Development of high-speed and high-efficiency monolithic silica capillary columns for high-performance liquid chromatography
| Project/Area Number |
20350036
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| Research Category |
Grant-in-Aid for Scientific Research (B)
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| Allocation Type | Single-year Grants |
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| Section | 一般 |
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| Research Field |
Analytical chemistry
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| Research Institution | Kyoto Institute of Technology |
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Principal Investigator |
TANAKA Nobuo Kyoto Institute of Technology, 法人本部, 学長特任補佐 (60127165)
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| Co-Investigator(Kenkyū-buntansha) |
IKEGAMI Tohru 京都工芸繊維大学, 工芸科学研究科, 准教授 (20301252)
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| Project Period (FY) |
2008 – 2010
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| Project Status |
Completed (Fiscal Year 2010)
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| Budget Amount *help |
¥13,390,000 (Direct Cost: ¥10,300,000、Indirect Cost: ¥3,090,000)
Fiscal Year 2010: ¥3,510,000 (Direct Cost: ¥2,700,000、Indirect Cost: ¥810,000)
Fiscal Year 2009: ¥3,120,000 (Direct Cost: ¥2,400,000、Indirect Cost: ¥720,000)
Fiscal Year 2008: ¥6,760,000 (Direct Cost: ¥5,200,000、Indirect Cost: ¥1,560,000)
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| Keywords | HPLC / モノリスカラム / シリカ / キャピラリー / 高性能化 / 理論段数 / ピークキャパシティ / ナノHPLC / モノリス / プロテオーム解析 / 透過率 / プロテオーム / HILIC / 化学修飾 / キャピラリーカラム / 100万段 |
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| Research Abstract |
Optimization of preparation conditions of monolithic silica capillary columns attained 10000 and 1000000 theoretical plates with a column dead time of 10s and 5000s, respectively, providing ultrahigh resolution of closely related substances.
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Report
(4 results)
Research Products
(74 results)
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[Journal Article] High-efficiency liquid chromatographic separation utilizing long monolithic silica capillary columns.2008
Author(s)
K.Miyamoto, T.Hara, H.Kobayashi, H.Morisaka, D.Tokuda, K.Horie, K.Koduki, S.Makino, O.Nunez, C.Yang, T.Kawabe, T.Ikegami, H.Takubo, Y.Ishihama, N.Tanaka, Anal.Chem.
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Journal Title
Related Report
Peer Reviewed
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