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Elucidation of the mechanism of very high cycle fatigue and the development of its evaluation method based on synchrotron radiation micro/nano- CT

Research Project

Project/Area Number 18H03748
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Review Section Medium-sized Section 18:Mechanics of materials, production engineering, design engineering, and related fields
Research InstitutionHokkaido University

Principal Investigator

Nakamura Takashi  北海道大学, 工学研究院, 教授 (30237408)

Co-Investigator(Kenkyū-buntansha) 戸田 裕之  九州大学, 工学研究院, 教授 (70293751)
藤村 奈央  北海道大学, 工学研究院, 助教 (40732988)
竹内 晃久  公益財団法人高輝度光科学研究センター, 分光・イメージング推進室, 主幹研究員 (70426526)
上杉 健太朗  公益財団法人高輝度光科学研究センター, 分光・イメージング推進室, 主席研究員 (80344399)
古谷 佳之  国立研究開発法人物質・材料研究機構, 構造材料研究拠点, グループリーダー (60354255)
小熊 博幸  国立研究開発法人物質・材料研究機構, 構造材料研究拠点, 主幹研究員 (80515122)
Project Period (FY) 2018-04-01 – 2022-03-31
Project Status Completed (Fiscal Year 2021)
Budget Amount *help
¥45,240,000 (Direct Cost: ¥34,800,000、Indirect Cost: ¥10,440,000)
Fiscal Year 2021: ¥5,460,000 (Direct Cost: ¥4,200,000、Indirect Cost: ¥1,260,000)
Fiscal Year 2020: ¥6,630,000 (Direct Cost: ¥5,100,000、Indirect Cost: ¥1,530,000)
Fiscal Year 2019: ¥6,370,000 (Direct Cost: ¥4,900,000、Indirect Cost: ¥1,470,000)
Fiscal Year 2018: ¥26,780,000 (Direct Cost: ¥20,600,000、Indirect Cost: ¥6,180,000)
Keywordsギガサイクル疲労 / 内部起点型破壊 / 真空 / 放射光 / き裂進展 / き裂伝搬 / 疲労
Outline of Final Research Achievements

The study aims to clarify the mechanism of very high cycle fatigue, which deteriorates the fatigue strength in the long-life regime due to the crack initiation inside materials. A nondestructive inspection technique of small cracks with a few micrometers was developed using synchrotron radiation X-ray computed tomography (SR-CT) at SPring-8. The SR-CT revealed that the crack growth rate of internal crack was much lower than that of surface crack and almost similar to that in a high vacuum. Fatigue fracture in the very high cycle regime can result from the extremely low internal crack growth rate, which propagates in a vacuum-like environment in materials.

Academic Significance and Societal Importance of the Research Achievements

超高張力鋼やチタン合金等の高強度金属において,長寿命で疲労強度が低下する現象(超高サイクル疲労)が近年広く知られるようになった.これは材料内部を起点とするき裂の発生・進展により生じるが,内部き裂の検出が困難なことから,その破壊機構は明らかにされていない.本研究は, SPring-8における放射光X線CTを用いて数十μmの内部微小疲労き裂をSEMレベルの分解能で観察する技術を構築し,これまで全く明らかにされていなかった内部き裂の挙動を解明することを目的としている.本研究の成果は最先端非破壊検査技術のさらなる高度化,疲労強度学の発展,超高サイクル疲労評価法の構築等に寄与するものである.

Report

(4 results)
  • 2021 Final Research Report ( PDF )
  • 2020 Annual Research Report
  • 2019 Annual Research Report
  • 2018 Annual Research Report
  • Research Products

    (45 results)

All 2021 2020 2019 2018

All Journal Article (24 results) (of which Peer Reviewed: 12 results,  Open Access: 4 results) Presentation (21 results) (of which Int'l Joint Research: 7 results,  Invited: 3 results)

  • [Journal Article] Initiation and Propagation Processes of Internal Fatigue Cracks in β Titanium Alloy Based on Fractographic Analysis2021

    • Author(s)
      Xue Gaoge、Nakamura Takashi、Fujimura Nao、Takahashi Kosuke、Oguma Hiroyuki
    • Journal Title

