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Development of WC-alloy for precision cutting tool by in-situ formation of fine WC and heat resistant binder

Research Project

Project/Area Number 19560726
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Material processing/treatments
Research InstitutionShiga University

Principal Investigator

ISONISHI Kazuo  Shiga University, 教育学部, 教授 (50223061)

Project Period (FY) 2007 – 2009
Project Status Completed (Fiscal Year 2009)
Budget Amount *help
¥5,070,000 (Direct Cost: ¥3,900,000、Indirect Cost: ¥1,170,000)
Fiscal Year 2009: ¥390,000 (Direct Cost: ¥300,000、Indirect Cost: ¥90,000)
Fiscal Year 2008: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2007: ¥4,030,000 (Direct Cost: ¥3,100,000、Indirect Cost: ¥930,000)
Keywords超硬 / メカニカルアロイング / その場生成 / 真空ホットプレス / 硬さ試験 / 曲げ試験 / 高温曲げ試験 / 破壊じん性 / 材料加工・処理 / 超微細WC / 超硬合金 / 固相焼結 / WC / FeAl / 曲げ強さ / 高温強度 / メカニカルアロイグ
Research Abstract

In this study, the formation WC-alloy fabricated by mechanical alloying and vacuum hot pressing from elemental powders was investigated. WC and binder phase were synthesized during consolidation process. First of all, conventional Co binder was discussed, and then the ability of FeAl or Fe_3AlC binder was discussed to order to increase the high temperature properties. In the case of WC-Co alloy, compact showed higher mechanical properties (hardness and bending strength at room and high temperature) compared to the commercial alloy due to the fine dispersed WC particle. The amounts of elemental powders for MA were determined from the fraction of WC and binder having stoichiometric chemical composition. On the other hand, Fe_3W_3C and α-Fe were formed during consolidation at 1100℃. It seems to be the lack of Al content. The hardness, fracture toughness and bending strength up to 1000℃ have strong correlation to the type of binder phase. After the further discussion, FeAl was synthesized as a binder phase by increasing Al content, and the further prospect was suggested.

Report

(4 results)
  • 2009 Annual Research Report   Final Research Report ( PDF )
  • 2008 Annual Research Report
  • 2007 Annual Research Report

Research Products

(23 results)

All 2010 2009 2008 2007 Other

All Journal Article (7 results) (of which Peer Reviewed: 7 results) Presentation (15 results) Remarks (1 results)

  • [Journal Article] Manufacturing of WC Alloys by Consolidation of MA powders Made from W-C-Co or W-C-Fe-Al Powder Mixtures2010

    • Author(s)
      K. Isonishi
    • Journal Title

      Steel Research Intewrnational (in press)

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] Manufacturing of WC Alloys by Consolidation of MA Powders Made from W-C-Co or W-C-Fe-Al Powder Mixture2010

    • Author(s)
      K.Isonishi
    • Journal Title

      Steel Research International (in press)

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Synthesis of WC Phase from Elemental Powders by Mechanical Alloying and SPS2009

    • Author(s)
      K. Isonishi
    • Journal Title

      J. Solid Mechanics and Solid Materials Enginnering. 3

      Pages: 178-188

    • Related Report
      2009 Final Research Report 2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] SYNTHESIS AND CHARACTERISTICS OF WC-Co ALLOY FABRICATED BY MECHANICAL ALLOYING AND PRESSURE SINTERING2008

    • Author(s)
      K. Isonishi
    • Journal Title

      Proceedings of 3rd JSME/ASM International Conference on Materials and Processing (CD-RON)

      Pages: 6-6

    • NAID

      130000667651

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] Effect of the Second Phase on Mechanical Properties of Fe3AlC Alloy Prepared by Mechanical Alloying2008

    • Author(s)
      K. Isonishi
    • Journal Title

      Advances in Powder Metallurgy & Paticulatte Materials 9

      Pages: 104-114

    • Related Report
      2009 Final Research Report
    • Peer Reviewed
  • [Journal Article] Effect of the Second Phase on Mechani cal Properties of Fe3AlC Alloy Prepared by Mechanical Alloying2008

    • Author(s)
      K. Isonishi
    • Journal Title

      Advances in Powder Metallurgy & Paticulatte Materials. (CR-ROM)

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Synthesis of WC Phase from Elemental Powders by Mechanical Alloying and SPS2008

    • Author(s)
      K. Isonishi
    • Journal Title

      Proceedings of 3rd JSME/ASM Tnternational Conference on Materisals and Processing, (2008) (CD-RON)

      Pages: 6-6

    • Related Report
      2008 Annual Research Report
    • Peer Reviewed
  • [Presentation] その場生成により作製したWC超硬合金の特性と結合相との関係2009

    • Author(s)
      磯西和夫
    • Organizer
      日本機械学会2009年度年次大会
    • Place of Presentation
      弘前大学
    • Year and Date
      2009-09-14
    • Related Report
      2009 Annual Research Report 2009 Final Research Report
  • [Presentation] Synthesis of WC Phase from Elemental Powders by Mechanical Alloying and SPS2009

