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Recovery of Damage Indued by Irradiation Reactor Pressure Vessel Steels

Research Project

Project/Area Number 15560725
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Nuclear engineering
Research InstitutionKyoto Universily

Principal Investigator

XU Qiu  Kyoto University, Research Reactor Institute, Associate Prof., 原子炉実験所, 助教授 (90273531)

Co-Investigator(Kenkyū-buntansha) YOSHIIE Toshimasa  Kyoto University, Research Reactor Institute, Prof., 原子炉実験所, 教授 (20124844)
Project Period (FY) 2003 – 2005
Project Status Completed (Fiscal Year 2005)
Budget Amount *help
¥3,600,000 (Direct Cost: ¥3,600,000)
Fiscal Year 2005: ¥900,000 (Direct Cost: ¥900,000)
Fiscal Year 2004: ¥1,000,000 (Direct Cost: ¥1,000,000)
Fiscal Year 2003: ¥1,700,000 (Direct Cost: ¥1,700,000)
KeywordsReactor Pressure Vessel Steel / Fe-Cu Alloys / Neutron Irradiation / Positron Lifetime / Doppler Broadening / Vacancy Cluster / Interstitial Cluster / Cu Precipitate / 同時計数ドップラー広がり / 欠陥の回復
Research Abstract

The main purpose of the present study was to investigate the mechanism of miorostructural evolution in dilute Fe-Cu alloys, the model alloys of the reactor pressure vessel steels, and the range of vary temperature under vary temperature irradiation.
Before investigation of effect of vary temperature on the microstructural evolution, it is necessary to investigate the miorostructural evolution at constant temperature. Two Fe-Cu alloys, namely Fe-0.3Cu and Fe-0.6Cu, were tested in this study. The neutron irradiations were carried out at the Kyoto University Reactor at 573 K. The results indicate that there are three stages in the formation of Cu precipitates. First, the precipitates nucleate by vacancy migration. Second, microvoids form and grow at these precipitates sites, and then the aggregation of Cu atoms is promoted at these microvoids because the surface energy of Cu is lower than that of Fe. Third, the microvoids form and grow in the matrix without any connection with Cu precipita … More tes.
Two types of vary temperature irradiations, 573 K/723 K and 573 K/673 K, were carried out to investigate the recovery behavior of defect clusters Fe-Cu alloys. Microvoids and interstitial clusters disappeared, and Cu precipitates grew under vary temperature irradiation. The disappearance of microvoids and interstitial clusters was more prominent in the irradiation than in the annealing at 723 K. The recovery of microvoids and interstitial clusters and the formation of Cu precipitates in the irradiation of 573 K/723 K were more prominent than those in the irradiation of 573 K/673 K. In addition, the irradiation dose at low temperature also influenced the microstructural evolution during subsequent irradiation at high temperature. The results suggest that the lower the irradiation dose at 573 K, the greater the extent recovery of defect clusters in Fe-Cu alloys during irradiation at 673 K. They also suggest that a higher irradiation dose is needed to recover the defect clusters formed at 573 K with low irradiation dose. Inversely, a lower irradiation dose is needed to recover the defect clusters formed at 573 K with high irradiation dose. Less

Report

(4 results)
  • 2005 Annual Research Report   Final Research Report Summary
  • 2004 Annual Research Report
  • 2003 Annual Research Report
  • Research Products

    (52 results)

All 2006 2005 2004 2003 Other

All Journal Article (46 results) Publications (6 results)

  • [Journal Article] Dose Dependence Of Cu Precipitate Formation in Fe-Cu Model Alloys Irradiated with Fission Neutrons.2006

    • Author(s)
      Q.Xu, T.Yoshiie, K.Sato
    • Journal Title

      Physical Review B 73

      Pages: 134115-134115

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Effects of Oversized Element Sn on Diffusion of Interstitial Clusters in Ni Irradiated by Ions and Neutrons.2006

