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ナノ構造のためのソリューション・パルス・プラズマの診断

Research Project

Project/Area Number 07F07712
Research Category

Grant-in-Aid for JSPS Fellows

Allocation TypeSingle-year Grants
Section外国
Research Field Material processing/treatments
Research InstitutionNagoya University

Principal Investigator

高井 治  Nagoya University, エコトピア科学研究所, 教授

Co-Investigator(Kenkyū-buntansha) APETROAEI NECULAI  名古屋大学, エコトピア科学研究所, 外国人特別研究員
APETROAEI Neculai  名古屋大学, エコトピア科学研究所, 外国人特別研究員
Project Period (FY) 2007 – 2008
Project Status Completed (Fiscal Year 2008)
Budget Amount *help
¥2,200,000 (Direct Cost: ¥2,200,000)
Fiscal Year 2008: ¥1,100,000 (Direct Cost: ¥1,100,000)
Fiscal Year 2007: ¥1,100,000 (Direct Cost: ¥1,100,000)
Keywordsソリューションプラズマ / 金属ナノ粒子 / 構造制御 / プラズマ診断
Research Abstract

本研究では液中での放電現象(ソリューションプラズマ)を利用した金属ナノ粒子(主に銅ナノ粒子)の作製と形状制御を試みた。以下に本年度で得られた具体的成果を示す。
(1)作製法
ワイヤもしくはロッド電極には銅やタングステンを用い、平板電極に銅を使用した。放電が発生した領域において電極の溶融・蒸発が進行し、誘電液体中、核生成とそれに続く凝縮によりナノ粒子へと変化し液中に分散した。ナノ粒子生成の確認にはTEMを用いた。
(2)形状制御
誘電液体の種類を変えることで、生成するCuOナノ粒子の形状を制御した。純水中では幅10nm、長さ100nm程の針状構造を確認した。エタノールもしくはエチレングリコール中では銅-炭素合金状を、水-ヒドラジン系では多角形構造やロッド構造の生成を確認した。初期状態の形状は同じだが、最終的には液体自体の特性に因るところが大きいことが分かった。
(3)電極表面
銅、モリブデン、タングステンなど各種電極の表面形状をSEM観察したところ、放電前後で表面形態が変化していることが分かった。
以上より、本年度はソリューションプラズマによるナノ構造制御の基礎的知見を得て、作製プロセスを確立することができた。

Report

(2 results)
  • 2008 Annual Research Report
  • 2007 Annual Research Report
  • Research Products

    (55 results)

All 2009 2008 2007 Other

All Journal Article (9 results) (of which Peer Reviewed: 9 results) Presentation (44 results) Remarks (1 results) Patent(Industrial Property Rights) (1 results)

  • [Journal Article] Synthesis and characterization of copper-based nanoparticles, via solution plasma2009

    • Author(s)
      N. Apetroaei, N. Saito, O. Takai
    • Journal Title

      Pros. ISGLP 2008 (印刷中)

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effect of water plasma on Cu and SUS electrode surface2009

    • Author(s)
      N. Apetroaei, N. Saito, O. Takai
    • Journal Title

      Pros. PSS-2009/SPP-26 (印刷中)

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] ソルーションプラズマによるナノ微粒子合成と界面制御2008

    • Author(s)
      高井 治
    • Journal Title

      粉砕 51

      Pages: 30-36

    • NAID

      130007495305

    • Related Report
      2007 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Reaction Dynamics for Gold Nanoparticles Synthesis in Solution Plasma2008

    • Author(s)
      J. Hieda, N. Saito, O Takai
    • Journal Title

      Proceedings of Materials Research Society Symposium 105

    • Related Report
      2007 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Special type of plasma dielectric barrier discharge reactor for directozonization of water and degradation of organic pollution2008

    • Author(s)
      P. Baroch, N. Saito, O. Takai
    • Journal Title

      Journal of Physics D: Applied Physics 41

      Pages: 85207-85207

    • Related Report
      2007 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Bipolar pulsed electrical discharge for decomposition2008

    • Author(s)
      P. Baroch, N. Saito, O. Takai
    • Journal Title

      Journal of Electrostatics (印刷中)

    • Related Report
      2007 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Size-regulated Gold Nanoparticles Fabricated by a Discharge in Reverse Micelle Solutions2008

    • Author(s)
      J. Hieda, N. Saito, O Takai
    • Journal Title

      Surface and Coatings Technology (印刷中)

    • Related Report
      2007 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Exotic shapes of gold nanopatricles synthesized using plasma in aqueous solution2008

