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Development of automated dynamic headspace extraction method for determination of halomethanes and application to bacterial culture samples

Research Project

Project/Area Number 20510013
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Environmental dynamic analysis
Research InstitutionUniversity of Shizuoka

Principal Investigator

HASHIMOTO Shinya  University of Shizuoka, 文理学部, 教授 (10228413)

Co-Investigator(Kenkyū-buntansha) TANI Yukinori  静岡県立大学, 環境科学研究所, 准教授 (10285190)
Project Period (FY) 2008 – 2010
Project Status Completed (Fiscal Year 2010)
Budget Amount *help
¥4,810,000 (Direct Cost: ¥3,700,000、Indirect Cost: ¥1,110,000)
Fiscal Year 2010: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2009: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2008: ¥3,510,000 (Direct Cost: ¥2,700,000、Indirect Cost: ¥810,000)
Keywordsハロカーボン / 微生物 / 色素分析 / 共存系 / 動態解析 / ダイナミックヘッドスペース法 / ガスクロマトグラフ質量分析装置 / バクテリア / イソプレン / 植物プランクトン / 共存 / 微量ガス / GC-MS / 共存培養
Research Abstract

Halomethane produced in the marine environment are thought to play a key role in atmospheric reactions, particularly those involved in the global radiation budget and the depression of tropospheric and stratospheric ozone. To evaluate halomethane concentrations in the bacterial culture samples, we developed an automated dynamic headspace extraction method for the determination of 15 halomethanes. The halomethanes in the gas phase above the culture samples were measured using dynamic headspace (GESTEL DHS)-gas chromatograph (Agilent 6890N)- mass spectrometer (Agilent 5975C). Productions of halomethane were observed for several days.

Report

(4 results)
  • 2010 Annual Research Report   Final Research Report ( PDF )
  • 2009 Annual Research Report
  • 2008 Annual Research Report
  • Research Products

    (13 results)

All 2010 2009

All Journal Article (5 results) (of which Peer Reviewed: 5 results) Presentation (8 results)

  • [Journal Article] Distributions of short-lived iodocarbons and biogenic trace gases in the open ocean and atmosphere in the western North Pacific.2010

    • Author(s)
      M.K.Kurihara, M.Kimura, Y.Iwamoto, Y.Narita, A.Ooki, Y.-J.Eum, A.Tsuda, K.Suzuki, Y.Tani, Y.Yokouchi, M.Uematsu, S.Hashimoto
    • Journal Title

      Marine Chemistry 118

      Pages: 156-170

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Distributions of short-lived iodocarbons and biogenic trace gases in the open ocean and atmosphere in the western North Pacific2010

    • Author(s)
      M.K.Kurihara, et al.
    • Journal Title

      Marine Chemistry 118

      Pages: 156-170

    • Related Report
      2009 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Responses of DMS in the seawater and atmosphere to iron enrichment in the subarctic western North Pacific (SEEDS-II).2009

    • Author(s)
      Ippei Nagao, Shinya Hashimoto, Koji Suzuki, Shuji Toda, Yasushi Narita, Atsushi Tsuda, Hiroaki Saito, Isao Kudo, Shungo Kato, Yoshizumi Kajii, Mitsuo Uematsu
    • Journal Title

      Deep-Sea Research part II 56

      Pages: 2899-2917

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Production and air-sea flux of methyl halides in the western subarctic Pacific in relation to phytoplankton pigment concentrations during iron fertilization experiment (SEEDS II).2009

    • Author(s)
      Shinya Hashimoto, Shuji Toda, Koji Suzuki, Shungo Kato, Yasusi Narita, Michiko K. Kurihara, Yoko Akatsuka, Hiroshi Oda, Takahiro Nagai, Ippei Nagao, Isao Kudo, Mitsuo Uematsu
    • Journal Title

