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2013 Fiscal Year Final Research Report

Investigation on Fracture Mechanisms and Size Effects of Nano-Films Using Nano-Mechanical Testing System based upon in-situ Observations and Analyses

Research Project

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Project/Area Number 23246026
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionOsaka University

Principal Investigator

MINOSHIMA Kohji  大阪大学, 工学(系)研究科(研究院), 教授 (50174107)

Co-Investigator(Kenkyū-buntansha) HIRAKATA Hiroyuki  大阪大学, 大学院工学研究科, 准教授 (40362454)
YONEZU Akio  大阪大学, 大学院工学研究科, 助教 (40398566)
Project Period (FY) 2011-04-01 – 2014-03-31
Keywordsマイクロ材料力学 / 材料強度学 / 薄膜 / 破壊 / 疲労 / クリープ
Research Abstract

We developed an experimental setup for clarifying the mechanics and mechanisms of fracture in freestanding submicron-thick metallic films. This system can conduct in situ FESEM observation of deformation/fracture and EBSD crystallographic analysis on the local region at stress concentration sites such as crack tips under controlled mechanical conditions. Systematic experiments clarified the thickness effect on fracture toughness in copper nano-films where the fracture toughness decreases with a decrease in thickness, the characteristic fatigue crack growth mechanism of copper films where a fatigue crack propagates through intrusions/extrusions formed ahead of the crack tip, the presence of fatigue crack closure and the impact on the fatigue crack propagation property, and the effect of thickness on creep properties of aluminum nano-films.

  • Research Products

    (16 results)

All 2014 2013 2012 2011 Other

All Journal Article (5 results) (of which Peer Reviewed: 5 results) Presentation (10 results) Remarks (1 results)

  • [Journal Article] Mechanics of fatigue crack propagation in submicron-thick freestanding copper films2014

    • Author(s)
      Hiroyuki Hirakata, Toshiyuki Kondo, Masayuki Sakihara, Kohji Minoshima
    • Journal Title

      Advanced Materials Research

      Volume: Vols.891-892 Pages: 1681-1687

    • DOI

      10.4028/www.scientific.net/AMR.891-892.1681

    • Peer Reviewed
  • [Journal Article] Effects of stress ratio on fatigue crack propagation properties of submicron-thick freestanding copper films2013

    • Author(s)
      Toshiyuki Kondo, Takahiro Imaoka, Hiroyuki Hirakata, Masayuki Sakihara, Kohji Minoshima
    • Journal Title

      Acta Materialia

      Volume: Vol.61 Pages: 6310-6327

    • DOI

      10.1016/j.actamat.2013.07.017

    • Peer Reviewed
  • [Journal Article] The effect of thickness on steady state creep properties of freestanding aluminum nano-films2012

    • Author(s)
      Hiroyuki Hirakata, Naomichi Fukuhara, Shoichi Ajioka, Akio Yonezu, Masayuki Sakihara, Kohji Minoshima
    • Journal Title

      Acta Materialia

      Volume: Vol.60 Pages: 4438-4447

    • DOI

      10.1016/j.actamat.2012.04.036

    • Peer Reviewed
  • [Journal Article] 自立ナノ薄膜の疲労き裂進展試験法の開発2012

    • Author(s)
      近藤 俊之, 今岡 貴裕, 平方 寛之, 米津 明生, 﨑原 雅之, 箕島 弘二
    • Journal Title

      日本機械学会論文集A編

      Volume: Vol.78 Pages: 808-816

    • DOI

      10.1299/kikaia.78.808

    • Peer Reviewed
  • [Journal Article] Size effect on fracture toughness of freestanding copper nano-films2011

    • Author(s)
      Hiroyuki Hirakata, Osamu Nishijima, Naomichi Fukuhara, Toshiyuki Kondo, Akio Yonezu, Kohji Minoshima
    • Journal Title

      Materials Science and Engineering A

      Volume: Vol.528 Pages: 8120-8127

    • DOI

      10.1016/j.msea.2011.07.071

    • Peer Reviewed
  • [Presentation] Mechanics of fatigue crack propagation in submicron-thick freestanding copper films2014