    • Author(s)
      J. Hieda, N. Saito, O Takai
    • Journal Title

      The Journal of Vacuum Science and Technology A (印刷中)

    • Related Report
      2007 Annual Research Report
    • Peer Reviewed
  • [Journal Article] ソリューションプラズマ材料プロセッシング2007

    • Author(s)
      斎藤 永宏, 稗田 純子, C. Miron, 高井 治
    • Journal Title

      表面技術 58

      Pages: 810-814

    • NAID

      10019979483

    • Related Report
      2007 Annual Research Report
    • Peer Reviewed
  • [Presentation] Synthesis and Characterization of Copper Nanoparticles Using Solution Glow ischarge2008

    • Author(s)
      N. Apetroaei, N. Saito, O. Takai
    • Organizer
      IUMRS-ICA 2008
    • Place of Presentation
      Nagoya, Japan
    • Year and Date
      2008-12-11
    • Related Report
      2008 Annual Research Report
  • [Presentation] Synthesis and Characterization of Copper-based Nanoparticles vis Solution Plasma2008

    • Author(s)
      N. Apetroaei, N. Saito, O. Takai
    • Organizer
      ISGLP 2008
    • Place of Presentation
      Sendai, Japan
    • Year and Date
      2008-09-06
    • Related Report
      2008 Annual Research Report
  • [Presentation] Synthesis and Characterization of Copper-based Nanoparticles using Liquid Discharge and Cu Electrode2008

    • Author(s)
      N. Apetroaei, N. Saito, O. Takai
    • Organizer
      IUMRS-ICEM 2008
    • Place of Presentation
      Hilton Sydney, Australia
    • Year and Date
      2008-07-29
    • Related Report
      2008 Annual Research Report
  • [Presentation] Synthesis and Characterization of Copper-based Nanoparticles by Electrode Erosion in Liquid Discharge2008

    • Author(s)
      N. Apetroaei, N. Saito, O. Takai
    • Organizer
      Interfinish 2008
    • Place of Presentation
      Pusan, Korea
    • Year and Date
      2008-06-17
    • Related Report
      2008 Annual Research Report
  • [Presentation] 逆ミセル溶液で生成したソリューションプラズマの発光分光および電流・電圧測定2008

    • Author(s)
      稗田 純子, 石崎 貴裕, 〓藤 永宏, 高井 治
    • Organizer
      2008年春季第55回応用物理学関係連合講演会
    • Place of Presentation
      千葉
    • Year and Date
      2008-03-29
    • Related Report
      2007 Annual Research Report
  • [Presentation] 新しい材料合成・加工の反応場としての・リユーションプラズマ2008

    • Author(s)
      高井 治
    • Organizer
      2008年春季第55回応用物理学関係連合講演会
    • Place of Presentation
      千葉
    • Year and Date
      2008-03-29
    • Related Report
      2007 Annual Research Report
  • [Presentation] ソリューションプラズマを用いたナノ粒子・異種イオン分散溶液からの金ナノマテリアルの合成2008

    • Author(s)
      稗田 純子, 〓藤 永宏, 高井 治
    • Organizer
      表面技術協会第117回講演大会
    • Place of Presentation
      千葉
    • Year and Date
      2008-03-13
    • Related Report
      2007 Annual Research Report
  • [Presentation] ソリューションプラズマによるFePt微粒子の合成とその評価2008

    • Author(s)
      李 京煕, 〓藤 永宏, 高井 治
    • Organizer
      表面技術協会第117回講演大会
    • Place of Presentation
      千葉
    • Year and Date
      2008-03-13
    • Related Report
      2007 Annual Research Report
  • [Presentation] ソリューションプラズマによる金ナノ微粒子の形状制御プロセスの開拓2008

    • Author(s)
      中村 泰啓, 石崎 貴裕, 〓藤 永宏, 高井 治
    • Organizer
      表面技術協会第117回講演大会
    • Place of Presentation
      千葉
    • Year and Date
      2008-03-12
    • Related Report
      2007 Annual Research Report
  • [Presentation] ソリューションプラズマに及ぼす溶存酸素の影響2008

    • Author(s)
      藤川 理大, 石崎 貴裕, 〓藤 永広, 高井 治
    • Organizer
      表面技術協会第117回講演大会
    • Place of Presentation
      千葉
    • Year and Date
      2008-03-12
    • Related Report
      2007 Annual Research Report
  • [Presentation] ソリューションプラズマによるPt/CNBの作製と触媒活性評価2008

