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Development of an Innovative Technique for Fabricating Functional Ceramic Thin Films on Plastics Surface

Research Project

Project/Area Number 24360277
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypePartial Multi-year Fund
Section一般
Research Field Inorganic materials/Physical properties
Research InstitutionKansai University

Principal Investigator

KOZUKA Hiromitsu  関西大学, 化学生命工学部, 教授 (80178219)

Co-Investigator(Kenkyū-buntansha) UCHIYAMA Hiroaki  関西大学, 化学生命工学部, 准教授 (10551319)
Project Period (FY) 2012-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥17,940,000 (Direct Cost: ¥13,800,000、Indirect Cost: ¥4,140,000)
Fiscal Year 2014: ¥2,600,000 (Direct Cost: ¥2,000,000、Indirect Cost: ¥600,000)
Fiscal Year 2013: ¥2,470,000 (Direct Cost: ¥1,900,000、Indirect Cost: ¥570,000)
Fiscal Year 2012: ¥12,870,000 (Direct Cost: ¥9,900,000、Indirect Cost: ¥2,970,000)
Keywordsセラミック薄膜 / 酸化物薄膜 / 結晶薄膜 / ゾル-ゲル法 / プラスチック / コーティング / フレキシブルデバイス / 成膜技術 / 転写 / プラスチックス / 表面機能化 / 成膜 / ゾル-ゲル法
Outline of Final Research Achievements

We conducted experimental studies on our technique that allows the fabrication of ceramic thin films on plastic substrates. First, even when fired at temperatures higher than 600℃, the ceramic thin films could be transferred to plastic substrates. Second, we noticed that there is an optimized thickness of release layers that enables successful transfer of ceramic thin films onto plastic subsrates. Third, plastic substrates with polar groups were demonstrated to have good adhesion, while those with no polar groups have poor adhesion. However, even such plastic substrates with no polar groups exhibit good adhesion when subjected beforehand by UV/ozone treatment, which oxidizes the substrate surface. Finally the degree of plastic substrate bending that is not accompanied by film cracking was found to decrease with increasing firing temperature.

Report

(4 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Annual Research Report
  • 2012 Annual Research Report
  • Research Products

    (44 results)

All 2015 2014 2013 2012 Other

All Journal Article (7 results) (of which Peer Reviewed: 3 results) Presentation (34 results) (of which Invited: 7 results) Remarks (3 results)

  • [Journal Article] Sol-gel and transfer technique for fabricating dual ceramic thin film patterns on plastics2013

    • Author(s)
      H. Kozuka, T. Fukui, H. Uchiyama
    • Journal Title

      J. Sol-Gel Sci. Techn.

      Volume: 67 Pages: 414-419

    • Related Report
      2013 Annual Research Report
    • Peer Reviewed
  • [Journal Article] ゾル-ゲル法によるプラスチックスへのセラミック薄膜の成膜技術2013

    • Author(s)
      幸塚広光
    • Journal Title

      光学薄膜の最適設計・成膜技術と膜厚・膜質・光学特性の制御

      Volume: なし Pages: 445-453

    • Related Report
      2013 Annual Research Report
  • [Journal Article] Wet processing for the fabrication of ceramic thin films on plastics2013

    • Author(s)
      H. Kozuka
    • Journal Title

      J. Mater. Res.

      Volume: 28 Issue: 5 Pages: 673-688

    • DOI

      10.1557/jmr.2013.13

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Ceramic thin films on plastics: A versatile transfer process for large area as well as patterned coating2012

    • Author(s)
      H. Kozuka, T. Fukui, M. Takahashi, H. Uchiyama, and S. Tsuboi
    • Journal Title

      ACS Appl. Mater. Interfaces

      Volume: 4 Issue: 12 Pages: 6415-6420

    • DOI

      10.1021/am3019993

    • Related Report
      2012 Annual Research Report
    • Peer Reviewed
  • [Journal Article] ソル-ゲル法により作製されるセラミック薄膜の面内応力について2012

