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2023 Fiscal Year Annual Research Report

Enhancement of strength-ductility trade-off by microstructure control of C-doped FeNiCoCr HEA.

Research Project

Project/Area Number 22K20478
Research InstitutionYokohama National University

Principal Investigator

THIRATHIPVIWAT PRAMOTE  横浜国立大学, 大学院工学研究院, 助教 (80965822)

Project Period (FY) 2022-08-31 – 2024-03-31
KeywordsHigh entropy alloys / Nutron diffraction / Microstructure control / Texture / Mechanical properties
Outline of Annual Research Achievements

The microstructure evolution of a cold-rolled 1at%C-doped CoCrFeNi during annealing was studied by in-situ neutron diffraction. In as-rolled sample, a strong <111>//ND fiber was evident for high deformability. Annealing at 700°C-1000°C leads to recrystallization and carbide precipitation. The particles retard growth of recrystallized grain limited to ~5 micron even after annealing at 1000°C. Heterogeneous grain sizes and fine chain-like particles are apparently observed after annealing at 700°C-900°C. Annealing at 1000°C leads to more uniform grain sizes and shorter particle chains, causing lower strength. The ductility of two different microstructures annealed at 900°C and 1000°C for 60 min are similar, >40% in elongation. Mechanical properties can be improved by microstructure control.

Remarks

The publication of a manuscript is in progress under a revision for a second round of peer review.

  • Research Products

    (5 results)

All 2023 Other

All Int'l Joint Research (1 results) Presentation (4 results) (of which Int'l Joint Research: 2 results,  Invited: 1 results)

  • [Int'l Joint Research] Technical University of Denmark(デンマーク)

    • Country Name
      DENMARK
    • Counterpart Institution
      Technical University of Denmark
  • [Presentation] In-situ heating neutron diffraction study on changes of microstructure, dislocation density and crystallographic texture in 1 %C-doped CoCrFeNi high entropy alloy2023

    • Author(s)
      Pramote Thirathipviwat, Yusuke Onuki, Makoto Hasegawa, Shigeo Sato
    • Organizer
      Thermec’2023
    • Int'l Joint Research / Invited
  • [Presentation] Precipitation and recrystallization behavior of 1 %C-doped CoCrFeNi high entropy alloy during isochronal annealing2023

    • Author(s)
      Pramote Thirathipviwat, Makoto Hasegawa, Yusuke Onuki, Shigeo Sato
    • Organizer
      2023 JIM Autumn Meeting
  • [Presentation] In-situ neutron diffraction study on microstructure and texture evolution of 1%C-doped CoCrFeNi during annealing2023

    • Author(s)
      Pramote Thirathipviwat, Makoto Hasegawa, Yusuke Onuki, Shigeo Sato
    • Organizer
      第2回 結晶性材料の結晶配向評価および結晶方位解析技術研究会
  • [Presentation] A study on microstructural change of 1 %C-doped CoCrFeNi high entropy alloy during isochronal annealing2023

    • Author(s)
      Pramote Thirathipviwat, Yusuke Onuki, Shigeo Sato, Makoto Hasegawa
    • Organizer
      28th IFHTSE2023
    • Int'l Joint Research

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Published: 2024-12-25  

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