      Applied Sciences

      Volume: 11 Issue: 1 Pages: 131-131

    • DOI

      10.3390/app11010131

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Effect of vacuum pressure on small crack propagation in Ti-6Al-4V2021

    • Author(s)
      Yoshinaka Fumiyoshi、Xue Gaoge、Fujimura Nao、Nakamura Takashi
    • Journal Title

      International Journal of Fatigue

      Volume: 142 Pages: 105961-105961

    • DOI

      10.1016/j.ijfatigue.2020.105961

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Detection of small internal fatigue cracks of TI-6Al-4V in the very high cycle regime via synchrotron radiation nanocomputed tomography2021

    • Author(s)
      Nakamura Takashi, Fujimura Nao, Tomoda Yuta, Xue Gaoge, Yoshinaka Fumiyoshi, Takeuchi Akihisa, Uesugi Masayuki, Uesugi Kentaro
    • Journal Title

      Proceedings of the 8th Engineering Integrity Society International Conference on Durability & Fatigue, 2021

      Volume: - Pages: 349-357

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed
  • [Journal Article] High-energy x-ray nanotomography introducing an apodization Fresnel zone plate objective lens2021

    • Author(s)
      A. Takeuchi, K. Uesugi, M. Uesugi, H. Toda, K. Hirayama, K. Shimizu, K. Matsuo and T. Nakamura
    • Journal Title

      Review of Scientific Instruments

      Volume: 92 Issue: 2 Pages: 023701-023701

    • DOI

      10.1063/5.0020293

    • NAID

      120007187739

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Recent progress in synchrotron radiation 3D-4D nano-imaging based on X-ray full-field microscopy2020

    • Author(s)
      Takeuchi Akihisa, Suzuki Yoshio
    • Journal Title

      Microscopy

      Volume: 69 Issue: 5 Pages: 259-279

    • DOI

      10.1093/jmicro/dfaa022

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed
  • [Journal Article] SCM440鋼のギガサイクル疲労特性に及ぼすMnSの影響2020

    • Author(s)
      古谷佳之
    • Journal Title

      鉄と鋼

      Volume: 106 Issue: 11 Pages: 799-806

    • DOI

      10.2355/tetsutohagane.tetsu-2020-051

    • NAID

      130007932329

    • Related Report
      2020 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Initiation and growth behaviour of small internal fatigue cracks in Ti‐6Al‐4V via synchrotron radiation microcomputed tomography2019

    • Author(s)
      Yoshinaka Fumiyoshi、Nakamura Takashi、Takeuchi Akihisa、Uesugi Masayuki、Uesugi Kentaro
    • Journal Title

      Fatigue & Fracture of Engineering Materials & Structures

      Volume: 42 Issue: 9 Pages: 2093-2105

    • DOI

      10.1111/ffe.13085

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effects of vacuum-like environment on small internal crack growth processes in very high cycle fatigue2019

    • Author(s)
      Nakamura Takashi、Yoshinaka Fumiyoshi
    • Journal Title

      Procedia Structural Integrity

      Volume: 14 Pages: 978-985

    • DOI

      10.1016/j.prostr.2019.07.079

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 10<sup>11</sup>-cycle Gigacycle Fatigue Properties of High-strength Steel2019

    • Author(s)
      古谷 佳之
    • Journal Title

      Tetsu-to-Hagane

      Volume: 105 Issue: 12 Pages: 1173-1178

    • DOI

      10.2355/tetsutohagane.TETSU-2019-071

    • NAID

      130007753127

    • ISSN
      0021-1575, 1883-2954
    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 放射光X線CTによるTi-6Al-4Vにおける超高サイクル疲労過程の観察2019

    • Author(s)
      吉中 奎貴、中村孝
    • Journal Title

      チタン

      Volume: 67 Pages: 184-188

    • NAID

      40021981405

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 放射光顕微CTによる内部微小疲労き裂発生・進展過程の観察2019

    • Author(s)
      中村孝
    • Journal Title

      日本材料学会第68期学術講演会講演論文集

      Volume: - Pages: 231-232

    • Related Report
      2019 Annual Research Report
  • [Journal Article] Ti-6Al-4V における表面および内部微小疲労き裂の開閉口挙動2019

