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Nanometer cale surface charge mapping in liquids

Research Project

Project/Area Number 22686007
Research Category

Grant-in-Aid for Young Scientists (A)

Allocation TypeSingle-year Grants
Research Field Thin film/Surface and interfacial physical properties
Research InstitutionKyoto University

Principal Investigator

KOBAYASHI Kei  京都大学, 産官学連携本部, 助教 (40335211)

Project Period (FY) 2010 – 2012
Project Status Completed (Fiscal Year 2012)
Budget Amount *help
¥24,830,000 (Direct Cost: ¥19,100,000、Indirect Cost: ¥5,730,000)
Fiscal Year 2012: ¥5,070,000 (Direct Cost: ¥3,900,000、Indirect Cost: ¥1,170,000)
Fiscal Year 2011: ¥8,190,000 (Direct Cost: ¥6,300,000、Indirect Cost: ¥1,890,000)
Fiscal Year 2010: ¥11,570,000 (Direct Cost: ¥8,900,000、Indirect Cost: ¥2,670,000)
Keywords走査プローブ顕微鏡 / 原子間力顕微鏡 / カンチレバー / 溶液環境
Research Abstract

A surface charge mapping technique based on frequency modulation atomic force microscopy (FM-AFM) working in liquid environments has been developed. We implemented a phototheimal excitation setup for cantilever oscillation in liquids to perform quantitative force measurements. We analyzed the cantilever oscillation caused by an external modulation voltage between the tip and sample surface, and found that the conventional voltage modulation schemes for surface potential measurement cannot be applied in polar liquids. We also developed a method to estimate surface charge density by comparing measured electrostatic force with theoretically calculated force.

Report

(4 results)
  • 2012 Annual Research Report   Final Research Report ( PDF )
  • 2011 Annual Research Report
  • 2010 Annual Research Report
  • Research Products

    (46 results)

All 2013 2012 2011 2010 Other

All Journal Article (16 results) (of which Peer Reviewed: 16 results) Presentation (23 results) Patent(Industrial Property Rights) (7 results)

  • [Journal Article] Analysis of capacitive force acting on a cantilever tip at solid/liquid interfaces2013

    • Author(s)
      K.-I. Umeda, K. Kobavashi, N. Oyabu, Y. Hirata, K. Matsushige and H. Yamada
    • Journal Title

      J. Appl. Phys

      Volume: 113 Issue: 15 Pages: 154311-154311

    • DOI

      10.1063/1.4801795

    • Related Report
      2012 Annual Research Report 2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Monotonic damping in nanoscopic hydration experiments2013

    • Author(s)
      A. Labuda, K. Kobayashi, K. Suzuki, H. Yamada and P. Grittier
    • Journal Title

      Phys. Rev. Lett

      Volume: 110 Issue: 5 Pages: 53703-53703

    • DOI

      10.1063/1.4712286

    • NAID

      120005439729

    • Related Report
      2012 Annual Research Report 2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Direct actuation of cantilever in aqueous solutions by electrostatic force using high-frequency electric fields2012

    • Author(s)
      K. Umeda, K. Kobayashi, K. Matsushige, H. Yamada
    • Journal Title

      Applied Physics Letters

      Volume: 101 Issue: 12 Pages: 123112-123112

    • DOI

      10.1063/1.4754289

    • Related Report
      2012 Annual Research Report 2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Atomic-Resolution Imaging of Graphite-Water Interface by Frequency Modulation Atomic Force Microscopy2011

    • Author(s)
      K.Suzuki, N.Oyabu, K.Kobayashi, K.Matsushige, H.Yamada
    • Journal Title

      Applied Physics Express

      Volume: 4 Issue: 12 Pages: 125102-125102

    • DOI

      10.1143/apex.4.125102

    • NAID

      10030154221

    • Related Report
      2012 Final Research Report 2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Modification of a commercial atomic force microscopy for low-noise, high-resolution frequency-modulation imaging in liquid environment2011

    • Author(s)
      S.Rode, R.Stark, J.Lubbe, L.Troger, J.Schutte, K.Umeda, K.Kobayashi, H.Yamada, A.Kuhnle
    • Journal Title

      Rev.Sci.Instrum.