    • Author(s)
      Hiroyuki Hirakata, Toshiyuki Kondo, Masayuki Sakihara, Kohji Minoshima
    • Organizer
      11th International Fatigue Congress (Fatigue 2014)
    • Place of Presentation
      Melbourne Australia
    • Year and Date
      20140302-07
  • [Presentation] 自立銅ナノ薄膜の疲労き裂進展過程のその場FESEM 観察2013

    • Author(s)
      近藤俊之, 平方寛之, 﨑原雅之, 箕島弘二
    • Organizer
      日本機械学会M&M2013材料力学カンファレンス
    • Place of Presentation
      岐阜大学
    • Year and Date
      20131012-14
  • [Presentation] ナノ観察とEBSD 援用応力解析による自立銅ナノ薄膜の疲労損傷発生機構の解明2013

    • Author(s)
      近藤俊之, 畢暁晨, 田村拓, 平方寛之, 箕島弘二
    • Organizer
      日本材料学会第62期学術講演会
    • Place of Presentation
      東京工業大学
    • Year and Date
      20130518-19
  • [Presentation] 自立Cu ナノ薄膜の疲労き裂進展特性に及ぼす膜厚効果2012

    • Author(s)
      今岡貴裕, 近藤俊之, 平方寛之, 米津明生, 崎原雅之, 箕島弘二
    • Organizer
      日本材料学会第31回疲労シンポジウム
    • Place of Presentation
      慶応義塾大学
    • Year and Date
      2012-11-21
  • [Presentation] ナノメートル厚金属薄膜の破壊じん性に及ぼす膜厚効果2012

    • Author(s)
      平方寛之, 近藤俊之, 竹田裕紀, 河尻隆宏, 米津明生, 箕島弘二
    • Organizer
      日本機械学会M&M2012 材料力学カンファレンス
    • Place of Presentation
      愛媛大学
    • Year and Date
      2012-09-22
  • [Presentation] 自立Cu ナノ薄膜の疲労き裂進展の下限界特性2012

    • Author(s)
      近藤俊之, 今岡貴裕, 平方寛之, 米津明生, 崎原雅之, 箕島弘二
    • Organizer
      日本材料学会第61期学術講演会
    • Place of Presentation
      岡山大学
    • Year and Date
      2012-05-27
  • [Presentation] Size effects on creep property in aluminum nano-films2012

    • Author(s)
      Hiroyuki Hirakata, Naomichi Fukuhara, Akio Yonezu, Kohji Minoshima
    • Organizer
      Asia Pacific Conference on Fracture and Strength - Mechanics and Materials (APCFS-MM 2012)
    • Place of Presentation
      Busan, Korea
    • Year and Date
      2012-05-15
  • [Presentation] Effects of stress ratio on fatigue crack propagation in freestanding Cu nano-films2012

    • Author(s)
      Toshiyuki Kondo, Takahiro Imaoka, Hiroyuki Hirakata, Akio Yonezu, Masayuki Sakihara, Kohji Minoshima
    • Organizer
      Asia Pacific Conference on Fracture and Strength - Mechanics and Materials (APCFS-MM 2012)
    • Place of Presentation
      Busan, Korea
    • Year and Date
      2012-05-15
  • [Presentation] 自立Cu ナノ薄膜の疲労き裂進展における膜厚効果2011

    • Author(s)
      平方寛之, 近藤俊之, 西嶋修, 米津明生, 箕島弘二
    • Organizer
      日本機械学会第3回マイクロ・ナノ工学シンポジウム
    • Place of Presentation
      タワーホール船堀(東京)
    • Year and Date
      2011-09-27
  • [Presentation] Fatigue crack propagation in freestanding copper nano-films2011

    • Author(s)
      Toshiyuki Kondo, Takahiro Imaoka, Hiroyuki Hirakata, Akio Yonezu, Masayuki Sakihara, Kohji Minoshima
    • Organizer
      International Conference on Advanced Technology in Experimental Mechanics 2011 (ATEM'11)
    • Place of Presentation
      神戸国際会議場
    • Year and Date
      2011-09-20
  • [Remarks] ホームページ

    • URL

      http://www-micro.mech.eng.osaka-u.ac.jp/home.html

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Published: 2015-06-25  

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