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Catalyst-type optical fiber sensors based on fiber Bragg gratings for hydrogen detection

Research Project

Project/Area Number 24560516
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Measurement engineering
Research InstitutionYokohama National University

Principal Investigator

OKAZAKI Shinji  横浜国立大学, 工学(系)研究科(研究院), 准教授 (50293171)

Co-Investigator(Kenkyū-buntansha) MIZUTANI Tadahito  宇宙航空研究開発機構, つくば宇宙センター研究開発本部, 研究員 (00401232)
MARU Yusuke  宇宙航空研究開発機構, 宇宙科学研究所, 助教 (20524101)
Project Period (FY) 2012-04-01 – 2015-03-31
Project Status Completed (Fiscal Year 2014)
Budget Amount *help
¥5,200,000 (Direct Cost: ¥4,000,000、Indirect Cost: ¥1,200,000)
Fiscal Year 2014: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Fiscal Year 2013: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Fiscal Year 2012: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Keywordsセンシングデバイス / 光ファイバガスセンサ / ファイバーブラッググレーティング / 水素漏えい検知 / 白金担持酸化タングステン / 白金担持シリカ / 白金触媒担持酸化タングステン / 白金触媒担持シリカ
Outline of Final Research Achievements

A highly sensitive hydrogen gas sensor based on a fiber Bragg grating (FBG) has been developed. Various potential hydrogen sensor materials were screened by assessing the catalytic activities of oxide-supported platinum particles prepared by a sol-gel method. It was determined that a Pt/SiO2 film was the most appropriate sensor material; exposure of this film to 4 vol% H2 in humid air for 30 s at room temperature produced a temperature change of 65 K. In addition, the Pt/SiO2 was able to respond to a concentration as low as 0.1 vol% H2 in dry air. Two types of sensor structures were fabricated and evaluated. The device incorporating a quartz glass substrate covered with the sensor film on one side was able to detect 0.4 vol% H2 in dry air at room temperature with a response time of approximately 25 min. The other device, in which the sensor film was immobilized on the periphery of the FBG section, exhibited rapid response to 0.6 vol% H2 within 20 s.

Report

(4 results)
  • 2014 Annual Research Report   Final Research Report ( PDF )
  • 2013 Research-status Report
  • 2012 Research-status Report
  • Research Products

    (7 results)

All 2015 2014 2013 2012

All Journal Article (2 results) (of which Peer Reviewed: 2 results,  Acknowledgement Compliant: 1 results) Presentation (5 results)

  • [Journal Article] Catalyst-type-an optical fiber sensor for hydrogen leakage basedon fiber Bragg gratings2015

    • Author(s)
      Satoshi Masuzawa, Shinji Okazaki, Yusuke Marb, Tadahito Mizutani
    • Journal Title

      Sensors and Actuators B: Chemical

      Volume: - Pages: 151-157

    • DOI

      10.1016/j.snb.2014.10.026

    • Related Report
      2014 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Sensing Characteristics of a Fiber Bragg Grating Hydrogen Gas Sensor Using Sol-gel Derived Pt/WO3 Film2012

    • Author(s)
      S. Okazaki, Y. Maru, and T. Mizutani
    • Journal Title

      ECS transaction

      Volume: 50 (12) Pages: 289-294

    • Related Report
      2012 Research-status Report
    • Peer Reviewed
  • [Presentation] A fiber Bragg grating sensor for hydrogen leakage detection based on catalytic oxidation heat2014

    • Author(s)
      S. Masuzawa, S. Okazaki, Y. Maru, T. Mizutani
    • Organizer
      15th International meeing on chemical sensors
    • Place of Presentation
      Buenos Aires, Argentina
    • Related Report
      2013 Research-status Report
  • [Presentation] 貴金属触媒担持酸化物を用いた光ファイバグレーティング水素センサの開発2013

    • Author(s)
      舛澤慧、岡崎慎司、丸祐介、水谷忠均
    • Organizer
      第55回化学センサ研究発表会
    • Place of Presentation
      東京・東京工業大学
    • Related Report
      2013 Research-status Report
  • [Presentation] Development of a fiber Bragg grating sensor for hydrogen leak detection using noble metal catalyst2013

    • Author(s)
      S. Masuzawa, S. Okazaki, Y. Maru, T. Mizutani
    • Organizer
      The 10th Asian Conference on Chemical Sensors
    • Place of Presentation
      Chiang Mai, Thailand
    • Related Report
      2013 Research-status Report
  • [Presentation] 光ファイバグレーティングを用いた反応熱検出型水素センサの開発2013

    • Author(s)
      舛澤慧、岡崎慎司、丸祐介、水谷忠均
    • Organizer
      第54回化学センサ研究発表会
    • Place of Presentation
      仙台・東北大学
    • Related Report
      2012 Research-status Report
  • [Presentation] Sensing characteristics of a fiber Bragg grating hydrogen gas sensor using sol-gel derived Pt/WO3 film2012

    • Author(s)
      S. Okazaki, Y. Maru, T. Mizutani
    • Organizer
      PRIME 2012 (222nd ECS Meeting)
    • Place of Presentation
      Honolulu, HI, USA
    • Related Report
      2012 Research-status Report

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Published: 2013-05-31   Modified: 2019-07-29  

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