      Volume: 82 Issue: 7 Pages: 73703-73703

    • DOI

      10.1063/1.3606399

    • Related Report
      2012 Final Research Report 2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Comparison of photothermal and piezoacoustic excitation methods for frequency and phase modulation atomic force microscopy in liquid environments2011

    • Author(s)
      A.Labuda, K.Kobayashi, D.Kiracofe, K.Suzuki, P.H.Grutter, H.Yamada
    • Journal Title

      AIP Advances

      Volume: 1 Issue: 2 Pages: 22136-22136

    • DOI

      10.1063/1.3601872

    • Related Report
      2012 Final Research Report 2011 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Reduction of frequency noise and frequency shift by phase shifting elements in frequency modulation atomic force microscopy2011

    • Author(s)
      K. Kobavashi, H. Yamada and K. Matsushige
    • Journal Title

      Rev. Sci. Instrum

      Volume: 82 Issue: 3

    • DOI

      10.1063/1.3557416

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] High efficiency laser photothermal excitation of microcantilever vibrations in air and liquids2011

    • Author(s)
      D. Kiracofe, K. Kobayashi, A. Labuda, A. Raman and H. Yamada
    • Journal Title

      Rev. Sci. Instrum

      Volume: 82 Issue: 1

    • DOI

      10.1063/1.3518965

    • NAID

      120004920381

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] High efficiency laser photothermal excitation of Microcantilever vibrations in air and liquids2011

    • Author(s)
      Daniel Kiracofe, Kei Kobayashi, Aleksander Labuda, Arvind Raman, Hirofumi Yamada
    • Journal Title

      Review of Scientific Instruments

      Volume: 82

    • NAID

      120004920381

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Reduction of frequency noise and frequency shift by phase shifting elements in frequency modulation atomic force microscopy2011

    • Author(s)
      Kei Kobayashi, Hirofumi Yamada, Kazumi Matsushige
    • Journal Title

      Review of Scientific Instruments

      Volume: 82

    • NAID

      120003039149

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Aqueous Solution Structure over a-Al203(01-12) Probed by Frequency-Modulation Atomic Force Microscopy2010

    • Author(s)
      T. Hiasa, K. Kimura, H. Onishi, M. Ohta, K. Watanabe, R. Kokawa, N. Oyabu, K. Kobavashi and H. Yamada
    • Journal Title

      J. Phys.Chem

      Volume: 114

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] Development of High-Resolution Imaging of Solid-Liquid Interface by Frequency Modulation Atomic Force Microscopy2010

    • Author(s)
      K. Suzuki, S. Kitamura, S. Tanaka, K. Kobayashi and H. Yamada
    • Journal Title

      Jpn. J. Appl. Phys

      Volume: 49

    • NAID

      210000069135

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] High-Resolution Frequency-Modulation Atomic Force Microscopy in Liquids Using Electrostatic Excitation Method2010

    • Author(s)
      K.-I. Umeda, N. Oyabu, K. Kobayashi Y. Hirata, K. Matsushige and H. Yamada
    • Journal Title

      Appl. Phys.

      Volume: 3 Issue: 6 Pages: 065205-065205

    • DOI

      10.1143/apex.3.065205

    • NAID

      10027015527

    • Related Report
      2012 Final Research Report
    • Peer Reviewed
  • [Journal Article] High-Resolution Frequency-Modulation Atomic Force Microscopy in Liquids Using Electrostatic Excitation Method2010

    • Author(s)
      Ken-ichi Umeda, Noriaki Oyabu, Kei Kobayashi, Yoshiki Hirata, Kazumi Matsushige, Hirofumi Yamada
    • Journal Title

      Applied Physics Express

      Volume: 3

    • NAID

      10027015527

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Development of High-Resolution Imaging of Solid-Liquid Interface by Frequency Modulation Atomic Force Microscopy2010

    • Author(s)
      Katsuyuki Suzuki, Shin-ichi Kitamura, Shukichi Tanaka, Kei Kobayashi, Hirofumi Yamada
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 49

    • NAID

      210000069135

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Aqueous Solution Structure over α-Al2O3(01-12) Probed by Frequency-Modulation Atomic Force Microscopy2010

    • Author(s)
      Takumi Hiasa, Kenjiro Kimura, Hiroshi Onishi, Masahiro Ohta, Kazuyuki Watanabe, Ryohei Kokawa, Noriaki Oyabu, Kei Kobayashi, Hirofumi Yamada
    • Journal Title

      Journal of Physical Chemistry C

      Volume: 114 Pages: 21423-21426

    • Related Report
      2010 Annual Research Report
    • Peer Reviewed
  • [Presentation] Quantitative charge density measurement of biomolecule in aqueous solutions by FM-AFM with force mapping technique2012