    • Author(s)
      友田悠太,中村孝,藤村奈央,吉中奎貴,小熊博幸, 竹内晃久,上椙真之,上杉健太朗
    • Journal Title

      日本材料学会第68期学術講演会講演論文集

      Volume: - Pages: 77-78

    • Related Report
      2019 Annual Research Report
  • [Journal Article] 大気および真空環境における微小疲労き裂の進展・停留挙動2019

    • Author(s)
      塚越拓摩,石原梨沙, Paras Mehendiratta,中村孝,藤村奈央,高橋航圭
    • Journal Title

      日本材料学会第68期学術講演会講演論文集

      Volume: - Pages: 87-88

    • Related Report
      2019 Annual Research Report
  • [Journal Article] 真空環境下におけるき裂進展速度に基づく内部き裂の疲労寿命推定2019

    • Author(s)
      ソラブ クマール モディ,メヘンディラッタパラス,塚越 拓摩, 中村 孝,藤村 奈央,髙橋 航圭
    • Journal Title

      日本機械学会M&M2019 材料力学カンファレンス 講演論文集

      Volume: -

    • NAID

      130007846707

    • Related Report
      2019 Annual Research Report
  • [Journal Article] 放射光顕微CT による高強度金属内部の高分解能非破壊観察2019

    • Author(s)
      今 佑宇真,中村 孝,藤村 奈央,吉中 奎貴,髙橋 航圭,竹内 晃久,上椙 真之,上杉 健太朗
    • Journal Title

      日本機械学会M&M2019 材料力学カンファレンス 講演論文集

      Volume: -

    • NAID

      130007846701

    • Related Report
      2019 Annual Research Report
  • [Journal Article] 破面解析に基づくTi-22V-4Al 合金における内部疲労き裂の発生・進展過程2019

    • Author(s)
      薛 高格,藤村 奈央,中村 孝,小熊 博幸,髙橋 航圭
    • Journal Title

      日本機械学会M&M2019 材料力学カンファレンス 講演論文集

      Volume: -

    • NAID

      130007846526

    • Related Report
      2019 Annual Research Report
  • [Journal Article] 放射光顕微CT によるTi-6Al-4V の内部疲労き裂発生過程2019

    • Author(s)
      中村 孝, 友田 悠太, 藤村 奈央, 吉中 奎貴, 小熊 博幸, 竹内 晃久, 上椙 真之,上杉 健太朗
    • Journal Title

      日本機械学会M&M2019 材料力学カンファレンス 講演論文集

      Volume: -

    • NAID

      130007846525

    • Related Report
      2019 Annual Research Report
  • [Journal Article] 高強度鋼の超高サイクル疲労における疲労限2019

    • Author(s)
      古谷 佳之
    • Journal Title

      日本機械学会M&M2019 材料力学カンファレンス 講演論文集

      Volume: -

    • NAID

      130007846498

    • Related Report
      2019 Annual Research Report
  • [Journal Article] チタン合金の内部起点型疲労破壊における特異な破面領域形成に及ぼす影響因子2019

    • Author(s)
      小熊博幸
    • Journal Title

      日本材料学会第68期学術講演会講演論文集

      Volume: - Pages: 281-282

    • Related Report
      2019 Annual Research Report
  • [Journal Article] Ti6Al4V 合金の内部起点型疲労破壊における特異な破面領域の形成機構と組織との相関2019

    • Author(s)
      小熊 博幸
    • Journal Title

      日本機械学会M&M2019 材料力学カンファレンス 講演論文集

      Volume: -

    • NAID

      130007846548

    • Related Report
      2019 Annual Research Report
  • [Journal Article] A new model for predicting the gigacycle fatigue strength of high-strength steels2019

    • Author(s)
      Y. Furuya
    • Journal Title

      Materials Science & Engineering A

      Volume: 743 Pages: 445-452

    • DOI

      10.1016/j.msea.2018.11.109

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Nondestructive Multiscale X-Ray Tomography by Combining Microtomography and High-Energy Phase-Contrast Nanotomography2018