    • Author(s)
      市野 善道, 石崎 貴裕, 〓藤 永宏, 高井 治
    • Organizer
      表面技術協会第117回講演大会
    • Place of Presentation
      千葉
    • Year and Date
      2008-03-12
    • Related Report
      2007 Annual Research Report
  • [Presentation] Formation Chemistry of Gold Nanoparticles Prepared in Solution Plasma2008

    • Author(s)
      J. Hieda, T. Ishizaki, N. Saito, O. Takai
    • Organizer
      Eighth International Symposium on Biomimetic Materials Processing(BMMP-8)
    • Place of Presentation
      名古屋
    • Year and Date
      2008-01-23
    • Related Report
      2007 Annual Research Report
  • [Presentation] Formation Chemistry of Gold Nanoparticles Prepated in Solution Plasma2008

    • Author(s)
      D. B. Allred, M. A. Bratescu, M. Sarikaya, N. Saito, O. Takai
    • Organizer
      Eighth International Symposium on Biomimetic Materials Processing(BMMP-8)
    • Place of Presentation
      名古屋
    • Year and Date
      2008-01-23
    • Related Report
      2007 Annual Research Report
  • [Presentation] Decoloration of Organic Dye by Solution Plasma Process2008

    • Author(s)
      S. Potocky, N. Saito, O. Takai
    • Organizer
      Eighth International Symposium on Biomimetic Materials Processing(BMMP-8)
    • Place of Presentation
      名古屋
    • Year and Date
      2008-01-23
    • Related Report
      2007 Annual Research Report
  • [Presentation] Biomimetic Nanomaterials and Processing2008

    • Author(s)
      O. Takai
    • Organizer
      Eighth International Symposium on Biomimetic Materials Processing(BMMP-8)
    • Place of Presentation
      名古屋
    • Year and Date
      2008-01-22
    • Related Report
      2007 Annual Research Report
  • [Presentation] ソリューションプラズマの生成とナノ合成および表面改質ヘの応用2007

    • Author(s)
      稗田 純子, 高井 治
    • Organizer
      第66回表面技術アカデミック研究討論会
    • Place of Presentation
      東京
    • Year and Date
      2007-12-10
    • Related Report
      2007 Annual Research Report
  • [Presentation] Initial Mechanisms of Nanomaterial Formation in a Solution Plasma2007

    • Author(s)
      D. B. Allred, M. A. Bratescu, N. Saito, O. Takai
    • Organizer
      第18回日本MRS学術シンポジウム
    • Place of Presentation
      東京
    • Year and Date
      2007-12-08
    • Related Report
      2007 Annual Research Report
  • [Presentation] Chemical Analysis of Solution Plasma by Gas Chromatography and ICP-MS2007

    • Author(s)
      S. Potocky, N. Saito, O. Takai
    • Organizer
      第18回日本MRS学術シンポジウム
    • Place of Presentation
      東京
    • Year and Date
      2007-12-07
    • Related Report
      2007 Annual Research Report
  • [Presentation] Preparation of copper nanoparticles by electrode etching in water discharge2007

    • Author(s)
      A. Neculai, N. Saita, O. Takai
    • Organizer
      第18回日本MRS学術シンポジウム
    • Place of Presentation
      東京
    • Year and Date
      2007-12-07
    • Related Report
      2007 Annual Research Report
  • [Presentation] Reaction Dynamics for Gold Nanoparticles Synthesis in Solution Plasma2007

    • Author(s)
      J. Hieda, T. Ishizadi, N. Saito, O. Takai
    • Organizer
      Material Research Society
    • Place of Presentation
      Boston,USA
    • Year and Date
      2007-11-26
    • Related Report
      2007 Annual Research Report
  • [Presentation] Solution Plasma Discharge for Water Treatment2007

    • Author(s)
      S. Potocky, N. Saito, O. Takai
    • Organizer
      International Symposium on Ecotopia Science(ISET)
    • Place of Presentation
      名古屋
    • Year and Date
      2007-11-25
    • Related Report
      2007 Annual Research Report
  • [Presentation] Time Resolve Electrical Characteristics of Discharge in Liquids2007

    • Author(s)
      A. Neculai, N. Saito, O. Takai
    • Organizer
      International Symposium on Ecotopia Science (ISET)
    • Place of Presentation
      名古屋
    • Year and Date
      2007-11-25
    • Related Report
      2007 Annual Research Report
  • [Presentation] 液中プラズマを用いた白金担持カーボンナノボーノレの合成2007

