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Pretreatment Technique for Environmental Tritium Analysis with Microwave Heating Method

Research Project

Project/Area Number 26340032
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Risk sciences of radiation and chemicals
Research InstitutionNational Institute for Fusion Science

Principal Investigator

Akata Naofumi  核融合科学研究所, ヘリカル研究部, 准教授 (10715478)

Co-Investigator(Kenkyū-buntansha) 高山 定次  核融合科学研究所, ヘリカル研究部, 准教授 (40435516)
Co-Investigator(Renkei-kenkyūsha) Tanaka Masahiro  核融合科学研究所, 准教授 (00435520)
Project Period (FY) 2014-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥4,680,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥1,080,000)
Fiscal Year 2016: ¥780,000 (Direct Cost: ¥600,000、Indirect Cost: ¥180,000)
Fiscal Year 2015: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2014: ¥2,470,000 (Direct Cost: ¥1,900,000、Indirect Cost: ¥570,000)
Keywordstritium / microwave / FWT / OBT / トリチウム / 迅速化 / マイクロ波 / 核融合
Outline of Final Research Achievements

To understand the behavior of the combustion and drying of organic samples for tritium analysis, we conducted TG/DTA analysis of pine needle samples. Next, we tried the water recovery from fresh pine needle samples by the multi-mode microwave heating system. It was provided to good recovery yield achieved more than 97% under these experimental conditions.
We made a new microwave heating furnace based on the results of preliminary test. As the results, we were able to recover the FWT samples in a few hours. And we were able to be combusted organic matter in approximately 1 hour. And we were able to recover the OBT sample. FWT and OBT sample water contain no organic matter. Therefore, we can analyze directly without distillation. These result shows more preferable for the pretreatment of organic samples by microwave irradiation method than the conventional method.

Report

(4 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Research-status Report
  • 2014 Research-status Report
  • Research Products

    (16 results)

All 2016 2015 2014

All Journal Article (7 results) (of which Peer Reviewed: 5 results,  Open Access: 1 results,  Acknowledgement Compliant: 2 results) Presentation (9 results) (of which Int'l Joint Research: 3 results)

  • [Journal Article] A simple method for sampling and analysis of particulate, inorganic gaseous and organic gaseous halogens in the atmosphere2016

    • Author(s)
      Akata, N., Tsukada, H., Takahashi, T., Fukutani, S.
    • Journal Title

      Radiation Environment Medicine

      Volume: 5 Pages: 29-32

    • NAID

      40020922505

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] A new pretreatment technique for environmental tritium analysis with microwave heating method2016

    • Author(s)
      Akata, N., Tanaka, M., Takayama, S., Kakiuchi, H., Tamari, T. and Sano, S.
    • Journal Title

      Plasma and Fusion Research

      Volume: 11

    • NAID

      130005243516

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Long-term monitoring of tritium concentration in environmental water samples collected at Tono area, Japan2016

    • Author(s)
      Akata, N., Tanaka, M., Kato, H., Yamanishi, H., Kakiuchi, H., Hayashi, H., Miyake, H., Nishimura, K.
    • Journal Title

      Plasma and Fusion Research

      Volume: 11

    • NAID

      130005311642

    • Related Report
      2015 Research-status Report
    • Peer Reviewed
  • [Journal Article] 環境水試料の水素同位体測定法と雪氷研究への応用2015

    • Author(s)
      赤田尚史,田中将裕,池本憲弘,島長義,柿内秀樹,柳澤文孝
    • Journal Title

      東北の雪と生活

      Volume: 30 Pages: 47-50

    • Related Report
      2015 Research-status Report
    • Acknowledgement Compliant
  • [Journal Article] 天然レベルの環境水中トリチウム分析2015

    • Author(s)
      赤田尚史,柿内秀樹
    • Journal Title

      放地研特別寄稿シリーズ

      Volume: 106 Pages: 1-5

    • Related Report
      2015 Research-status Report
  • [Journal Article] FWT and OBT concentration in pine needle samples collected at Toki, Japan (1998-2012)2015

    • Author(s)
      Akata, N., Kakiuchi, H., Tamari, T., Tanaka, M., Kawano, T., Miyake, H., Nishimura, K.
    • Journal Title

      Radiation Protection Dosimetry

      Volume: - Issue: 1-3 Pages: 210-214

    • DOI

      10.1093/rpd/ncv246

    • Related Report
      2014 Research-status Report
    • Peer Reviewed
  • [Journal Article] Behavior of magnetization in magnetic oxide compact sintered by magbetic and electric field of microwave irradiation2015