    • Author(s)
      幸塚広光
    • Journal Title

      セラミックデータブック

      Volume: 40 Pages: 76-80

    • Related Report
      2012 Annual Research Report
  • [Journal Article] プラスチックス表面に数十~数百nm厚の機能性セラミック薄膜を付与するための新しい湿式成膜技術2012

    • Author(s)
      幸塚広光,内山弘章,福井隆文,高橋充,山野晃裕
    • Journal Title

      プラスチックス

      Volume: 63(5) Pages: 25-29

    • Related Report
      2012 Annual Research Report
  • [Journal Article] ゾル-ゲルウェツトコーティング2012

    • Author(s)
      幸塚広光,内山弘章
    • Journal Title

      ガラス高機能化への加工技術書

      Pages: 231-243

    • Related Report
      2012 Annual Research Report
  • [Presentation] Sol-gel and transfer technique for preparing crystalline oxide thin films on plastic substrates2015

    • Author(s)
      H. Kozuka, S. Tsuboi, N. Amano, K. Izutsu, R. Hamano, H. Uchiyama, T. Fukui and M. Takahashi
    • Organizer
      Materials Science & Technology 2015 (MS&T15)
    • Place of Presentation
      Columbus (U.S.A.)
    • Year and Date
      2015-10-04 – 2015-10-08
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] Fired crystalline oxide thin films on plastic substrates: Sol-gel combined with transfer2015

    • Author(s)
      H. Kozuka, S. Tsuboi, N. Amano, K. Izutsu, R. Hamano, H. Uchiyama, T. Fukui and M. Takahashi
    • Organizer
      The 11th Pacific Rim Conference of Ceramic Societies (PacRim11)
    • Place of Presentation
      Jeju (Korea)
    • Year and Date
      2015-08-30 – 2015-09-04
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] プラスチック材料の表面にセラミック薄膜を作る2015

    • Author(s)
      幸塚広光
    • Organizer
      日本ゾル-ゲル学会第12回セミナー
    • Place of Presentation
      大阪市立工業研究所(大阪府)
    • Year and Date
      2015-06-05
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] ゾル-ゲル法と転写によりプラスチック基板上に作製されるセラミック薄膜の柔軟性に関する基礎的研究2015

    • Author(s)
      幸塚広光,濱野亮介,内山弘章
    • Organizer
      日本セラミックス協会2015年年会
    • Place of Presentation
      岡山大学(岡山県)
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Annual Research Report
  • [Presentation] ゾル-ゲル転写技術によりプラスチック基板上に作製されるセラミック薄膜の密着性に関する基礎的研究2015

    • Author(s)
      天野夏美,幸塚広光,内山弘章
    • Organizer
      日本セラミックス協会2015年年会
    • Place of Presentation
      岡山大学(岡山県)
    • Year and Date
      2015-03-18 – 2015-03-20
    • Related Report
      2014 Annual Research Report
  • [Presentation] ゾル-ゲル法と転写によるプラスチック基板上セラミック薄膜の作製: 剥離補助層がセラミック薄膜の形成に及ぼす影響2015

    • Author(s)
      坪井翔平,幸塚広光,内山弘章
    • Organizer
      第53回セラミックス基礎科学討論会
    • Place of Presentation
      京都テルサ(京都府)
    • Year and Date
      2015-01-08 – 2015-01-09
    • Related Report
      2014 Annual Research Report
  • [Presentation] Sol-gel thin film deposition: Scientific issues and technical proposals2014

    • Author(s)
      H. Kozuka
    • Organizer
      2014 China Sol-gel Symposium, Kunming University of Science and Technology
    • Place of Presentation
      Kunming (P.R. China)
    • Year and Date
      2014-10-17 – 2014-10-20
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] ゲル化を経由するプロセスによる薄膜形成: 課題と提案2014