    • Author(s)
      伊藤 経之, M. A. Bratescu, 石崎 貴裕, 〓藤 永宏, 高井 治
    • Organizer
      第21回「ナノテク部会」研究会
    • Place of Presentation
      長野
    • Year and Date
      2007-11-17
    • Related Report
      2007 Annual Research Report
  • [Presentation] ソリューションプラズマによる異形金ナノ微粒子の合成2007

    • Author(s)
      中村 泰啓, 石崎 貴裕, 〓藤 永宏, 高井 治
    • Organizer
      第21回「ナノテク部会」研究会
    • Place of Presentation
      長野
    • Year and Date
      2007-11-17
    • Related Report
      2007 Annual Research Report
  • [Presentation] Size Distribution Factor of Platinum Nanoparticles Synthesized by Plasmain Aqueous Solution2007

    • Author(s)
      T. Nishigaki, T. Ishizaki, N. Saito, O. Takai
    • Organizer
      AVS 54th lnternational Symposium&Exhibition
    • Place of Presentation
      Seattle,USA
    • Year and Date
      2007-10-16
    • Related Report
      2007 Annual Research Report
  • [Presentation] Diagnostic of Plasma Generated in Water by Time-Resolved Optical Spectroscopy2007

    • Author(s)
      C. Miron, M. A. Bratescu, N. Saito, O. Takai
    • Organizer
      AVS 54th lnternational Symposium&Exhibition
    • Place of Presentation
      Seattle,USA
    • Year and Date
      2007-10-16
    • Related Report
      2007 Annual Research Report
  • [Presentation] Exotic Shapes of Gold Nanoparticles Synthesized with Plasma in an Aqueous Solution2007

    • Author(s)
      J. Hieda, M. Oda, N. Saito, O. Takai
    • Organizer
      AVS 54th International Symposium&Exhibition
    • Place of Presentation
      Seattle,USA
    • Year and Date
      2007-10-16
    • Related Report
      2007 Annual Research Report
  • [Presentation] Syntheses of Nanoparticles by Solution Plasma Processing(SPP)2007

    • Author(s)
      O. Takai
    • Organizer
      Japan-India Symposiumon Advanced MATERIALS(10th INUMRS International Conference on Advanced Materials
    • Place of Presentation
      Bangalore,India
    • Year and Date
      2007-10-08
    • Related Report
      2007 Annual Research Report
  • [Presentation] Sterilization mechanism of bacteria by a pulsed discharge in water2007

    • Author(s)
      T. Takeda, P. Baroch, T. Ishizaki, N. Saito, M. Ohta, O. Takai
    • Organizer
      AEPSE2007
    • Place of Presentation
      長崎
    • Year and Date
      2007-09-29
    • Related Report
      2007 Annual Research Report
  • [Presentation] Diagnostic of plasma in aqueous systems by time-resolved optical spectroscopy2007

    • Author(s)
      C. Miron, M. A. Bratescu, N. Saito, O.Takai
    • Organizer
      AEPSE2007
    • Place of Presentation
      長崎
    • Year and Date
      2007-09-27
    • Related Report
      2007 Annual Research Report
  • [Presentation] Size Control of Gold Nanoparticles fabricated with discharge in reversemicelle solutions2007

    • Author(s)
      J. Hieda, M. Oda, N. Saito, O. Takai
    • Organizer
      AEPSE2007
    • Place of Presentation
      長崎
    • Year and Date
      2007-09-25
    • Related Report
      2007 Annual Research Report
  • [Presentation] ソリューションプラズマによる窒化プロセスの探索2007

    • Author(s)
      入江 和徳, 石崎 貴裕, 〓藤 永宏, 高井 治
    • Organizer
      資源・素材2007
    • Place of Presentation
      名古屋
    • Year and Date
      2007-09-25
    • Related Report
      2007 Annual Research Report
  • [Presentation] ソリューションプラズマによる異形金ナノ微粒子合成プロセスの開拓2007

    • Author(s)
      中村 泰啓, 石崎 貴裕, 〓藤 永宏, 高井 治
    • Organizer
      資源・素材2007
    • Place of Presentation
      名古屋
    • Year and Date
      2007-09-25
    • Related Report
      2007 Annual Research Report
  • [Presentation] 窒化反応のためのソリューションプラズマの設計と診断2007

    • Author(s)
      入江 和徳, 石崎 貴裕, 〓藤 永宏, 高井 治
    • Organizer
      表面技術協会第116回講演大会
    • Place of Presentation
      長崎
    • Year and Date
      2007-09-18
    • Related Report
      2007 Annual Research Report
  • [Presentation] Synthesis of platinum Nanopatricles by Solution Plasma Processing2007

