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2013 Fiscal Year Final Research Report

Occurrence and decomposition behavior of neonicotinoids in food and water environment

Research Project

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Project/Area Number 22790050
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeSingle-year Grants
Research Field Physical pharmacy
Research InstitutionHoshi University

Principal Investigator

KAWAGUCHI Rie (伊藤 里恵)  星薬科大学, 薬学部, 助教 (90398892)

Project Period (FY) 2010-04-01 – 2014-03-31
Keywordsネオニコチノイド / 残留分析 / ハチミツ
Research Abstract

In recent years, as an alternative of organophosphate insecticides, neonicotinoids has been widely used. In order to clarify the residue of neonicotinoids in honey, solid phase extraction (SPE) followed by liquid chromatography tandem mass spectrometry was developed for simultaneous determination of neonicotinoids in honey. When ENVI-Carb/LC-NH2 cartridge was used for SPE, the recoveries of neonicotinoids were improved. In addition, the limits of detection (LODs) and limits of qualification (LOQs) of neonicotinoids were 0.002-0.02 ng/mL and 0.005-0.1 ng/mL, respectively. Compared to liquid-liquid extraction or other SPE cartridge, proposed method is sensitive and simple. The results showed that proposed method is applicable to the determination of trace amounts of neonicotinoids in honey.

  • Research Products

    (2 results)

All Other

All Presentation (2 results)

  • [Presentation] 液液抽出-LC-MS/MS法を用いた蜂蜜中ネオニコチノイド系農薬の分析

    • Author(s)
      大久保哲生, 伊藤里恵, 岩崎雄介, 斉藤貢一, 中澤裕之
    • Organizer
      第130回日本薬学会
    • Place of Presentation
      岡山
  • [Presentation] 蜂蜜中のネオニコチノイド系農薬分析における前処理の検討

    • Author(s)
      大久保哲生, 伊藤里恵, 岩崎雄介, 斉藤貢一, 中澤裕之
    • Organizer
      第71回分析化学討論会
    • Place of Presentation
      島根

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Published: 2015-06-25   Modified: 2015-07-14  

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