    • Author(s)
      K.-I. Umeda, Y. Hirata, N. Oyabu, K. Kobayashi and H. Yamada
    • Organizer
      20th International Colloquium on Scarming Probe Microscopy
    • Place of Presentation
      那覇
    • Year and Date
      2012-12-18
    • Related Report
      2012 Final Research Report
  • [Presentation] Molecular-Scale Investigations of Self-Assembled Surfactant Aggregates on Graphite by Force Mapping Using FM-AFM2012

    • Author(s)
      K. Suzuki, K. Kobayashi, K. Matsushige and H. Yamada
    • Organizer
      20th International Colloquium on Scarming Probe Microscopy
    • Place of Presentation
      ggg
    • Year and Date
      2012-12-17
    • Related Report
      2012 Final Research Report
  • [Presentation] Quantitative study of local electric double layer force by FM-AFM in aqueous solutions2012

    • Author(s)
      Ken-ichi Umeda, Yoshiki Hirata, Noriaki Oyabu, Kei Kobayashi, Kazumi Matsushige, Hirfumi Yamada
    • Organizer
      14th International Conference on non-contact Atomic Force Microscopy
    • Place of Presentation
      Lindau, Germany
    • Year and Date
      2012-09-17
    • Related Report
      2011 Annual Research Report
  • [Presentation] FM-AFMによる界面活性剤分子集合体上の電気二重層力の評価2012

    • Author(s)
      鈴木一博,大藪範昭,止埜圭,松重和美,山田啓文
    • Organizer
      第73回応用物理学会学術講演会
    • Place of Presentation
      愛媛大学・松山大学
    • Year and Date
      2012-09-12
    • Related Report
      2012 Final Research Report
  • [Presentation] 液中動作周波数変調AFMにおけるエネルギー散逸一定モードを用いた電荷密度計測2012

    • Author(s)
      梅田健一,平田芳樹,大藪範昭,小林圭,山田啓文
    • Organizer
      第73回応用物理学会学術講演会
    • Place of Presentation
      愛媛大学・松山大学
    • Year and Date
      2012-09-12
    • Related Report
      2012 Final Research Report
  • [Presentation] FM-AFMによる界面活性剤分子集合体上の電気二重層可視化および界面電荷分布の評価2012

    • Author(s)
      鈴木一博,大藪範昭,小林圭,松重和美,山田啓文
    • Organizer
      第59回応用物理学関係連合講演会
    • Place of Presentation
      早稲田大学
    • Year and Date
      2012-03-17
    • Related Report
      2012 Final Research Report 2011 Annual Research Report
  • [Presentation] 3次元フォースマッピング法によるカチオン性界面活性剤分子集合体上の電気二重層力評価2012

    • Author(s)
      伊藤史晃,鈴木一博,大藪範昭,小林圭,松重和美,山田啓文
    • Organizer
      第59回応用物理学関係連合講演会
    • Place of Presentation
      早稲田大学
    • Year and Date
      2012-03-17
    • Related Report
      2012 Final Research Report 2011 Annual Research Report
  • [Presentation] 液中動作周波数変調AFMにおけるエネルギー散逸像コントラストの起源の解明2012

    • Author(s)
      梅田健一,平田芳樹,大藪範昭,小林圭,松重和美,山田啓文
    • Organizer
      第59回応用物理学関係連合講演会
    • Place of Presentation
      早稲田大学
    • Year and Date
      2012-03-17
    • Related Report
      2012 Final Research Report 2011 Annual Research Report
  • [Presentation] Quantitative study of local electric double layer force by FM-AFM in aqueous solutions2011

    • Author(s)
      K.-I. Umeda, Y. Hirata, N. Oyabu, K. Kobayashi, K. Matsushige and H. Yamada
    • Organizer
      14th International Conference on non-contact Atomic Force Microscopy
    • Place of Presentation
      Lindau, Germany
    • Year and Date
      2011-09-17
    • Related Report
      2012 Final Research Report
  • [Presentation] FM-AFMを用いた局所電荷分布計測技術の開発に向けたコロイダルプローブによる電気二重層力検出2011

    • Author(s)
      梅田健一,平田芳樹,大藪範昭,止埜圭,松重和美,山田啓文
    • Organizer
      イダルプローブによる電気二重層力検出",第72回応用物理学会学術講演会
    • Place of Presentation
      山形大学
    • Year and Date
      2011-09-01
    • Related Report
      2012 Final Research Report
  • [Presentation] FM-AFMを用いた局所電荷分布計測技術の開発に向けたコロイダルプローブによる電気二重層力検出2011