    • Author(s)
      K. Isonishi
    • Organizer
      2nd German- Japanese Symposium on Nanostructures
    • Place of Presentation
      Ristumeikan University
    • Related Report
      2009 Final Research Report
  • [Presentation] Synthesi s of we Phase from Elemental Powders by Mechanical Alloying and SPS2009

    • Author(s)
      K. Isonishi
    • Organizer
      2nd German-Japanese Symposium on Nanostructures
    • Place of Presentation
      立命館大学
    • Related Report
      2008 Annual Research Report
  • [Presentation] 固相反応によるWC超硬合金の合成2008

    • Author(s)
      磯西和夫
    • Organizer
      日本機械学会2008年度年次大会
    • Place of Presentation
      横浜国立大学
    • Year and Date
      2008-08-04
    • Related Report
      2008 Annual Research Report
  • [Presentation] W, C, Co素粉末を用いた超硬合金の作製2008

    • Author(s)
      磯西和夫
    • Organizer
      粉体粉末冶金協会平成20年度春季大会
    • Place of Presentation
      早稲田大学
    • Year and Date
      2008-05-28
    • Related Report
      2008 Annual Research Report
  • [Presentation] MA法で作製したFe_3AlC合金の組織と機械的性質2008

    • Author(s)
      磯西和夫
    • Organizer
      日本塑性加工学会春季講演会
    • Place of Presentation
      日本大学生産工学部
    • Year and Date
      2008-05-24
    • Related Report
      2008 Annual Research Report
  • [Presentation] SYNTHESIS AND CHARACTERISTICS OF WC-Co ALLOY FABRICATED BY MECHANICAL ALLOYING AND PRESSURE SINTERING2008

    • Author(s)
      K. Isonishi
    • Organizer
      ICM&P2008, (2008), 3rd JSME/ASME International Conference on Materials and Processing
    • Place of Presentation
      North Western University
    • Related Report
      2009 Final Research Report
  • [Presentation] 固相反応によるWC超硬合金の合成2008

    • Author(s)
      磯西和夫
    • Organizer
      日本機械学会2008年度年次大会講演論文集
    • Place of Presentation
      横浜国立大学
    • Related Report
      2009 Final Research Report
  • [Presentation] Effect of the Second Phase on Mechanical Properties of Fe3AlC Alloy Prepared by Mechanical Alloying2008

    • Author(s)
      K. Isonishi
    • Organizer
      2008 World Congress on Powder Metallurgy & Particulate Materials
    • Place of Presentation
      Washington D. C
    • Related Report
      2009 Final Research Report
  • [Presentation] W, C, Co素粉末を用いた超硬合金の作製2008

    • Author(s)
      磯西和夫
    • Organizer
      粉体粉末冶金協会平成20年度春季大会講演概要集
    • Place of Presentation
      早稲田大学国際会議場
    • Related Report
      2009 Final Research Report
  • [Presentation] MA法で作製したFe3AlC合金の組織と機械的性質2008

    • Author(s)
      磯西和夫
    • Organizer
      日本塑性加工学会春季講演会講演論文集
    • Place of Presentation
      日本大学
    • Related Report
      2009 Final Research Report
  • [Presentation] Effect of the Second Phase on Mechani cal Properties of Fe_3AlC Alloy Prepared by Mechanical Alloying2008

    • Author(s)
      K. Isonishi
    • Organizer
      PM2008(2008 World Congress on Powder Metallurgy & Particulate Materials)
    • Place of Presentation
      米国・ワシントンDC Gay lord National Resort & Convention Center
    • Related Report
      2008 Annual Research Report
  • [Presentation] SYNTHESIS AND CHARACTERISTICS OF WC-Co ALLOY FABRICATED BY MECHANICAL ALLOYING AND PRESSURE SINTERING2008

    • Author(s)
      K. Isonishi
    • Organizer
      3rd JSME/ASME ICM&P (International Conference on Materials and Processing)2008
    • Place of Presentation
      米国シカゴNorthwes tern University
    • Related Report
      2008 Annual Research Report
  • [Presentation] 粉末冶金で作製したFe-Al-C系Perovskite型合金の機械的性質s2007

    • Author(s)
      磯西 和夫
    • Organizer
      日本鉄鋼協会
    • Place of Presentation
      岐阜大学
    • Year and Date
      2007-09-20
    • Related Report
      2007 Annual Research Report
  • [Presentation] 微細結晶を有するFe3AlC合金の特性2007

    • Author(s)
      磯西 和夫
    • Organizer
      日本機械学会
    • Place of Presentation
      関西大学
    • Year and Date
      2007-09-12
    • Related Report
      2007 Annual Research Report
  • [Remarks] 2009年度の研究を元に、2つの国際会議にて発表予定。2010 Metall Forming では投稿論文が査読の上、受理された。PM2010は abstract をもって発表申し込みし、accept された。

    • Related Report
      2009 Annual Research Report

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Published: 2007-03-31   Modified: 2016-04-21  

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