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2013 Fiscal Year Final Research Report

Preparation of Giant Pseudo-Single Crystals of Superelastic Alloys and the Mechanism of Grain Growth

Research Project

  • PDF
Project/Area Number 24656426
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeSingle-year Grants
Research Field Material processing/treatments
Research InstitutionTohoku University

Principal Investigator

ISHIDA Kiyohito  東北大学, 工学(系)研究科(研究院), 名誉教授 (20151368)

Co-Investigator(Kenkyū-buntansha) OHNUMA Ikuo  東北大学, 大学院工学研究科, 准教授 (20250714)
OMORI Toshihiro  東北大学, 大学院工学研究科, 助教 (60451530)
Project Period (FY) 2012-04-01 – 2014-03-31
Keywords結晶粒成長 / Cu基形状記憶合金 / 熱処理 / 異常粒成長 / 繰り返し熱処理 / 亜結晶粒
Research Abstract

The grain growth of beta(bcc) phase in Cu-Al-Mn base shape memory alloys has been studied. The abnormal grain growth was realized when the Cu-Al-Mn alloys were first quenched from the beta single-phase region at high temperature round 1173K and then was slowly cooled at about 773K, and subsequent heating to the beta single-region. The pseudo-single crystals due to abnormal grain growth were obtained by thermally cycling where beta phase leads to a precipitation and subsequent dissolution of the alpha phase. This abnormal grain growth phenomenon results from the formation of subgrain structure introduced through phase transformation, where the subgrain-boundary energy might be one of the driving force. These findings provide a method of fabricating a single-crystal or large-grain structure important for superelastic properties.

  • Research Products

    (8 results)

All 2014 2013

All Journal Article (3 results) (of which Peer Reviewed: 3 results) Presentation (4 results) Patent(Industrial Property Rights) (1 results)

  • [Journal Article] Grain size dependence of pseudoelasticity in polycrystalline, Cu-Al-Mn-based shape memory sheets2013

    • Author(s)
      Y. Sutou, T. Omori, R. Kainuma, K. Ishida
    • Journal Title

      Acta Mater

      Volume: 61 Pages: 3842-3850

    • DOI

      10.1016/j.actamat.2013.03.022

    • Peer Reviewed
  • [Journal Article] Two- and Three-Dimensional Grain Growth in the CuAlMn Shape Memory Alloy2013

    • Author(s)
      Tomoe Kusama, Toshihiro Omori, Takashi Saito, Ikuo Ohnuma, Kiyohito Ishida and Ryosuke Kainuma
    • Journal Title

      Materials Transactions

      Volume: 54 Pages: 2044 -2048

    • DOI

      10.2320/matertrans.M2013167

    • Peer Reviewed
  • [Journal Article] Abnormal Grain Growth Induced by Cyclic Heat Treatment2013

    • Author(s)
      Toshihiro Omori, Tomoe Kusama, Shingo Kawata, Ikuo Ohnuma, Yuji Sutou, Yoshikazu Araki, Kiyohito Ishida and Ryosuke Kainuma
    • Journal Title

      Science

      Volume: 341 Pages: 1500-1502

    • DOI

      10.1126/science.1238017

    • Peer Reviewed
  • [Presentation] Cu-Al-Mn 形状記憶合金における相変態を利用した異常粒成長2014

    • Author(s)
      草間知枝、川田紳悟、大森俊洋、大沼郁雄、須藤祐司、石田清仁、貝沼亮介
    • Organizer
      日本金属学会2014年(第154回)春期講演大会
    • Place of Presentation
      東京工業大学
    • Year and Date
      2014-03-22
  • [Presentation] Normal grain growth behavior in two- and three- dimensional modes of Cu-Al-Mn shape memory alloy2013

    • Author(s)
      T. Kusama, T. Omori, T. Saito, I. Ohnuma, K. Ishida, R. Kainuma
    • Organizer
      Joint Symposium on Materials Science and engineering for the 21^<st> Century
    • Place of Presentation
      Hsinchu, Taiwan
    • Year and Date
      2013-06-23
  • [Presentation] Grain Growth Behavior of Cu-Al-Mn Shape Memory Alloys with BCC Structure2013

    • Author(s)
      T. Kusama, T. Omori, T. Saito, I. Ohnuma, K. Ishida, R. Kainuma
    • Organizer
      5^<th> International Conferenceon Recrystallization & Grain Growth
    • Place of Presentation
      Sedney Australia
    • Year and Date
      2013-05-06
  • [Presentation] 合金の相安定性と材料開発2013

    • Author(s)
      石田清仁
    • Organizer
      日本金属学会2013年(第152回)春期講演大会
    • Place of Presentation
      東京理科大学
    • Year and Date
      2013-03-28
  • [Patent(Industrial Property Rights)] 安定した超弾性を示すCu-Al-Mn 系棒材及び板材、その製造方法、それを用いた制震部材、並びに制震部材を用いた制震構造体2013

    • Inventor(s)
      大森俊洋、草間知枝、貝沼亮介、石田清仁、田中豊延、喜瀬純男、中溝賢治、石川浩司、中野美里、勅使河原 聡
    • Industrial Property Rights Holder
      株式会社古河テクノマテリアル、国立大学法人東北大学、古河電気工業株式会社
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      出願2013-099996
    • Filing Date
      2013-05-10

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Published: 2015-06-25  

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