    • Author(s)
      幸塚広光
    • Organizer
      日本セラミックス協会第27回秋季シンポジウム
    • Place of Presentation
      鹿児島大学(鹿児島県)
    • Year and Date
      2014-09-09 – 2014-09-11
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] ゾル-ゲル法により作製されるセラミック薄膜のプラスチックス湾曲表面への転写2014

    • Author(s)
      井筒功祐,内山弘章,幸塚広光
    • Organizer
      日本ゾル-ゲル学会第12回討論会
    • Place of Presentation
      つくば国際会議場(茨城県)
    • Year and Date
      2014-08-07 – 2014-08-08
    • Related Report
      2014 Annual Research Report
  • [Presentation] ゾル‐ゲル法と転写によるプラスチック基板上へのITO薄膜の作製2014

    • Author(s)
      坪井翔平,内山弘章,幸塚広光
    • Organizer
      日本セラミックス協会第9回関西支部学術講演会
    • Place of Presentation
      大阪府立大学(大阪府)
    • Year and Date
      2014-07-25
    • Related Report
      2014 Annual Research Report
  • [Presentation] Classical sol-gel thin film deposition towards innovations2014

    • Author(s)
      H. Kozuka
    • Organizer
      IX Workshop Italiano Sol-Gel, Parma
    • Place of Presentation
      Parma (Italy)
    • Year and Date
      2014-06-17 – 2014-06-18
    • Related Report
      2014 Annual Research Report
    • Invited
  • [Presentation] Sol-gel-based technique for fabricating ceramic thin films on plastics surface2014

    • Author(s)
      H. Kozuka, T. Fukui, M. Takahashi, S. Tsuboi and H. Uchiyama
    • Organizer
      2014 Materials Research Society Spring Meeting
    • Place of Presentation
      San Francisco (U.S.A.)
    • Year and Date
      2014-04-21 – 2014-04-25
    • Related Report
      2014 Annual Research Report
  • [Presentation] Wet processing and transfer technique for fabricating ceramic thin films on plastics2013

    • Author(s)
      H. Kozuka, T. Fukui, M. Takahashi, H. Uchiyama, S. Tsuboi
    • Organizer
      5th International Symposium on Advanced Ceramics (ISAC-5)
    • Place of Presentation
      Wuhan, P.R.China
    • Related Report
      2013 Annual Research Report
    • Invited
  • [Presentation] Sol-Gel and Transfer Technique for Preparing Ceramic Thin Films on Plastic Substrates2013

    • Author(s)
      H. Kozuka, T. Fukui, M. Takahashi, H. Uchiyama and S. Tsuboi
    • Organizer
      The 30th Japan-Korea International Seminar on Ceramics
    • Place of Presentation
      北九州国際会議場(福岡県小倉市)
    • Related Report
      2013 Annual Research Report
  • [Presentation] プラスチックスを基材とするセラミック薄膜の作製2013

    • Author(s)
      幸塚広光, 内山弘章, 福井隆文, 高橋充, 坪井翔平
    • Organizer
      2013年度セラミックス総合研究会
    • Place of Presentation
      ホテルウェルシーズン浜名湖(静岡県浜松市)
    • Related Report
      2013 Annual Research Report
  • [Presentation] Ceramic thin films on plastics: A versatile route realizing large area as well as patterned coating2013

    • Author(s)
      H. Kozuka, T. Fukui, M. Takahashi, H. Uchiyama and S. Tsuboi
    • Organizer
      XVII International Sol-Gel Conference (Sol-Gel 2013)
    • Place of Presentation
      Madrid, Spain
    • Related Report
      2013 Annual Research Report
  • [Presentation] Ceramic Thin Films on Plastics: A Versatile Sol-Gel Route Realizing Large Area as Well as Patterned Coating2013

    • Author(s)
      H. Kozuka, T. Fukui, M. Takahashi, S. Tsuboi and H. Uchiyama
    • Organizer
      The Eighth International Symposium in Scientific and Technology at Kansai University 2013
    • Place of Presentation
      関西大学千里山キャンパス(吹田市)
    • Related Report
      2013 Annual Research Report
  • [Presentation] Fabrication of Ceramic Thin Films on Plastics: A Versatile Route Utilizing Sol-Gel and Transfer Techniques2013

