2012 Fiscal Year Final Research Report
Formulation of Liquid-Liquid-Liquid Reaction System in Microreactor
| Project/Area Number |
24656483
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| Research Category |
Grant-in-Aid for Challenging Exploratory Research
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| Allocation Type | Multi-year Fund |
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| Research Field |
Reaction engineering/Process system
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| Research Institution | Sojo University |
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Principal Investigator |
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| Project Period (FY) |
2012
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| Keywords | マイクロリアクター / 相関移動 / 有機合成 / 液滴 |
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| Research Abstract |
When potassium hydroxide solution, benzene and dichloromethane including equimolar mixture of benzyltriphenylphosphonium bromide and p-methoxybenzaldehyde was fed through a cross joint into a microreactor, segmented flow consisting water droplet and oil droplets was formed and the Wittig reaction proceeded in the tube. The reaction yield in liquid-liquid-liquid reaction system was higher than that in liquid-liquid one due to the contribution of mass transfer effect.
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