    • Author(s)
      Q.Xu, T.Yoshiie, H.Watanabe, N.Yoshida
    • Journal Title

      Journal of Nuclear Materials (in press)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Thermally Stimulated Current Studies on Neutron Irradiation Induced Defects in GaN2006

    • Author(s)
      K.Kuriyama, M.Ooi, A.Onoue, K.Kushida, M.Okada, Q.Xu
    • Journal Title

      Applied Physics Letters 88

      Pages: 132109-132109

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Dose Dependence Of Cu Precipitate Formation in Fe-Cu Model Alloys Irradiated with Fission Neutrons2006

    • Author(s)
      Q.Xu, T.Yoshuie, K.Sato
    • Journal Title

      Physical Review B 73

      Pages: 134115-134115

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Effects of Oversized Element Sn on Diffusion of Interstitial Clusters in Ni Irradiated by Ions and Neutrons2006

    • Author(s)
      Q.Xu, T.Yoshiie, H.Watanabe, N.Yoshida
    • Journal Title

      Journal of Nuclear Materials (in press)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Thermally Stimulated Current Studies on Neutron Irradiation Induced Defects in GaN2006

    • Author(s)
      K.Kuriyama, M.Ooi, A.Onoue, K.Kushida, M.Okada, O.Xu
    • Journal Title

      Applied Physics Letters 88

      Pages: 132109-132109

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Dose Dependence of Cu Precipitate Fomation in Fe-Cu Model Alloys Irradiated with Fission Neutrons2006

    • Author(s)
      Q.Xu, T.Yoshiie, K.Sato
    • Journal Title

      Physical Review B (in press)

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Dynamic Simulation of Multiplier Effects of Helium Plasma and Neutron Irradiation on Microstructural Evolution in Tungsten.2005

    • Author(s)
      Q.Xu, N.Yoshida, T.Yoshiie
    • Journal Title

      Materials Transactions, JIM 46

      Pages: 1255-1260

    • NAID

      10016438842

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Defect Structural Evolution in High Purity Tungsten Irradiated with Electrons using High Voltage Electron Microscope.2005

    • Author(s)
      S.Fukuzumi, T.Yoshiie, Y.Satoh, Q.Xu, H.Mori, M.Kawai
    • Journal Title

      Journal of Nuclear Materials 343

      Pages: 308-312

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Point Defect Formation in V-4Cr-4Ti and F82H Irradiated with Fission And Fusion Neutrons. Materials Transactions.2005

    • Author(s)
      K.Sato, T.Yoshiie, Q.Xu, Y.Satoh, E.Wakai, C.Kutsukake, T.Nishitani
    • Journal Title

      Materials Transactions, JIM 46

      Pages: 308-312

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Effect of Impurities on Vacancy Mobility in V-4Cr-4Ti.2005

    • Author(s)
      Q.Xu, T.Yoshiie, T.Nagasaka, T.Muroga
    • Journal Title

      Materials Science Forum 475-479

      Pages: 1441-1444

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Dynamic Simulation of Multiplier Effects of Helium Plasma and Neutron Irradiation on Microstructural Evolution in Tungsten2005

    • Author(s)
      Q.Xu, N.Yoshida, T.Yoshiie
    • Journal Title

      Materials Transactions, JIM 46

      Pages: 1255-1260

    • NAID

      10016438842

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Defect Structural Evolution in High Purity Tungsten Irradiated with Electrons using High Voltage Electron Microscope2005

    • Author(s)
      S.Fukuzumi, T.Yoshiie, Y.Satoh, Q.Xu, H.Mori, M.Kawai
    • Journal Title

      Journal of Nuclear Materials 343

      Pages: 308-312

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Point Defect Formation in V-4Cr-4Ti and F82H Irradiated with Fission and Fusion Neutrons. Materials Transactions.2005

