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Fabrication of Intermetallic Fiber/Metal Matrix Graded and/or Smart Composites by a Reaction at Narrow Holes Method

Research Project

Project/Area Number 15560596
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Composite materials/Physical properties
Research InstitutionShinshu University

Principal Investigator

WATANABE Yoshimi  Shinshu University, Faculty of Textile and Technology Dept.of Functional Machinary and Mechanics, Associate Professor, 繊維学部, 助教授 (50231014)

Project Period (FY) 2003 – 2004
Project Status Completed (Fiscal Year 2004)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,900,000)
Fiscal Year 2004: ¥700,000 (Direct Cost: ¥700,000)
Fiscal Year 2003: ¥3,200,000 (Direct Cost: ¥3,200,000)
KeywordsFiber Reinforced Composite / Intermetallic Compound / Fiber / Reaction / Functionally Graded Material / Nickel-aluminide / Hardness / Copper-Aluminum System / 界面
Research Abstract

The reaction at narrow holes method (RANH method) has been proposed as a method for fabricating an intermetallic compound fiber/metal matrix composite. Narrow holes having a small diameter are drilled in a metal matrix A. Metal fibers B are inserted into these narrow holes. The assembly comprising the metal matrix A and metal fibers B is heated at elevated temperatures to obtain molten metal B in the narrow holes. Then, the reaction of mA+nB→AmBn should occur at least in the narrow holes. After the processing, the assembly is cooled to ambient temperature. Consequently, the intermetallic compound AmBn fiber/metal matrix A composite can be fabricated.
In this study, a nickel-aluminides fiber/nickel composite and a copper-aluminum system composite are fabricated by the novel method, RANH method. The results are summarized as follows.
Nickel-aluminides fiber/nickel composite
1)Reacted region is limited to the fiber shaped region, since the nickel-aluminide replaces the pure aluminum maintaining its fiber shape surrounded by the nickel matrix.
2)High hardness could be achieved for specimens beat-treated at 1000 ℃.
3)Specimens heat-treated at 1000 ℃ and 1200 ℃ have lots of pores.
Copper-aluminum system composite
1)Double annular regions are formed around the hole by heating at a temperature less than about 700 ℃. The inner annular region consists of γ1 intermetallic compound in a single phase having very high hardness. The outer annular region consists of Al-Cu solid-solution having a mid-level hardness. The annular regions may work as a reinforcing metal fiber in FRM.
2)When the annular region is formed with a constant width along the edge of the hole, the resultant specimen has the hole maintaining its circular section shape of the original narrow hole.

Report

(3 results)
  • 2004 Annual Research Report   Final Research Report Summary
  • 2003 Annual Research Report
  • Research Products

    (10 results)

All 2005 2004 2003 Other

All Journal Article (8 results) Book (1 results) Publications (1 results)

  • [Journal Article] Graded Microstructure at Fiber / Copper Matrix Interface in FRM Fabricated by a Reaction at Narrow Holes Method2005

    • Author(s)
      Yasuhiko Tanaka, Takeshi Goto, Yoshimi Watanabe
    • Journal Title

      Materials Science Forum 492-493

      Pages: 737-742

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Graded Microstructure at Fiber/Copper Matrix Interface in FRM Fabricated by a Reaction at Narrow Holes Method2005

    • Author(s)
      Yasuhiko Tanaka, Takeshi Goto, Yoshimi Watanabe
    • Journal Title

      Materials Science Forum 492-493

      Pages: 737-742

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Graded Microstructure at Fiber / Copper Matrix Interface in FRM Fabricated by a Reaction at Narrow Holes Method2005

    • Author(s)
      Yasuhiko Tanaka, Takeshi Got, Yoshimi Watanabe
    • Journal Title

      Materials Science Forum 492-493

      Pages: 737-742

    • Related Report
      2004 Annual Research Report
  • [Journal Article] 細孔反応法で作製した繊維強化複合材料における繊維/母相間の組織傾斜2004

    • Author(s)
      渡辺義見, 後藤岳志
    • Journal Title

      2003年度傾斜機能材料論文集

      Pages: 81-86

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] 金属間化合物を強化相とした連続繊維強化複合材料製造法の提案-細孔反応法とは-2004

    • Author(s)
      渡辺義見
    • Journal Title

      バウンダリー 20(10)

      Pages: 10-12

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] Graded Microstructure at Fiber/Matrix Interface in FRM Fabricated by the Reaction at Narrow Holes Method2004

    • Author(s)
      Yoshimi Watanabe, Takeshi Goto
    • Journal Title

      Functionally Graded Materials 2003

      Pages: 81-86

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Fabrication of Nickel-Aluminides Fiber / Nickel Composite by Reaction at Narrow Holes2003

    • Author(s)
      Yoshimi Watanabe, Takeshi Goto
    • Journal Title

      Materials Science Forum 426-432

      Pages: 1957-1962

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] Fabrication of Nickel-Aluminides Fiber/Nickel Composite by Reaction at Narrow Holes2003

    • Author(s)
      Yoshimi Watanabe, Takeshi Goto
    • Journal Title

      Materials Science Forum 426-432

      Pages: 1957-1962

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Book] ファイバー工学2005

    • Author(s)
      渡辺義見
    • Publisher
      丸善
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Publications] 渡辺義見, 後藤岳志: "細孔反応法で作製した繊維強化複合材料における繊維/母相間の組織傾斜"平成15年度傾斜機能材料論文集. (印刷中). (2004)

    • Related Report
      2003 Annual Research Report

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Published: 2003-04-01   Modified: 2016-04-21  

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