    • Author(s)
      梅田健一, 平田芳樹, 大藪範昭, 小林圭, 松重和美, 山田啓文
    • Organizer
      第72回応用物理学会学術講演会
    • Place of Presentation
      山形大学
    • Year and Date
      2011-09-01
    • Related Report
      2011 Annual Research Report
  • [Presentation] High Efficiency Laser Photothennal Excitation of Microcantilever Vibrations in Air and Liquids2010

    • Author(s)
      D. Kiracofe, K. Kobayashi A. Labuda, A. Raman and H. Yamada
    • Organizer
      18th International Colloquium on Scanning Probe Microscopy
    • Place of Presentation
      熱川ハイツ
    • Year and Date
      2010-12-09
    • Related Report
      2012 Final Research Report
  • [Presentation] High Efficiency Laser Photothermal Excitation of Microcantilever Vibrations in Air and Liquids2010

    • Author(s)
      Daniel Kiracofe, Kei Kobayashi, Aleksander Labuda, Arvind Raman, Hirofumi Yamada
    • Organizer
      18th International Colloquium on Scanning Probe Microscopy (ICSPM18)
    • Place of Presentation
      熱川ハイツ(静岡県賀茂郡東伊豆町)
    • Year and Date
      2010-12-09
    • Related Report
      2010 Annual Research Report
  • [Presentation] Force Spectroscopy Study in Liquids by Frequency Modulation AFM Toward Local Charge Mapping at Solid/liquid Interface2010

    • Author(s)
      K.-I. Umeda, Y. Hirata, N. Oyabu, K. Kobayashi, K. Matsushige and H. Yamada
    • Organizer
      MRS 2010 Fall Meeting
    • Place of Presentation
      Boston, USA
    • Year and Date
      2010-10-29
    • Related Report
      2012 Final Research Report
  • [Presentation] Force Spectroscopy Study in Liquids by Frequency Modulation AFM Toward Local Charge Mapping at Solid/liquid Interface2010

    • Author(s)
      Ken-ichi Umeda, Yoshiki Hirata, Noriaki Oyabu, Kei Kobayashi, Kazumi Matsushige, Hirofumi Yamada
    • Organizer
      MRS 2010 Fall Meeting
    • Place of Presentation
      Sheraton Boston Hotel (Boston, MA, USA)
    • Year and Date
      2010-10-29
    • Related Report
      2010 Annual Research Report
  • [Presentation] 液中FM-AFMにおける圧電励起法および光熱励振法の比較2010

    • Author(s)
      A.Labuda,鈴木一博,⊥埜圭,大藪範昭,P.Grutter,山田啓文
    • Organizer
      第71回応用物理学会学術講演会
    • Place of Presentation
      長崎大学
    • Year and Date
      2010-09-17
    • Related Report
      2012 Final Research Report
  • [Presentation] 液中FM-AFMにおける圧電励起法および光熱励振法の比較2010

    • Author(s)
      Aleksander Labuda, 鈴木一博, 小林圭, 大藪範昭, Peter Grutter, 山田啓文
    • Organizer
      第71回応用物理学会学術講演会
    • Place of Presentation
      長崎大学(長崎県長崎市)
    • Year and Date
      2010-09-17
    • Related Report
      2010 Annual Research Report
  • [Presentation] 固液界面における局所電荷分布計測へ向けた静電気力の探針-試料間距離依存性に関する研究2010

    • Author(s)
      梅田健一,平田芳樹,大藪範昭,止埜圭,松重和美,山田啓文
    • Place of Presentation
      長崎大学
    • Year and Date
      2010-09-16
    • Related Report
      2012 Final Research Report
  • [Presentation] 固液界面における局所電荷分布計測へ向けた静電気力の探針-試料間距離依存性に関する研究2010

    • Author(s)
      梅田健一, 平田芳樹, 大藪範昭, 小林圭, 松重和美, 山田啓文
    • Organizer
      第71回応用物理学会学術講演会
    • Place of Presentation
      長崎大学(長崎県長崎市)
    • Year and Date
      2010-09-16
    • Related Report
      2010 Annual Research Report
  • [Presentation] Molecular-Scale Investigations of Self-Assembled Surfactant Aggregates on Graphite by Force Mapping Using FM-AFM

    • Author(s)
      Kazuhiro Suzuki, Kei Kobayashi, Kazumi Matsushige, and Hirofumi Yamada
    • Organizer
      20th International Colloquium on Scanning Probe Microscopy
    • Place of Presentation
      Naha, Japan
    • Related Report
      2012 Annual Research Report
  • [Presentation] Quantitative charge density measurement of biomolecule in aqueous solutions by FM-AFM with force mapping technique