      Deep-Sea Research part II 56

      Pages: 2928-2935

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Journal Article] Photosynthetic pigments in sediment core HDP-04 from Lake Hovsgol, Mongolia, and their implication in algal productivity and lake environment for the last 1 Ma.2009

    • Author(s)
      Yukinori Tani, Genki I. Matsumoto, Mitsuyuki Soma, Yuko Soma, Shinya Hashimoto, Takayoshi Kawai
    • Journal Title

      Quaternary International 205

      Pages: 74-83

    • Related Report
      2010 Final Research Report
    • Peer Reviewed
  • [Presentation] Optimization of dynamic headspace extraction system for measurement of halogenated volatile organic compounds in liquid or viscous samples.2010

    • Author(s)
      G.Taniai, H.Oda, M.Kurihara, S.Hashimoto
    • Organizer
      American Geophysical Union, Fall Meeting 2010
    • Place of Presentation
      米国サンフランシスコ
    • Year and Date
      2010-12-15
    • Related Report
      2010 Final Research Report
  • [Presentation] Production of volatile organic compounds in cultures of cryptophytes2010

    • Author(s)
      T.Yamakoshi, M.Kurihara, S.Hashimoto
    • Organizer
      American Geophysical Union, Fall Meeting 2010
    • Place of Presentation
      米国サンフランシスコ
    • Year and Date
      2010-12-15
    • Related Report
      2010 Annual Research Report 2010 Final Research Report
  • [Presentation] Production of halomethanes and isoprene in the culture of bacteria isolated from brackish water.2010

    • Author(s)
      T.Fujimori, G.Taniai, M.Kurihara, H.Tamegai, S.Hashimoto
    • Organizer
      American Geophysical Union, Fall Meeting 2010
    • Place of Presentation
      米国サンフランシスコ
    • Year and Date
      2010-12-13
    • Related Report
      2010 Final Research Report
  • [Presentation] Production of halomethanes and isoprene in the culture of bacteria isolated from brackish water2010

    • Author(s)
      T.Fujimori, G.Taniai, M.Kurihara, H.Tamegai, S.Hashimoto
    • Organizer
      American Geophysical Union, Fall Meeting 2010
    • Place of Presentation
      米国サンフランシスコ
    • Year and Date
      2010-12-13
    • Related Report
      2010 Annual Research Report
  • [Presentation] Optimization of dynamic headspace extraction system for measurement of halogenated volatile organic compounds in liquid or viscous samples2010

    • Author(s)
      G.Taniai, H.Oda, M.Kurihara, S.Hashimoto
    • Organizer
      American Geophysical Union, Fall Meeting 2010
    • Place of Presentation
      米国サンフランシスコ
    • Year and Date
      2010-12-13
    • Related Report
      2010 Annual Research Report
  • [Presentation] DHS-GC/MS分析法によるCH3Brを含むハロカーボンの測定2010

    • Author(s)
      谷合元, 栗原路子, 橋本伸哉
    • Organizer
      日本海洋学会春季大会
    • Place of Presentation
      東京海洋大学、東京
    • Year and Date
      2010-03-27
    • Related Report
      2010 Final Research Report
  • [Presentation] DHS-GC/MS分析法によるCH_3Brを含むハロカーボンの測定2010

    • Author(s)
      谷合元, ら
    • Organizer
      日本海洋学会
    • Place of Presentation
      東京海洋大学(東京都)
    • Year and Date
      2010-03-27
    • Related Report
      2009 Annual Research Report
  • [Presentation] DHS(ダイナミックヘッドスペース)-GC/MS分析法による揮発性有機ハロゲン化合物(VHOCs)の測定2009

    • Author(s)
      小田祐史, 和久田千晴, 栗原路子, 橋本伸哉
    • Organizer
      日本海洋学会春季大会
    • Place of Presentation
      東京大学、東京
    • Year and Date
      2009-04-06
    • Related Report
      2010 Final Research Report

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Published: 2008-04-01   Modified: 2016-04-21  

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