    • Author(s)
      T. Nishigaki, T. Ishizaki, N. Saito, O. Takai
    • Organizer
      The Doyama Symposium on Advaned Materials
    • Place of Presentation
      東京
    • Year and Date
      2007-09-06
    • Related Report
      2007 Annual Research Report
  • [Presentation] Synthesis of gold nanoparticles by discharge in aqueous solution2007

    • Author(s)
      Y. Nakamura, T. Ishizaki, N. Saito, O. Takai
    • Organizer
      The Doyama Symposium on Advanced Materials
    • Place of Presentation
      東京
    • Year and Date
      2007-09-06
    • Related Report
      2007 Annual Research Report
  • [Presentation] Reaction kinetics for synthesis of gold nanoparticles in solution plasma field2007

    • Author(s)
      J. Hieda, M. Oda, N. Saito, O. Takai
    • Organizer
      18th International Symposium on Plasma Chemistry
    • Place of Presentation
      京都
    • Year and Date
      2007-08-31
    • Related Report
      2007 Annual Research Report
  • [Presentation] Solution plasma processing(SPP)2007

    • Author(s)
      O. Takai
    • Organizer
      18th International Symposium on Plasma Chemistry
    • Place of Presentation
      京都
    • Year and Date
      2007-08-31
    • Related Report
      2007 Annual Research Report
  • [Presentation] Diagnostic of water plasma by time resolved optical spectroscopy2007

    • Author(s)
      C. Miron, M. A. Bratescu, N. Saito, O. Takai
    • Organizer
      18th International Symposium on Plasma Chemistry
    • Place of Presentation
      京都
    • Year and Date
      2007-08-31
    • Related Report
      2007 Annual Research Report
  • [Presentation] Sterilization treatment of bacteria by discharge in an aqueous solution and elucidation of the mechanism2007

    • Author(s)
      T. Takeda, P. Baroch, T. Ishizaki, N. Saito, M. Ohta, O. Takai
    • Organizer
      18th International Symposium on Plasma Chemistry
    • Place of Presentation
      京都
    • Year and Date
      2007-08-27
    • Related Report
      2007 Annual Research Report
  • [Presentation] NanoTopological Particles Synthesized by Sub-μ-second Pulsed Solution Plasma Processing(SPP)2007

    • Author(s)
      O. Takai
    • Organizer
      The 20th Symposium on Plasma Science for Materials
    • Place of Presentation
      名古屋
    • Year and Date
      2007-06-21
    • Related Report
      2007 Annual Research Report
  • [Presentation] Solution Plasma Processing2007

    • Author(s)
      O. Takai
    • Organizer
      5th International Symposium on Advanced Plasma Processes and Diagnostics&1st International Symposium on Flexible Electronics Technology
    • Place of Presentation
      水原,韓国
    • Year and Date
      2007-04-07
    • Related Report
      2007 Annual Research Report
  • [Presentation] Preparation of gold nanoparticles by discharge in aqueous and non-aqueous solutions2007

    • Author(s)
      J. Hieda, M. Oda, N. Saito, O. Takai
    • Organizer
      5th International Symposium on Advanced Plasma Processes and Diagnostics&1st International Symposium on Flexible Electronics Technology
    • Place of Presentation
      水原,韓国
    • Year and Date
      2007-04-07
    • Related Report
      2007 Annual Research Report
  • [Presentation] Plasma generation in purified water by Ar bubble support and application to sterilization processing2007

    • Author(s)
      T. Takeda, P. Baroch, T. Ishizaki, N. Saito, M. Ohta, O. Takai
    • Organizer
      5th International Symposium on Advanced Plasma Processes and Diagnostics&1st International Symposium on Flexible Electronics Technology
    • Place of Presentation
      水原,韓国
    • Year and Date
      2007-04-07
    • Related Report
      2007 Annual Research Report
  • [Remarks]

    • URL

      http://eco-t.esi.nagoya-u.ac.jp/~takai

    • Related Report
      2008 Annual Research Report
  • [Patent(Industrial Property Rights)] 水中プラズマ滅菌方法及び水中プラズマ滅菌装置2008

    • Inventor(s)
      高井 治, 〓藤 永宏, 石崎 貴裕, 長伸 朗, 田中 和士
    • Industrial Property Rights Holder
      中部電力株式会社
    • Filing Date
      2008-03-27
    • Related Report
      2007 Annual Research Report

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Published: 2007-04-01   Modified: 2024-03-26  

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