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2015 Fiscal Year Final Research Report

Detection of environmental transformation products without standard chemical reagent

Research Project

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Project/Area Number 26550064
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Environmental engineering and reduction of environmental burden
Research InstitutionKagoshima University

Principal Investigator

TAKANASHI Hirokazu  鹿児島大学, 理工学域工学系, 准教授 (40274740)

Project Period (FY) 2014-04-01 – 2016-03-31
Keywords環境変化体 / 農薬 / LC/MS/MS
Outline of Final Research Achievements

Using a liquid chromatograph-high resolution mass spectrometer (LC-MS) and a liquid chromatograph-triple quadrupole mass spectrometer (LC-MS/MS), we have developed a new technique to detect environmental transformation products (TPs) without any standard chemical reagent. A purchased reagent was irradiated with a Xeon ramp to produce the TPs. The produced TPs were not purified and used as a crude sample. The crude sample was injected to LC-MS/MS to determine selected reaction monitoring (SRM) conditions. By using the determined SRM conditions, unreported TPs were successfully detected from actual environmental samples.

Free Research Field

環境質量分析

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Published: 2017-05-10  

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