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On the Mechanism and ControLof Nanoparticles Co-deposition in Electrochemical Processes

Research Project

Project/Area Number14550685
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionNagaoka University of Technology

Principal Investigator

MATSUBARA Hiroshi  Nagaoka University of Technology, Analysis and Instrumentation Center, Associate professor, 分析計測センター, 助教授 (00202325)

Project Period (FY) 2002 – 2003
Project Status Completed(Fiscal Year 2003)
Budget Amount *help
¥3,300,000 (Direct Cost : ¥3,300,000)
Fiscal Year 2003 : ¥1,000,000 (Direct Cost : ¥1,000,000)
Fiscal Year 2002 : ¥2,300,000 (Direct Cost : ¥2,300,000)
KeywordsElectroless Plating / Nanoparticle / Composite Plating / Nanodiamond / Cluster Diamond / 初期析出 / 微細構造
Research Abstract

At first, co-deposition. conditions of nanoparticles into electrolessly plated films were studied. Effects of concentration, temperature and pH of the baths were investigated. Size of particles also affected co-deposition characteristics. Next co-deposition mechanism of nanoparticles into electrolessly plated films were studied in detail. It was suggested that nanodiamond particles were co-deposited into the film after adsorption of metal ion onto the surface of the particles. It was found that citrate complex of nickel effectively adsorbed on the surface of nanodiamond particles and the particles co-deposited large amount. Charge of particles in solutions seemed to have no effect on the co-deposition mechanism. No aggregation of the paticles was observed by transmission electron microscope. It was also found that direct observation of nanodiamond particles was impossible.

Report

(3results)
  • 2003 Annual Research Report   Final Research Report Summary
  • 2002 Annual Research Report

Research Products

(6results)

All Other

All Publications

  • [Publications] 松原 浩, 田澤尚志, 斉藤信雄, 西山 洋, 井上泰宜, 黛 政男: "無電解ニッケルめっき膜中へのクラスターダイヤモンド微粒子の共析"表面技術. 第54巻第5号. 374-375 (2003)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] Hiroshi MATSUBARA, Mikinori KOBAYASHI, Hiroshi NISHIYAMA, Nobuo SAITO, Yasunobu INOUE, Masao MAYUZUMI: "Co-deposition Characteristics of Nanodiamond Particles in Electrolessly Plated Nickel Films"Electrochemistry. Vol.72,No.6. 446-448 (2004)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] Hiroshi MATSUBARA, Hisashi TAZAWA, Nobuo SAITO, Hiroshi NISHIYAMA, Yasunobu INOUE, Masao MAYUZUMI: "Co-Deposition of Cluster Diamond into Electrolessly Plated Nickel Films"Journal of the Surface Finishing Society of Japan. 54. 374-375 (2003)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] Hiroshi MATSUBARA, Mikinori KOBAYASHI, Hiroshi NISHIYAMA, Nobuo SAITO, Yasunobu INOUE, Masao MAYUZUMI: "Co-Deposition Characteristics of Nanodiamond Particles in Electrolessly Plated Nickel Film"Electrochemistry. 72. 446-448 (2004)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2003 Final Research Report Summary
  • [Publications] 松原 浩, 田澤尚志, 斉藤信雄, 西山 洋, 井上泰宣, 黛 政男: "無電解ニッケルめっき膜中へのクラスターダイヤモンド微粒子の共析"表面技術. 第54巻第5号. 374-375 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] Hiroshi MATSUBARA, Mikinori KOBAYASHI, Hiroshi NISHIYAMA, Nobuo SAITO, Yasunobu INOUE, Masao MAYUZUMI: "Co-deposition Characteristics of Nanodiamond Particles in Electrolessly Plated Nickel Films"Electrochemistry. Vol.72,No.6(印刷中). (2004)

    • Related Report
      2003 Annual Research Report

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Published : 2002-04-01   Modified : 2016-04-21  

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