    • Author(s)
      Ken-ichi Umeda, Yoshiki Hirata, Noriaki Oyabu, Kei Kobayashi, and Hirofumi Yamada
    • Organizer
      20th International Colloquium on Scanning Probe Microscopy
    • Place of Presentation
      Naha, Japan
    • Related Report
      2012 Annual Research Report
  • [Presentation] FM-AFMによる界面活性剤分子集合体上の電気二重層力の評価

    • Author(s)
      鈴木一博, 大藪範昭, 小林圭, 松重和美, 山田啓文
    • Organizer
      第73回応用物理学会学術講演会
    • Place of Presentation
      愛媛大学・松山大学
    • Related Report
      2012 Annual Research Report
  • [Presentation] 液中動作周波数変調AFMにおけるエネルギー散逸一定モードを用いた電荷 密度計測

    • Author(s)
      梅田健一, 平田芳樹, 大藪範昭, 小林圭, 山田啓文
    • Organizer
      第73回応用物理学会学術講演会
    • Place of Presentation
      愛媛大学・松山大学
    • Related Report
      2012 Annual Research Report
  • [Patent(Industrial Property Rights)] 原子間力顕微鏡を用いた表面電荷密度測定装置2013

    • Inventor(s)
      大田昌弘, 梅田健一, 小林圭, 山田啓文
    • Industrial Property Rights Holder
      株式会社島津製作所
    • Industrial Property Rights Type
      特許
    • Filing Date
      2013-02-26
    • Related Report
      2012 Annual Research Report
  • [Patent(Industrial Property Rights)] 原子間力顕微鏡を用いた誘電特性測定方法2011

    • Inventor(s)
      粉川良平,大田昌弘,梅田健一,木林圭,山田啓文,松重和美
    • Industrial Property Rights Holder
      株式会社島津製作所
    • Industrial Property Number
      2011-190981
    • Filing Date
      2011-09-01
    • Related Report
      2012 Final Research Report
  • [Patent(Industrial Property Rights)] 原子間力顕微鏡におけるカンチレバー励振方法及び原子間力顕微鏡2011

    • Inventor(s)
      粉川良平,大田昌弘,梅田健一,木林圭,山田啓文,松重和美
    • Industrial Property Rights Holder
      株式会社島津製作所
    • Industrial Property Number
      2011-190980
    • Filing Date
      2011-09-01
    • Related Report
      2012 Final Research Report
  • [Patent(Industrial Property Rights)] 原子間力顕微鏡におけるカンチレバー励振方法及び原子間力顕微鏡2011

    • Inventor(s)
      粉川良平, 大田昌弘, 梅田健一, 小林圭, 山田啓文, 松重和美
    • Industrial Property Rights Holder
      株式会社島津製作所
    • Industrial Property Number
      2011-190980
    • Filing Date
      2011-09-01
    • Related Report
      2011 Annual Research Report
  • [Patent(Industrial Property Rights)] 原子間力顕微鏡を用いた誘電特性測定方法2011

    • Inventor(s)
      粉川良平, 大田昌弘, 梅田健一, 小林圭, 山田啓文, 松重和美
    • Industrial Property Rights Holder
      株式会社島津製作所
    • Industrial Property Number
      2011-190981
    • Filing Date
      2011-09-01
    • Related Report
      2011 Annual Research Report
  • [Patent(Industrial Property Rights)] 原子間力顕微鏡におけるカンチレバー励振方法及び原子間力顕微鏡2010

    • Inventor(s)
      粉川良平,大田昌弘,梅田健一,大藪範昭,盛圭,山田啓文,松重和美
    • Industrial Property Rights Holder
      株式会社島津製作所
    • Industrial Property Number
      2010-128127
    • Filing Date
      2010-06-03
    • Related Report
      2012 Final Research Report
  • [Patent(Industrial Property Rights)] 原子間力顕微鏡におけるカンチレバー励振方法及び原子間力顕微鏡2010

    • Inventor(s)
      粉川良平, 大田昌弘, 梅田健一, 大藪範昭, 小林圭, 山田啓文, 松重和美
    • Industrial Property Rights Holder
      株式会社島津製作所
    • Industrial Property Number
      2010-128127
    • Filing Date
      2010-06-03
    • Related Report
      2010 Annual Research Report

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Published: 2010-08-23   Modified: 2019-07-29  

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