Advanced application of atmospheric-pressure plasma jet using a surgical needle to microfabrication
Project/Area Number |
17560645
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Research Category |
Grant-in-Aid for Scientific Research (C)
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Allocation Type | Single-year Grants |
Section | 一般 |
Research Field |
Material processing/treatments
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Research Institution | Tsuruoka National College of Technology |
Principal Investigator |
YOSHIKI Hiroyuki Tsuruoka National College of Technology, General Education, Associate Professor, 総合科学科, 准教授 (00300525)
|
Project Period (FY) |
2005 – 2006
|
Project Status |
Completed (Fiscal Year 2006)
|
Budget Amount *help |
¥3,600,000 (Direct Cost: ¥3,600,000)
Fiscal Year 2006: ¥1,000,000 (Direct Cost: ¥1,000,000)
Fiscal Year 2005: ¥2,600,000 (Direct Cost: ¥2,600,000)
|
Keywords | Plasma processing / Plasma jet / Surgical needle / Atmospheric-pressure plasma / Removal of insulator films / Localized etching / Carbon nanotubes / Localized CVD / プラズマ加工 / 局所CVD成長 |
Research Abstract |
Atmospheric-pressure microplasma jets (AP μ PJs) of Ar, Ar/0_2 and air were generated from the tip of a stainless steel surgical needle having outer and inner diameter of 0.4 and 0.2 mm, respectively, with a rf excitation of 13.56 MHz. The steel needle functions both as a powered electrode and gas nozzle. The operating power is 1-6 W and the corresponding peak-to-peak voltage is about 1.5 kV. The AP μ PJ was applied to the localized etching of a polyamide-imide insulator film (thickness of 10 μ m) of a copper winding wire of 90μ m diameter. The insulator film around the copper wire was completely removed by the irradiated plasma from a certain direction without fusing the wire. The removal time under the Ar AP μ PJ irradiation was only 3 s at a rf power of 4 W. Fluorescence microscopy and scanning electron microscope images reveal that good selectivity of the insulator film to the copper wire was achieved. Vertically aligned bundles of multiwalled carbon nanotubes (MWNTs) were grown on the tip of a φ 0.5 mm Ni wire using an AP μ PJ generated by a RF-powered surgical needle. A CH_4/H_2 gas mixture was used for the source gas, and the Ni wire used as the substrate was negatively biased to heat it by ion bombardment. At a ratio of CH_4:H_2=1:35,a RF power of 6 W, a DC bias voltage of-100 V and a growth time of 2 min, the tip of the Ni wire was covered by bamboo-like MWNT bundles, whose diameter and length were about 600 nm and 2-3μm, respectively. Each bundle consisted of about 1500 tubes with diameters of 10-25 nm. The growth temperature of the MWNT bundles was approximately 500℃.
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Report
(3 results)
Research Products
(17 results)