    • Author(s)
      H. Kozuka, T. Fukui, M. Takahashi, H. Uchiyama and S. Tsuboi
    • Organizer
      12th International Conference on Ceramic Processing Science (ICCPS-12)
    • Place of Presentation
      Portland, U.S.A.
    • Related Report
      2013 Annual Research Report
  • [Presentation] ゾル-ゲルセラミック薄膜のプラスチック基板への加熱転写2013

    • Author(s)
      坪井翔平,内山弘章,幸塚広光
    • Organizer
      日本ゾル-ゲル学会第11回討論会
    • Place of Presentation
      広島大学東広島キャンパス(東広島市)
    • Related Report
      2013 Annual Research Report
  • [Presentation] ゾル-ゲル法により作製される焼成セラミック薄膜をプラスチック基材に転写する技術の開発2013

    • Author(s)
      高橋充,内山弘章,幸塚広光
    • Organizer
      日本セラミックス協会関西支部第8回学術講演会
    • Place of Presentation
      龍谷大学理工学部(滋賀県大津市)
    • Related Report
      2013 Annual Research Report
  • [Presentation] Sol-Gel-Derived Ceramic Thin Films on Plastics: A Versatile Technique Utilizing Transfer Process2013

    • Author(s)
      H. Kozuka, T. Fukui, M. Takahashi, H. Uchiyama, and S. Tsuboi
    • Organizer
      The 10th Pacific Rim Conference on Ceramic and Glass Technology (PacRim10)
    • Place of Presentation
      San Diego, U.S.A.
    • Related Report
      2013 Annual Research Report
  • [Presentation] A Versatile Route to Large Area Ceramic Thin Films on Plastics Using Sol-Gel and Transfer Techniques2013

    • Author(s)
      H. Kozuka, T. Fukui, M. Takahashi, H. Uchiyama, and S. Tsuboi
    • Organizer
      2013 Materials Research Society Spring Meeting
    • Place of Presentation
      San Francisco, U.S.A.
    • Related Report
      2013 Annual Research Report
  • [Presentation] Large Area Crystalline Metal Oxide Thin Films on Plastics: A Versatile Route Utilizing Sol-Gel and Transfer Techniques2013

    • Author(s)
      H. Kozuka, T. Fukui, M. Takahashi, H. Uchiyama, and S. Tsuboi
    • Organizer
      2013 Materials Research Society Spring Meeting
    • Place of Presentation
      San Francisco, U.S.A.
    • Related Report
      2013 Annual Research Report
  • [Presentation] ソル-ゲル法と転写によるプラスチックス表面上セラミック薄膜の作製とパターニング2013

    • Author(s)
      幸塚広光,福井隆文,高橋充,坪井翔平,内山弘章
    • Organizer
      日本セラミックス協会第51回セラミックス基礎科学討論会
    • Place of Presentation
      仙台市
    • Related Report
      2012 Annual Research Report
  • [Presentation] セラミック薄膜をプラスチックスの表面に作製する技術の提案2012

    • Author(s)
      幸塚広光、福井隆文、高橋充、内山弘章、山野晃裕
    • Organizer
      日本セラミックス協会関西支部第7回学術講演会
    • Place of Presentation
      神戸大学百年記念館(兵庫県)
    • Year and Date
      2012-07-13
    • Related Report
      2012 Annual Research Report
  • [Presentation] ソル-ゲル法により作製されるITO焼成膜のプラスチック基材への転写2012

    • Author(s)
      福井隆文、内山弘章、幸塚広光
    • Organizer
      日本セラミックス協会関西支部第7回学術講演会
    • Place of Presentation
      神戸大学百年記念館(兵庫県)
    • Year and Date
      2012-07-13
    • Related Report
      2012 Annual Research Report
  • [Presentation] Ceramic thin films on plastics: a versatile solution-route towards roll-to-roll processing2012