    • Author(s)
      Akihisa Takeuchi, Kentaro Uesugi, Masayuki Uesugi, Fumiyoshi Yoshinaka and Takashi Nakamura
    • Journal Title

      Microscopy and Microanalysis

      Volume: 24 Issue: S2 Pages: 106-107

    • DOI

      10.1017/s1431927618012928

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Effects of vacuum environment on the fatigue crack growth properties of high strength steel - behavior of long crack by ΔK decreasing test -2018

    • Author(s)
      Paras Mehendiratta, Risa Ishihara, Takashi Nakamura, Nao Fujimura, Kosuke Takahashi
    • Journal Title

      日本機械学会M&M2018材料力学カンファレンス 講演論文集

      Volume: 1

    • NAID

      130007667546

    • Related Report
      2018 Annual Research Report
  • [Journal Article] 高強度鋼の疲労き裂進展特性に及ぼす真空環境の影響ーΔK漸増試験による微小き裂の挙動ー2018

    • Author(s)
      石原梨沙,メヘンディラッタ パラス,中村孝,藤村奈央,高橋航圭
    • Journal Title

      日本機械学会M&M2018材料力学カンファレンス 講演論文集

      Volume: 1

    • NAID

      130007667547

    • Related Report
      2018 Annual Research Report
  • [Presentation] Detection of small internal fatigue cracks of Ti-6Al-4V in the very high cycle regime via synchrotron radiation nanocomputed tomography2021

    • Author(s)
      T. Nakamura, N. Fujimura, Y. Tomoda, G. Xue, F. Yoshinaka, A. Takeuchi, M. Uesugi, K. Uesugi
    • Organizer
      Fatigue 2021
    • Related Report
      2020 Annual Research Report
    • Int'l Joint Research
  • [Presentation] A fractographic study of the initiation and propagation progress of internal fatigue cracks in Ti-22V-4Al with different alpha-phase precipitation2021

    • Author(s)
      G. Xue, T. Nakamura, N. Fujimura, K. Takahashi, H. Oguma
    • Organizer
      Fatigue 2021
    • Related Report
      2020 Annual Research Report
    • Int'l Joint Research
  • [Presentation] A Study of Vacuum Pressure Effect on Small Surface Crack Propagation in Ti-6Al-4V2020

    • Author(s)
      G. Xue, F. Yoshinaka, N. Fujimura, K. Takahashi and T. Nakamura
    • Organizer
      Asia-Pacific Conference on Fracture and Strength 2020
    • Related Report
      2020 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 微小内部き裂の発生・進展挙動に基づくα+β型チタン合金の疲労寿命分布解析2020

    • Author(s)
      森下弘法, 中村孝, 藤村奈央, 髙橋航圭
    • Organizer
      日本材料学会 第69期学術講演会
    • Related Report
      2020 Annual Research Report
  • [Presentation] 放射光を用いるX線マイクロCTの基礎と最前線2020

    • Author(s)
      竹内晃久
    • Organizer
      日本化学会第101春季年会
    • Related Report
      2020 Annual Research Report
    • Invited
  • [Presentation] Initiation and growth behavior of small internal fatigue cracks in Ti-6Al-4V via synchrotron radiation micro computed tomography2019

    • Author(s)
      Takashi Nakamura
    • Organizer
      International Symposium on: Advances in Fatigue and Fracture, Celebrating the 40th Anniversary of FFEMS
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 放射光顕微CTによる内部微小疲労き裂発生・進展過程の観察2019

    • Author(s)
      中村孝
    • Organizer
      日本材料学会第68期学術講演会
    • Related Report
      2019 Annual Research Report
    • Invited
  • [Presentation] Ti-6Al-4V における表面および内部微小疲労き裂の開閉口挙動2019

    • Author(s)
      友田悠太,中村孝,藤村奈央,吉中奎貴,小熊博幸, 竹内晃久,上椙真之,上杉健太朗
    • Organizer
      日本材料学会第68期学術講演会
    • Related Report
      2019 Annual Research Report
  • [Presentation] 大気および真空環境における微小疲労き裂の進展・停留挙動2019