    • Author(s)
      Takayama, S., Sano, S., Sato, M.
    • Journal Title

      Trans. Mat. Res. Sox.Japan

      Volume: 40 Pages: 65-68

    • Related Report
      2014 Research-status Report
    • Peer Reviewed
  • [Presentation] 環境条件下における疎水性酸化触媒の分子状水素転換率評価2016

    • Author(s)
      池本憲弘,田中将裕,赤田尚史,佐瀬卓也,柿内秀樹
    • Organizer
      日本放射線安全管理学会第15回学術大会
    • Place of Presentation
      岡山市
    • Year and Date
      2016-11-30
    • Related Report
      2016 Annual Research Report
  • [Presentation] マイクロ波を応用したトリチウム分析の為の前処理法の開発2016

    • Author(s)
      高山定次,赤田尚史,田中将裕,佐野三郎
    • Organizer
      第10回日本電磁波エネルギー応用学会シンポジウム
    • Place of Presentation
      仙台市
    • Year and Date
      2016-10-13
    • Related Report
      2016 Annual Research Report
  • [Presentation] Tritium concentration and δD・δ18O composition of monthly precipitation collected at Toki, Japan2016

    • Author(s)
      Akata, N., Hasegawa, H., Sugihara, S., Tanaka, M., Furukawa, M., Kakiuchi, H.
    • Organizer
      V. Terrestrial Radioisotopes in Environment International Conference on Environmental Protection
    • Place of Presentation
      ベスプレーム,ハンガリー
    • Year and Date
      2016-05-17
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Concentration of tritium in precipitation and inland waters collected in Okinawa Island, southwestern part of Japan2016

    • Author(s)
      Furukawa, M., Ishizu, Y., Tsukayama, J., Ikemoto, N., Akata, N., Tanaka, M., Sanada, T.
    • Organizer
      V. Terrestrial Radioisotopes in Environment International Conference on Environmental Protection
    • Place of Presentation
      ベスプレーム,ハンガリー
    • Year and Date
      2016-05-17
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] A new pretreatment technique for environmental tritium analysis with microwave heating method2015

    • Author(s)
      Akata, N., Tanaka, M., Takayama, S., Kakiuchi, H., Tamari, To and Sano, S.
    • Organizer
      25th International Toki Conference
    • Place of Presentation
      セラトピア土岐
    • Year and Date
      2015-11-03
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] 固体高分子膜電解濃縮装置におけるトリチウム分離係数の温度依存性2015

    • Author(s)
      池本憲弘,赤田尚史,田中将裕,島長義,柿内秀樹
    • Organizer
      日本保健物理学会第48回研究発表会
    • Place of Presentation
      首都大学東京
    • Year and Date
      2015-07-02
    • Related Report
      2015 Research-status Report
  • [Presentation] 環境水試料の水素同位体測定法と雪氷研究への応用2015

    • Author(s)
      赤田尚史,田中将裕,池本憲弘,島長義,柿内秀樹,柳澤文孝
    • Organizer
      2015年度日本雪氷学会東北支部大会
    • Place of Presentation
      日本大学工学部
    • Year and Date
      2015-05-15 – 2015-05-16
    • Related Report
      2014 Research-status Report
  • [Presentation] FWT and OBT concentration in pine needle samples collected at Toki, Japan (1998-2012)2014

    • Author(s)
      Akata, N., Kakiuchi, H., Tamari, T., Tanaka, M., Kawano, T., Miyake, H., Nishimura, K.
    • Organizer
      The 9th International Symposium on the Natural Radiation Environment (NRE-IX)
    • Place of Presentation
      弘前キャッスルホテル
    • Year and Date
      2014-09-22 – 2014-09-26
    • Related Report
      2014 Research-status Report
  • [Presentation] マイクロ波を利用した環境試料中トリチウムの分析前処理手法に関する基礎検討2014

    • Author(s)
      赤田尚史,高山定次,田中将裕,玉利俊哉,柿内秀樹,佐野三郎
    • Organizer
      2014日本放射化学会年会・第58回放射化学討論会
    • Place of Presentation
      名古屋大学
    • Year and Date
      2014-09-11 – 2014-09-13
    • Related Report
      2014 Research-status Report

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Published: 2014-04-04   Modified: 2018-03-22  

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