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Neutron diffraction and surface morhology observation of ultra-fine grained materials

Research Project

Project/Area Number 13450283
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionIbaraki University

Principal Investigator

TOMOTA Yo  IBARAKI Univ., College of Engineering, Professor, 工学部, 教授 (90007782)

Co-Investigator(Kenkyū-buntansha) 鈴木 徹也  茨城大学, 工学部, 講師 (70261740)
Project Period (FY) 2001 – 2003
Project Status Completed (Fiscal Year 2003)
Budget Amount *help
¥17,100,000 (Direct Cost: ¥17,100,000)
Fiscal Year 2003: ¥2,500,000 (Direct Cost: ¥2,500,000)
Fiscal Year 2002: ¥2,700,000 (Direct Cost: ¥2,700,000)
Fiscal Year 2001: ¥11,900,000 (Direct Cost: ¥11,900,000)
Keywordsneutron diffraction / nano-structure / pearlite / cementite dissolution / ferrite / strength / phase stress / residual stress / セメンタイト溶解 / 応力分配
Research Abstract

Ultra-fine grained materials were prepared through themo-mechanical heat treatment and their microstructures and tensile behavior were examined by using neutron diffraction and laser conforcal microscopy. The materials studied include (1)pearlite, (2)ferrite and (3)severely drawn ferrite or pearlite steel wires.
The internal stresses, i.e., phase stress, block stress and lamellar stress are generated by multi-scale inhomogeneity in plastic flow. Leading to high work-hardening. The stress in cementite plates embedded into the ferrite matrix was determined approximately 5GPa when a pearlite steel is subjected to the applied stress of 1.6GPa.
A ferrite steel consisting of submicron meters ferrite and cementite particles exhibits a high strength but little work-hardening. Using tensile and compression tests and surface observations, the plastic instability in the early stage of tensile deformation was made clear.
Heavily drawn ferrite steel was found to show continuous recrystalisation during plastic deformation and hence only grain growth was observed by annealing. The strength of such nano-grain sized specimen show 1.4GPa. In case of peralite steel, cementite plates dissolve during drawing and exhibited the tensile strength as high as 4GPa. The elastic behavior was revealed nonlinear at the higher stress regime by insitu neutron diffraction during tensile loading.

Report

(4 results)
  • 2003 Annual Research Report   Final Research Report Summary
  • 2002 Annual Research Report
  • 2001 Annual Research Report
  • Research Products

    (12 results)

All Other

All Publications (12 results)

  • [Publications] Y.Tomota, O.Watanabe, A.Kanie, A.Moriai, N.Minakawa, Y.Morii: "Effect of carbon concentration on tensile behavior of pearlite steels"Materials Science and Technology. 19. 1715-1720 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] 蟹江厚臣, 友田 陽, 鈴木徹也, 鳥居周輝, 盛合 敦, 皆川宣明, 森井幸生, 神山 崇: "中性子回折によるパーライト組織鋼における加工硬化機構の"材料(材料学会誌). 印刷中.

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] T.Suzuki, Y.Tomota, M.Isaka, A.Moriai, N.Minakawa, Y.Morii: "Strength Anisotropy and Residual Stress in Drawn Pearlite Steel Wire"ISIJ Inter.. 印刷中.

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] Y.Tomota, O.Watanabe, A.Kanie, A.Moriai, N.Minakawa, Y.Morii: "Effect of carbon concentration on tensible behavior of pearlite steels"Materi.Sci.Technology. 19 NO.23. 1715-1720 (2003)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] A.Kanie, Y.Tomota, T.Suzuki, A.Moriai, N.Minakawa, Y.Morii: "Work-hardening of pearlite steels studied by neutron diffraction"Journal of the society of Materials Science, Japan. (in print).

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] T.Suzuki, Y.Tomota, M.Isaka, A.Moriai, N.Minakawa, Y.Morii: "Strength anisotropy and Residual Stress in Drawn Pearlite Steel Wire"ISIJ Inter.. (accepted for publication). (2004)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] A.Kanie, Y.Tomota, N.Minakawa, T.Kamiyama: "Strength of Cementite in Pearlite Steels"Current Advances in Materials and Processing ISIJ. 16巻3号. 484-487 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] T.Suzuki, Y.Tomota, A.Moriai, N.Minakawa: "Strength Difference Effect in a Drawn Pearlite Steel Wire"Current Advances in Materials and Processing ISIJ. 16巻3号. 487-489 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] Y.Tomota, O.Watanabe, A.Kanie, A.Moriai, N.Minakawa, Y.Morii: "Effect of carbon concentration on tensile behavior of pearlite steels"Materials Science and Technology. 19巻12号. 1715-1720 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 蟹江厚臣, 友田 陽, 鈴木徹也, 鳥居周輝, 盛合 敦, 皆川宣明, 森井幸生, 神山 崇: "中性子回折によるパーライト組織鋼における加工硬化機構の考察"材料. (掲載決定). (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] A.Kanie, Y.Tomota, N.Minakawa, T.Kamiyama: "Strength of Cementite in Pearlite Steels"Current Advances in Materials and Processing ISIJ. 16. 484-487 (2003)

    • Related Report
      2002 Annual Research Report
  • [Publications] T.Suzuki, Y.Tomota, A.Moriai, N.Minakawa: "Strength Difference Effect in a Drawn Pearlite Steel Wire"Current Advances in Materials and Processing ISIJ. 16. 487-489 (2003)

    • Related Report
      2002 Annual Research Report

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Published: 2001-04-01   Modified: 2016-04-21  

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