    • Author(s)
      塚越拓摩,石原梨沙, Paras Mehendiratta,中村孝,藤村奈央,高橋航圭
    • Organizer
      日本材料学会第68期学術講演会
    • Related Report
      2019 Annual Research Report
  • [Presentation] 真空環境下におけるき裂進展速度に基づく内部き裂の疲労寿命推定2019

    • Author(s)
      ソラブ クマール モディ,メヘンディラッタパラス,塚越 拓摩, 中村 孝,藤村 奈央,髙橋 航圭
    • Organizer
      日本機械学会M&M2019 材料力学カンファレンス
    • Related Report
      2019 Annual Research Report
  • [Presentation] 放射光顕微CT による高強度金属内部の高分解能非破壊観察2019

    • Author(s)
      今 佑宇真,中村 孝,藤村 奈央,吉中 奎貴,髙橋 航圭,竹内 晃久,上椙 真之,上杉 健太朗
    • Organizer
      日本機械学会M&M2019 材料力学カンファレンス
    • Related Report
      2019 Annual Research Report
  • [Presentation] 破面解析に基づくTi-22V-4Al 合金における内部疲労き裂の発生・進展過程2019

    • Author(s)
      薛 高格,藤村 奈央,中村 孝,小熊 博幸,髙橋 航圭
    • Organizer
      日本機械学会M&M2019 材料力学カンファレンス
    • Related Report
      2019 Annual Research Report
  • [Presentation] 放射光顕微CT によるTi-6Al-4V の内部疲労き裂発生過程2019

    • Author(s)
      中村 孝, 友田 悠太, 藤村 奈央, 吉中 奎貴, 小熊 博幸, 竹内 晃久, 上椙 真之,上杉 健太朗
    • Organizer
      日本機械学会M&M2019 材料力学カンファレンス
    • Related Report
      2019 Annual Research Report
  • [Presentation] 高強度鋼に対する10^11回ギガサイクル疲労試験2019

    • Author(s)
      古谷佳之
    • Organizer
      日本鉄鋼協会秋季講演大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] 高強度鋼の超高サイクル疲労における疲労限2019

    • Author(s)
      古谷佳之
    • Organizer
      日本機械学会M&M材料力学カンファレンス
    • Related Report
      2019 Annual Research Report
  • [Presentation] チタン合金の内部起点型疲労破壊における特異な破面領域形成に及ぼす影響因子2019

    • Author(s)
      小熊博幸
    • Organizer
      日本材料学会第68期学術講演会
    • Related Report
      2019 Annual Research Report
  • [Presentation] Effects of vacuum-like environment on small internal crack growth processes in very high cycle fatigue2018

    • Author(s)
      Takashi Nakamura, Fumiyoshi Yoshinaka
    • Organizer
      2nd International Conference on Structural Integrity and Exhibition 2018
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Initiation and propagation processes of internal fatigue cracks in Ti-6Al-4V visualized by synchrotron radiation μCT imaging2018

    • Author(s)
      Takashi Nakamura, Fumiyoshi Yoshinaka, Akihisa Takeuchi, Kentaro Uesugi, Masayuki Uesugi
    • Organizer
      12th International Fatigue Congress, FATIGUE 2018
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Nondestructive Multiscale X-Ray Tomography by Combining Microtomography and High-Energy Phase-Contrast Nanotomography2018

    • Author(s)
      Akihisa Takeuchi
    • Organizer
      International Conference on X-Ray Microscopy (XRM2018)
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Effects of vacuum environment on the fatigue crack growth properties of high strength steel - behavior of long crack by ΔK decreasing test -2018

    • Author(s)
      Paras Mehendiratta
    • Organizer
      日本機械学会M&M2018材料力学カンファレンス
    • Related Report
      2018 Annual Research Report
  • [Presentation] 高強度鋼の疲労き裂進展特性に及ぼす真空環境の影響ーΔK漸増試験による微小き裂の挙動ー2018

    • Author(s)
      石原梨沙
    • Organizer
      日本機械学会M&M2018材料力学カンファレンス
    • Related Report
      2018 Annual Research Report

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Published: 2018-04-23   Modified: 2023-01-30  

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