    • Author(s)
      K.Sato, T.Yoshiie, Q.Xu, Y.Satoh, E.Wakai, C.Kutsukake, T.Nishitani
    • Journal Title

      Materials Transactions, JIM 46,No.3

      Pages: 445-449

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Effect of Impurities on Vacancy Mobility in V-4Cr-4Ti2005

    • Author(s)
      Q.Xu, T.Yoshiie, T.Nagasaka, T.Muroga
    • Journal Title

      Materials Science Forum 475-479

      Pages: 1441-1444

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Dynamic Simulation of Multiplier Efeccts of Helium Plasma and Neutron Irradiation on Microstructural Evolution in Tungsten2005

    • Author(s)
      Q.Xu, N.Yoshida, T.Yoshiie
    • Journal Title

      Materials Transactions, JIM 46・6

      Pages: 1255-1260

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Defect Structural Evolution in High Purity Tungsten Irradiated with Electrons Using High Votage Electron Microscope2005

    • Author(s)
      S.Fukuzimi, T.Yoshiie, Y.Satoh, Q.Xu
    • Journal Title

      Journal of Nuclear Materials 343

      Pages: 308-312

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Effect of Impurities on Vacancy Mobility in V-4Cr-4Ti2005

    • Author(s)
      O.Xu, T.Yoshiie et al.
    • Journal Title

      Materials Science Forum 475-479

      Pages: 1441-1444

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Point Defect Formation in V-4Cr-4Ti and F82H Irradiated with Fission and Fusion Neutrons2005

    • Author(s)
      K.Sato, T.Yoshiie, O.Xu et al.
    • Journal Title

      Materials Transactions, JIM 46・3

      Pages: 1-5

    • NAID

      10015578601

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Microstructural Evolution and Hardness Changes in the Interface of Cu/316L Joint Materials under Aging and Ion Irradiation.2004

    • Author(s)
      Q.Xu, T.Yoshiie, T.Muroga, N.Yoshida, T.Iwai, D.J.Edwards
    • Journal Title

      Journal of Nuclear Materials 329-333

      Pages: 1558-1562

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Recovery Behavior of Defect Clusters in Fe-Cu Alloy Irradiated with Neutrons at High Temperature.2004

    • Author(s)
      Q.Xu, T.Yoshiie
    • Journal Title

      Materials Science Forum 445-446

      Pages: 216-218

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Comparison of Defect Structures in Fe-Cu Alloys Introduced by High-speed and Low-speed Deformation.2004

    • Author(s)
      T.Ishizaki, T.Yoshiie, Q.Xu, M.Komastu
    • Journal Title

      Materials Science Forum 445-446

      Pages: 117-119

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Anisotropic Motion of Point Defects near Edge Dislocations.2004

    • Author(s)
      K.Sato, T.Yoshiie, Q.Xu
    • Journal Title

      Journal of Nuclear Materials 329-333

      Pages: 929-932

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Detection of Interstitials and Their Clusters by PAC and Positron Lifetime Measurements on Neutron Irradiated Ni-Hf Alloy.2004

    • Author(s)
      H.Okazawa, T.Yoshiie, T.Ishizaki, K.Sato, Q.Xu, Y.Satoh, Y.Ohkubo, Y.Kawase
    • Journal Title

      Journal of Nuclear Materials 329-333

      Pages: 967-970

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Analysis of Defect Structural Evolution in FCC Metals Irradiated with Neutrons under Well Defined Boundary Conditions.2004

    • Author(s)
      T.Yoshiie, Y.Satoh, Q.Xu
    • Journal Title

      Journal of Nuclear Materials 329-333

      Pages: 81-87

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Computer Simulation of Formation Energy and Migration Energy of Vacancies under High Strain in Cu2004

    • Author(s)
      K.Sato, T.Yoshiie, Y.Satoh, Q.Xu
    • Journal Title

      Materials Transactions, JIM 45

      Pages: 833-838

    • NAID

      10012717207

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] The Effect of Hydrogen-charge in Neutron Irradiated Nickel Studied by Positron Annihilation.2004

