2013 Fiscal Year Final Research Report
Monitoring of trace elements in coal gasification gas by double pulse LIBS
Project/Area Number |
23561029
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Research Category |
Grant-in-Aid for Scientific Research (C)
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Allocation Type | Multi-year Fund |
Section | 一般 |
Research Field |
Energy engineering
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Research Institution | Nagoya University |
Principal Investigator |
YOSHIIE Ryo 名古屋大学, 工学(系)研究科(研究院), 准教授 (60293544)
|
Co-Investigator(Kenkyū-buntansha) |
NARUSE Ichiro 名古屋大学, エコトピア科学研究所, 教授 (80218065)
|
Project Period (FY) |
2011 – 2013
|
Keywords | 環境調和 / 微量成分 / 石炭 / 分光分析 |
Research Abstract |
To investigate trace element emissions in coal combustion/gasification gas, we worked on the development of a rapid analytical method to monitor trace elements in vapor/aerosol phase. Double pulse LIBS (Laser Induced Breakdown Spectroscopy) system with a single optical lens and small angled two lasers were built up and examined to improve detection ranges, but it fell short of our expectations. An infrared image furnace with a quartz reactor was arranged to achieve coal combustion/gasification experiments with rapid heating. Trace elements downstream of the reactor were analyzed by single pulse LIBS. Signals from As and Sb were successfully detected. Concentration of Sb in coal combustion gas was measured based on calibration curve method.
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Research Products
(8 results)