    • Author(s)
      H. Kozuka, T. Fukui, M. Takahashi, H. Uchiyama, S. Tsuboi, A. Yamano
    • Organizer
      2012 Materials Research Society Fall Meeting
    • Place of Presentation
      Boston, USA
    • Related Report
      2012 Annual Research Report
  • [Presentation] A new versatile route to ceramic thin films on plastics: a solution-based"high-temperature" processing2012

    • Author(s)
      H. Kozuka, T. Fukui, M. Takahashi, H. Uchiyama and A. Yamano.
    • Organizer
      2nd International Conference on Competitive Materials and Technology Processes
    • Place of Presentation
      Miskolc-Lillaftired, Hugary
    • Related Report
      2012 Annual Research Report
  • [Presentation] プラスチック基材表面に焼成ITO薄膜を転写する技術の開発2012

    • Author(s)
      福井隆文、内山弘章、幸塚広光
    • Organizer
      日本セラミックス協会第25回秋季シンポジウム
    • Place of Presentation
      名古屋大学東山キャンパス(愛知県)
    • Related Report
      2012 Annual Research Report
  • [Presentation] ソル-ゲル法により作製されるセラミック薄膜の種々のプラスチック基材への転写性2012

    • Author(s)
      高橋充、内山弘章、幸塚広光
    • Organizer
      日本セラミックス協会第25回秋季シンポジウム
    • Place of Presentation
      名古屋大学東山キャンパス(愛知県)
    • Related Report
      2012 Annual Research Report
  • [Presentation] プラスチックスを基材とする機能性セラミック薄膜作製技術の提案2012

    • Author(s)
      幸塚広光、福井隆文、高橋充、内山弘章、山野晃裕
    • Organizer
      日本ソル-ゲル学会第10回討論会
    • Place of Presentation
      慶應義塾大学創想館(神奈川県)
    • Related Report
      2012 Annual Research Report
  • [Presentation] ソル-ゲル法により作製されるセラミック薄膜の種々のプラスチック基材への転写性2012

    • Author(s)
      高橋充、内山弘章、幸塚広光
    • Organizer
      日本ソル-ゲル学会第10回討論会
    • Place of Presentation
      慶應義塾大学創想館(神奈川県)
    • Related Report
      2012 Annual Research Report
  • [Presentation] Deposition of functional crystalline metal oxide thin films on plastic substrates via sol-gel "firing"process2012

    • Author(s)
      H. Kozuka, T. Fukui, A. Yamano, H. Uchiyama and M.Takahashi
    • Organizer
      10th CMCEE (International Symposium on Ceramic Materials and Components for Energy and Environmental Applications)
    • Place of Presentation
      Dresden, Germany(招待講演)
    • Related Report
      2012 Annual Research Report
  • [Presentation] Crystalline Metal Oxide Thin Films on Plastics: A Potential Deposition Technique with Sol-Gel-Based Firing Process2012

    • Author(s)
      H. Kozuka, A. Yamano, T. Fukui, H. Uchiyama, M. Takahashi, M. Yoki, T. Akase
    • Organizer
      2012 Materials Research Society Spring Meeting
    • Place of Presentation
      San Francisco, USA(招待講演)
    • Related Report
      2012 Annual Research Report
  • [Remarks] セラミックス工学研究室ホームページ

    • URL

      http://www.chemmater.kansai-u.ac.jp/ceramics/TOP.htm

    • Related Report
      2014 Annual Research Report
  • [Remarks] 幸塚広光 関西大学学術情報システム

    • URL

      http://gakujo.kansai-u.ac.jp/profile/ja/ddd30417cvc594+x13d0fc16a0f0.html

    • Related Report
      2014 Annual Research Report
  • [Remarks]

    • URL

      http://www.chemmater.kansai-u.ac.jp/ceramics/TOP.htm

    • Related Report
      2012 Annual Research Report

URL: 

Published: 2012-04-24   Modified: 2019-07-29  

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