    • Author(s)
      C.He, Q.Xu, T.Yoshiie, K.Sato, D.Troev
    • Journal Title

      Materials Science Forum 445-446

      Pages: 105-107

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] The Recovery of Gas-Vacancy-Complexes in Fe Irradiated with High Energy H or He Ions.2004

    • Author(s)
      T.Ishizaki, Q.Xu, T.Yoshiie, S.Nagata
    • Journal Title

      Materials Transactions, JIM 45

      Pages: 9-12

    • NAID

      10011981446

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Microstructural Evolution and Hardness Changes in the Interface of Cu/316L Joint Materials under Aging and Ion Irradiation2004

    • Author(s)
      Q.Xu, T.Yoshiie, T.Muroga, N.Yoshida, T.Iwai, D.J.Edwards
    • Journal Title

      Journal of Nuclear Materials 329-333

      Pages: 1558-1562

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Recovery Behavior of Defect Clusters in Fe-Cu Alloy Irradiated with Neutrons at High Temperature2004

    • Author(s)
      Q.Xu, T.Yoshiie
    • Journal Title

      Materials Science Forum 445-446

      Pages: 216-218

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Comparison of Defect Structures in Fe-Cu Alloys Introduced by High-speed and Low-speed Deformation2004

    • Author(s)
      T.Ishizaki, T.Yoshiie, Q.Xu, M.Komastu
    • Journal Title

      Materials Science Forum 445-446

      Pages: 117-119

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Anisotropic Motion of Point Defects near Edge Dislocations2004

    • Author(s)
      K.Sato, T.Yoshiie, Q.Xuv
    • Journal Title

      Journal of Nuclear Materials 329-333

      Pages: 929-932

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Detection of Interstitials and Their Clusters by PAC and Positron Lifetime Measurements on Neutron Irradiated Ni-Hf Alloy2004

    • Author(s)
      H.Okazawa, T.Yoshiie, T.Ishizaki, K.Sato, Q.Xu, Y.Satoh, Y.Ohkubo, Y.Kawase
    • Journal Title

      Journal of Nuclear Materials 329-333

      Pages: 967-970

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Computer Simulation of Formation Energy and Migration Energy of Vacancies under High Strain in Cu.2004

    • Author(s)
      K.Sato, T.Yoshiie, Y.Satoh, Q.Xu
    • Journal Title

      Materials Transactions, JIM 45,No.3

      Pages: 833-838

    • NAID

      10012717207

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] The Recovery of Gas-Vacancy-Complexes in Fe Irradiated with High Energy H or He Ions.2004

    • Author(s)
      T.Ishizaki, Q.Xu, T.Yoshiie, S.Nagata
    • Journal Title

      Materials Transactions, JIM 45,No.1

      Pages: 9-12

    • NAID

      10011981446

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Microstructural Evolution and Hardness Changes in the Interface of Cu/316L Joint Materials under Aging and Ion Irradiation2004

    • Author(s)
      O.Xu, T.Yoshiie et al.
    • Journal Title

      Journal of Nuclear Materials 329-333

      Pages: 1558-1562

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Anisotropic Motion of Point Defects near Edge Dislocations2004

    • Author(s)
      K.Sato, T.Yoshiie, O.Xu et al.
    • Journal Title

      Journal of Nuclear Materials 329-333

      Pages: 929-932

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Analysis of Defect Structural Evolution in FCC Metals Irradiated with Neutrons under Well Defined Boundary Conditions2004

    • Author(s)
      T.Yoshiie, K.Sato, O.Xu et al.
    • Journal Title

      Journal of Nuclear Materials 329-333

      Pages: 81-87

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Computer Simulation of Formation Energy and Migration Energy of Vacancy under high Strain in Cu2004

