. Ceram. Soc.

      Volume: 93[8] Pages: 158-2160

    • Peer Reviewed
  • [Journal Article] Light scattering in MgO-doped alumina fabricated by spark plasma sintering2010

    • Author(s)
      B.-N. Kim, K. Hiraga, K. Morita, H. Yoshida and Y. Kagawa
    • Journal Title

      Acta Mater

      Volume: 58[13] Pages: 4527-4535

    • Peer Reviewed
  • [Journal Article] Densification behavior of a fine- grained MgAl_2O_4 spinel during spark plasma sintering (SPS)2010

    • Author(s)
      K. Morita, B.-N. Kim, H. Yoshida and K. Hiraga
    • Journal Title

      Scripta Mater

      Volume: 63[6] Pages: 565-568

    • Peer Reviewed
  • [Journal Article] Optimization of high-pressure sintering of transparent zirconia with nano-sized grains2010

    • Author(s)
      H. B. Zhang, B.-N. Kim, K. Morita, H. Yoshida, J.-H. Lim and K. Hiraga
    • Journal Title

      J. Alloy. Compd.

      Volume: 508[1] Pages: 196-199

    • Peer Reviewed
  • [Journal Article] Spark-Plasma-Sintering (SPS) Processing of High Strength Transparent MgAl2O4 Spinel Polycrystals2010

    • Author(s)
      K. Morita, B.-N. Kim, H. Yoshida, K. Hiraga
    • Journal Title

      PACRIM8 2009 Meeting, Ceram. Trans

      Volume: 212 Pages: 19-29

    • Peer Reviewed
  • [Journal Article] High-Strain-Rate Superplastic Flow Mechanism in ZrO2-30vol% Spinel Two-Phase Composite2010

    • Author(s)
      K. Morita, K. Hiraga, B.-N. Kim, H. Yoshida
    • Journal Title

      Key Eng. Mat.

      Volume: 433 Pages: 333-338

    • Peer Reviewed
  • [Journal Article] Densification Behavior in Spark-Plasma-Sintering of MgAl2O4 Spinel2010

    • Author(s)
      K. Morita, B.-N. Kim, H. Yoshida, K. Hiraga
    • Journal Title

      Mat. Sci. Forum

      Volume: 654-656 Pages: 1986-1989

    • Peer Reviewed
  • [Presentation] Fabrication of Transparent MgAl2O4 Spinel using Pulsed-Current-Sintering (PCS) Processing2013

    • Author(s)
      K. Morita, B.-N. Kim, H. Yoshida, Z. Zhang, Y. Sakka, K. Hiraga
    • Organizer
      Seminar in KIMS
    • Place of Presentation
      Changwon Korea
    • Year and Date
      2013-05-27
  • [Presentation] ジルコニアセラミックスの超塑性変形と高速化に関する研究2013

    • Author(s)
      森田孝治
    • Organizer
      日本金属学会2013春期大会
    • Place of Presentation
      東京理科大学
    • Year and Date
      2013-03-27
  • [Presentation] Spark- Plasma-Sintering of Transparent MgAl_2O_4 Spinel2012

    • Author(s)
      K. Morita, B.-N. Kim, H. Yoshida, K. Hiraga, Y. Sakka
    • Organizer
      29th K-J Ceramics Seminar
    • Place of Presentation
      Daegu Korea
    • Year and Date
      20121121-24
  • [Presentation] Development of high-strain-rate superplastic oxide ceramics based on flow mechanism2012

    • Author(s)
      K. Morita, B.-N. Kim, H. Yoshida, Y. Sakka and K. Hiraga
    • Organizer
      ICSAM2012
    • Place of Presentation
      Albi Francs
    • Year and Date
      2012-07-04
  • [Presentation] Spark-plasma-sintering (SPS) processing for the synthesis of transparent MgAl_2O_4 spinel2012

    • Author(s)
      K. Morita, B.-N. Kim, H. Yoshida, Z. Zhang, Y. Sakka, K. Hiraga
    • Organizer
      CMCee2012
    • Place of Presentation
      Dresden Germany
    • Year and Date
      2012-05-21
  • [Presentation] Transparent Materials Obtained by SPS Densification2011

    • Author(s)
      K. Morita, B.-N. Kim, H. Yoshida, H. Zhang, K. Hiraga, Y. Sakka
    • Organizer
      2nd Int. Workshop on Spark Plasma Sintering
    • Place of Presentation
      Capbreton France
    • Year and Date
      20111020-21
  • [Presentation] Diffusive Model of Pore Shrinkage in Final-Stage Sintering2011

    • Author(s)
      B.-N. Kim, K. Hiraga, K. Morita, H. Yoshida, H. Zhang
    • Organizer
      Sintering 2011
    • Place of Presentation
      Jeju Korea
    • Year and Date
      20110828-0901
  • [Presentation] Fabrication of high-strength transparent MgAl_ 2O_ 4 by optimizing spark-plasma-sintering (SPS) conditions2011

    • Author(s)
      K. Morita, B.-N. Kim, H. Yoshida, K. Hiraga, Y. Sakka
    • Organizer
      International workshop on Field Assisted Sintering Technology
    • Place of Presentation
      Pen State Univ. US
    • Year and Date
      20110824-25
  • [Presentation] Grain-boundary-diffusion model of final-stage sintering under hydrostatic pressure2011

    • Author(s)
      B.-N. Kim, K. Hiraga, K. Morita, H. Yoshida, H. Zhang
    • Organizer
      12th Conf. of the European Ceramic Society
    • Place of Presentation
      Stockholm Sweden
    • Year and Date
      20110619-23
  • [Presentation] 加圧下最終焼結段階における緻密化挙動の粒界拡散モデル2011

    • Author(s)
      金炳男, 平賀啓二郎, 森田孝治, 吉田英弘, 張海斌
    • Organizer
      日本セラミックス協会年会
    • Place of Presentation
      静岡大学
    • Year and Date
      20110316-18
  • [Presentation] Microstructural Evolution of MgAl2O4 Spinel ceramics during Spark-Plasma-Sintering (SPS) Process2011

    • Author(s)
      K. Morita, B.-N. Kim, H. Yoshida, H. Zhang, K. Hiraga, Y. Sakka
    • Organizer
      European Symp. Current developments in TEM
    • Place of Presentation
      Freiberg Germany
    • Year and Date
      20110310-11
  • [Presentation] 放電プラズマ焼結法により作成したMgO添加透明アルミナ2010

    • Author(s)
      B.-N. Kim, K. Hiraga, K. Morita, H. Yoshida, H. Zhang, J. Lim
    • Organizer
      27th K-J Ceramics Seminar
    • Place of Presentation
      Kurashiki Japan
    • Year and Date
      20101124-26
  • [Presentation] Optimum Spark-Plasma-Sintering (SPS) Condition for Attaining Transparent MgAl2O4 Spinel Polycrystal2010

    • Author(s)
      K. Morita, B.-N. Kim, H. Yoshida, K. Hiraga
    • Organizer
      MSE2010
    • Place of Presentation
      Darmstadt Germany
    • Year and Date
      20100824-26

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Published: 2014-08-29  

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