    • Author(s)
      K.Sato, T.Yoshiie, O.Xu et al.
    • Journal Title

      Materials Transactions, JIM 45・3

      Pages: 833-838

    • NAID

      10012717207

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Precipitation of Cu in Fe-Cu Alloys by High-Speed Deformation.2003

    • Author(s)
      T.Ishizaki, T.Yoshiie, K.Sato, S.Yanagita, Q.Xu, M.Komastu, M.Kiritani
    • Journal Title

      Materrials Science and Engineering A350

      Pages: 102-107

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Simulation of Vacancy Migration Energy in Cu under High Strain.2003

    • Author(s)
      K.Sato, T.Yoshiie, Y.Satoh, Q.Xu, M.Kiritani
    • Journal Title

      Materrials Science and Engineering A350

      Pages: 220-222

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Molecular Dynamics Simulation of Vacancy Diffusion in Tungsten Induced by Irradiation.2003

    • Author(s)
      Q.Xu, T.Yoshiie, H.C.Huang
    • Journal Title

      Nuclear Instruments and Methods in Physics Research B 206

      Pages: 123-126

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] A New Materials Irradiation Facility at the Kyoto University Reactor.2003

    • Author(s)
      T.Yoshiie, Y.Hayashi, S.Yanagita, Q.Xu
    • Journal Title

      Nuclear Instruments and Methods in Physics Research A 498

      Pages: 522-531

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Simulation of Vacancy Migration Energy in Cu under High Strain.2003

    • Author(s)
      K.Sato, T.Yoshiie, Y.Satoh, Q.Xu, M.Kiritani
    • Journal Title

      Materials Science and Engineering A350

      Pages: 220-222

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Precipitation of Cu in Fe-Cu Alloys by High-Speed Deformation.2003

    • Author(s)
      T.Ishizaki, T.Yoshiie, K.Sato, S.Yanagita, Q.Xu, M.Komastu, M.Kiritani
    • Journal Title

      Materials Science and Engineering A350

      Pages: 102-107

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] A New Materials Irradiation Facility at the Kyoto University Reactor2003

    • Author(s)
      T.Yoshiie, Y.Hayashi, S.Yanagita, Y.Satoh, H.Tsujimoto, T.Kozuka, K.Kamae, K.Mishima, S.Shiroya, K.Kobayashi, M.Utsuro, Y.Fujita
    • Journal Title

      Nuclear Instruments and Methods in Physics Research A 498

      Pages: 522-531

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Publications] Q.Xu, T.Yoshiie: "Recovery Behavior of Defect Clusters in Fe-Cu Alloy Irradiated with Neutrons at High Temperature"Materials Science Forum. 445-446. 216-218 (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] T.Ishizaki, T.Yoshiie, Q.Xu, M.Komastu: "Comparison of Defect Structures in Fe-Cu Alloys Introduced by High-speed and Low-speed Deformation"Materials Science Forum. 445-446. 117-119 (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] T.Ishizaki, Q.Xu, T.Yoshiie, S.Nagata: "The Recovery of Gas-vacancy-Complexes in Fe Irradiated with High Energy H or He Ions"Materials Transactions. 45. 9-12 (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] T.Ishizaki, T.Yoshiie, K.Sato, S.Yanagita, Q.Xu: "Precipitation of Cu in Fe-Cu Alloys by High-Speed Deformation"Material Science & Engineering. A350. 102-107 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] Q.Xu, T.Yoshiie, H.C.Huang: "Molecular Dynamics Simulation of Vacancy Diffusion in Tungsten Induced by Irradiation"Nuclear Instruments & Methods in Physics Research. B206. 123-126 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] K.Sato, T.Yoshiie, Y.Satoh, Q.Xu, M.Kiritani: "Simulation of Vacancy Migration Energy in Cu under High Strain"Material Science & Engineering. A350. 220-222 (2003)

    • Related Report
      2003 Annual Research Report

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Published: 2003-04-01   Modified: 2016-04-21  

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